Synthesis of γ-(Al1-xFex)2O3 solid solutions from oxinate precursors and formation of carbon nanotubes from the solid solutions using methane or ethylene as carbon source
This work reports for the first time the synthesis of γ-(Al1-xFex)2O3 solid solutions with a high specific surface area (200-230 m2/g) by the decomposition of metal oxinate [(Al1-xFex)(C9H6ON)3] and investigated the potential of these materials as catalysts for the synthesis of carbon nanotubes by c...
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| Published in: | Journal of materials research Vol. 23; no. 11; pp. 3096 - 3111 |
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| Main Authors: | , , , , , , , |
| Format: | Journal Article |
| Language: | English |
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Cambridge University Press
01-11-2008
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| Abstract | This work reports for the first time the synthesis of γ-(Al1-xFex)2O3 solid solutions with a high specific surface area (200-230 m2/g) by the decomposition of metal oxinate [(Al1-xFex)(C9H6ON)3] and investigated the potential of these materials as catalysts for the synthesis of carbon nanotubes by catalytic chemical vapor deposition using methane or ethylene as carbon the source. The nanocomposite powders prepared by reduction in H2-CH4 contain carbon nanotubes (CNTs), which are mostly double-walled but also contain a fair amount of undesirable carbon nanofibers, hollow carbon particles, and metal particles covered by carbon layers. Moreover, abundant metallic particles are observed to cover the surfaces of the matrix grains. By contrast, the nanocomposite powders prepared by reduction in N2-C2H4 are not fully reduced, and the CNTs are much more abundant and homogeneous. However, they are multiwalled CNTs with a significant proportion of defects. The powders were studied by several techniques including Mössbauer spectroscopy and electron microscopy. |
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| AbstractList | This work reports for the first time the synthesis of γ-(Al1-xFex)2O3 solid solutions with a high specific surface area (200-230 m2/g) by the decomposition of metal oxinate [(Al1-xFex)(C9H6ON)3] and investigated the potential of these materials as catalysts for the synthesis of carbon nanotubes by catalytic chemical vapor deposition using methane or ethylene as carbon the source. The nanocomposite powders prepared by reduction in H2-CH4 contain carbon nanotubes (CNTs), which are mostly double-walled but also contain a fair amount of undesirable carbon nanofibers, hollow carbon particles, and metal particles covered by carbon layers. Moreover, abundant metallic particles are observed to cover the surfaces of the matrix grains. By contrast, the nanocomposite powders prepared by reduction in N2-C2H4 are not fully reduced, and the CNTs are much more abundant and homogeneous. However, they are multiwalled CNTs with a significant proportion of defects. The powders were studied by several techniques including Mössbauer spectroscopy and electron microscopy. This work reports for the first time the synthesis of ?-(Al1-xFex)2O3 solid solutions with a high specific surface area (200-230 m2/g) by the decomposition of metal oxinate [(Al1-xFex)(C9H6ON)3] and investigated the potential of these materials as catalysts for the synthesis of carbon nanotubes by catalytic chemical vapor deposition using methane or ethylene as carbon the source. The nanocomposite powders prepared by reduction in H2-CH4 contain carbon nanotubes (CNTs), which are mostly double-walled but also contain a fair amount of undesirable carbon nanofibers, hollow carbon particles, and metal particles covered by carbon layers. Moreover, abundant metallic particles are observed to cover the surfaces of the matrix grains. By contrast, the nanocomposite powders prepared by reduction in N2-C2H4 are not fully reduced, and the CNTs are much more abundant and homogeneous. However, they are multiwalled CNTs with a significant proportion of defects. The powders were studied by several techniques including Mössbauer spectroscopy and electron microscopy. This work reports for the first time the synthesis of γ-(Al 1-x Fe x ) 2 O 3 solid solutions with a high specific surface