Vacancies-engineered and heteroatoms-regulated N-doped porous carbon aerogel for ultrahigh microwave absorption

Carbon materials are expected to be the promising candidates for lightweight absorbers, however, structure design and composition control still possess a formidable challenge. Herein, we develop a controllable method to synthesize vacancies-engineered and heteroatoms-regulated N-doped porous carbon...

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Published in:	Carbon (New York) Vol. 169; pp. 276 - 287
Main Authors:	Liu, Panbo, Gao, Sai, Chen, Chen, Zhou, Fengtao, Meng, Zhuoyue, Huang, Ying, Wang, Yang
Format:	Journal Article
Language:	English
Published:	New York Elsevier Ltd 01-11-2020 Elsevier BV
Subjects:	Aerogels Carbon Carbon aerogel Composition Conduction losses Controllability Gelatin Heteroatoms Imines Impedance matching Lightweight Microwave absorbers Microwave absorption Microwave heating Nanotubes Organic polymer aerogel Polymers Porous materials Pyrolysis Stability Synthesis Vacancies Vacancies Microwave absorption Carbon aerogel Heteroatoms Organic polymer aerogel
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Abstract	Carbon materials are expected to be the promising candidates for lightweight absorbers, however, structure design and composition control still possess a formidable challenge. Herein, we develop a controllable method to synthesize vacancies-engineered and heteroatoms-regulated N-doped porous carbon aerogel (NPCA), involving the formation of the gelatin of rigiditied organic polymer aerogel via a Schiff-base reaction and a subsequent pyrolysis process. By increasing the pyrolysis temperature, the proportion of N heteroatoms decreases while more vacancies can be generated, resulting in adjusted microwave absorption performance. As microwave absorber, the NPCA exhibits ultrahigh absorption performance because of matched impedance, interconnected conductive network and multiple scattering. Balancing the conduction loss and dipolar/interfacial polarization, an optimal reflection loss of −61.7 dB is achieved at 2.6 mm and the effective bandwidth is as wide as 11.7 GHz when the thickness ranges from 1 mm to 4 mm for NPCA-800. Considering the outstanding performance and precise controllability, we believe that the synthesized carbon aerogel can be used as lightweight microwave absorbers and this strategy provides the most cutting-edge topic for the fabrication of carbon aerogel derived from organic polymer aerogel with tunable composition/structure. [Display omitted]
AbstractList	Carbon materials are expected to be the promising candidates for lightweight absorbers, however, structure design and composition control still possess a formidable challenge. Herein, we develop a controllable method to synthesize vacancies-engineered and heteroatoms-regulated N-doped porous carbon aerogel (NPCA), involving the formation of the gelatin of rigiditied organic polymer aerogel via a Schiff-base reaction and a subsequent pyrolysis process. By increasing the pyrolysis temperature, the proportion of N heteroatoms decreases while more vacancies can be generated, resulting in adjusted microwave absorption performance. As microwave absorber, the NPCA exhibits ultrahigh absorption performance because of matched impedance, interconnected conductive network and multiple scattering. Balancing the conduction loss and dipolar/interfacial polarization, an optimal reflection loss of −61.7 dB is achieved at 2.6 mm and the effective bandwidth is as wide as 11.7 GHz when the thickness ranges from 1 mm to 4 mm for NPCA-800. Considering the outstanding performance and precise controllability, we believe that the synthesized carbon aerogel can be used as lightweight microwave absorbers and this strategy provides the most cutting-edge topic for the fabrication of carbon aerogel derived from organic polymer aerogel with tunable composition/structure. Carbon materials are expected to be the promising candidates for lightweight absorbers, however, structure design and composition control still possess a formidable challenge. Herein, we develop a controllable method to synthesize vacancies-engineered and heteroatoms-regulated N-doped porous carbon aerogel (NPCA), involving the formation of the gelatin of rigiditied organic polymer aerogel via a Schiff-base reaction and a subsequent pyrolysis process. By increasing the pyrolysis temperature, the proportion of N heteroatoms decreases while more vacancies can be generated, resulting in adjusted microwave absorption performance. As microwave absorber, the NPCA exhibits ultrahigh absorption performance because of matched impedance, interconnected conductive network and multiple scattering. Balancing the conduction loss and dipolar/interfacial polarization, an optimal reflection loss of −61.7 dB is achieved at 2.6 mm and the effective bandwidth is as wide as 11.7 GHz when the thickness ranges from 1 mm to 4 mm for NPCA-800. Considering the outstanding performance and precise controllability, we believe that the synthesized carbon aerogel can be used as lightweight microwave absorbers and this strategy provides the most cutting-edge topic for the fabrication of carbon aerogel derived from organic polymer aerogel with tunable composition/structure. [Display omitted]
Author	Wang, Yang Chen, Chen Liu, Panbo Gao, Sai Zhou, Fengtao Meng, Zhuoyue Huang, Ying
Author_xml	– sequence: 1 givenname: Panbo surname: Liu fullname: Liu, Panbo email: liupanbo@nwpu.edu.cn organization: School of Chemistry and Chemical Engineering, Northwestern Polytechnical University, Xi’an, 710129, China – sequence: 2 givenname: Sai surname: Gao fullname: Gao, Sai organization: School of Chemistry and Chemical Engineering, Northwestern Polytechnical University, Xi’an, 710129, China – sequence: 3 givenname: Chen surname: Chen fullname: Chen, Chen organization: School of Chemistry and Chemical Engineering, Northwestern Polytechnical University, Xi’an, 710129, China – sequence: 4 givenname: Fengtao surname: Zhou fullname: Zhou, Fengtao email: fengtaozhou@163.com organization: School of Pharmacy, Jinan University, Guangzhou, 510632, China – sequence: 5 givenname: Zhuoyue surname: Meng fullname: Meng, Zhuoyue organization: College of Chemistry and Chemical Engineering, Xi’an University of Science and Technology, Xi’an, 710054, China – sequence: 6 givenname: Ying surname: Huang fullname: Huang, Ying organization: School of Chemistry and Chemical Engineering, Northwestern Polytechnical University, Xi’an, 710129, China – sequence: 7 givenname: Yang surname: Wang fullname: Wang, Yang organization: School of Chemistry and Chemical Engineering, Northwestern Polytechnical University, Xi’an, 710129, China
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Snippet	Carbon materials are expected to be the promising candidates for lightweight absorbers, however, structure design and composition control still possess a...
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SubjectTerms	Aerogels Carbon Carbon aerogel Composition Conduction losses Controllability Gelatin Heteroatoms Imines Impedance matching Lightweight Microwave absorbers Microwave absorption Microwave heating Nanotubes Organic polymer aerogel Polymers Porous materials Pyrolysis Stability Synthesis Vacancies
Title	Vacancies-engineered