area (200-230 m 2 /g) by the decomposition of metal oxinate [(Al 1-x Fe x )(C 9 H 6 ON) 3 ] and investigated the potential of these materials as catalysts for the synthesis of carbon nanotubes by catalytic chemical vapor deposition using methane or ethylene as carbon the source. The nanocomposite powders prepared by reduction in H 2 -CH 4 contain carbon nanotubes (CNTs), which are mostly double-walled but also contain a fair amount of undesirable carbon nanofibers, hollow carbon particles, and metal particles covered by carbon layers. Moreover, abundant metallic particles are observed to cover the surfaces of the matrix grains. By contrast, the nanocomposite powders prepared by reduction in N 2 -C 2 H 4 are not fully reduced, and the CNTs are much more abundant and homogeneous. However, they are multiwalled CNTs with a significant proportion of defects. The powders were studied by several techniques including Mössbauer spectroscopy and electron microscopy. |
| Author | Vandenberghe, Robert E. Weibel, Alicia Laurent, Christophe De Grave, Eddy de Resende, Valdirene G. da Costa, Geraldo M. Peigney, Alain Cordier, Anne |
| Author_xml | – sequence: 1 givenname: Valdirene G. surname: de Resende fullname: de Resende, Valdirene G. organization: Department of Subatomic and Radiation Physics, University of Ghent, B-9000 Gent, Belgium; and CIRIMAT UMR CNRS 5085/LCMIE, Centre Interuniversitaire de Recherche et d’Ingénierie des Matériaux, Université Paul-Sabatier, 31062 Toulouse cedex 9, France – sequence: 2 givenname: Anne surname: Cordier fullname: Cordier, Anne organization: CIRIMAT UMR CNRS 5085/LCMIE, Centre Interuniversitaire de Recherche et d’Ingénierie des Matériaux, Université Paul-Sabatier, 31062 Toulouse cedex 9, France – sequence: 3 givenname: Eddy surname: De Grave fullname: De Grave, Eddy organization: Department of Subatomic and Radiation Physics, University of Ghent, B-9000 Gent, Belgium – sequence: 4 givenname: Alicia surname: Weibel fullname: Weibel, Alicia organization: CIRIMAT UMR CNRS 5085/LCMIE, Centre Interuniversitaire de Recherche et d’Ingénierie des Matériaux, Université Paul-Sabatier, 31062 Toulouse cedex 9, France – sequence: 5 givenname: Alain surname: Peigney fullname: Peigney, Alain organization: CIRIMAT UMR CNRS 5085/LCMIE, Centre Interuniversitaire de Recherche et d’Ingénierie des Matériaux, Université Paul-Sabatier, 31062 Toulouse cedex 9, France – sequence: 6 givenname: Geraldo M. surname: da Costa fullname: da Costa, Geraldo M. organization: Chemistry Department, Federal University of Ouro Preto, 35400-000, Ouro Preto (MG), Brazil – sequence: 7 givenname: Christophe surname: Laurent fullname: Laurent, Christophe organization: CIRIMAT UMR CNRS 5085/LCMIE, Centre Interuniversitaire de Recherche et d’Ingénierie des Matériaux, Université Paul-Sabatier, 31062 Toulouse cedex 9, France – sequence: 8 givenname: Robert E. surname: Vandenberghe fullname: Vandenberghe, Robert E. organization: Department of Subatomic and Radiation Physics, University of Ghent, B-9000 Gent, Belgium |
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| Keywords | Nanoscale Scanning electron microscopy (SEM) Transmission electron microscopy (TEM) Matériaux |
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| Snippet | This work reports for the first time the synthesis of γ-(Al1-xFex)2O3 solid solutions with a high specific surface area (200-230 m2/g) by the decomposition of... This work reports for the first time the synthesis of γ-(Al 1-x Fe x ) 2 O 3 solid solutions with a high specific surface area (200-230 m 2 /g) by the... This work reports for the first time the synthesis of ?-(Al1-xFex)2O3 solid solutions with a high specific surface area (200-230 m2/g) by the decomposition of... |
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| SubjectTerms | Applied and Technical Physics Biomaterials Chemical Sciences Inorganic Chemistry Material chemistry Materials Engineering Materials Science Nanoscale Nanotechnology Scanning electron microscopy (SEM) Transmission electron microscopy (TEM) |
| Title | Synthesis of γ-(Al1-xFex)2O3 solid solutions from oxinate precursors and formation of carbon nanotubes from the solid solutions using methane or ethylene as carbon source |
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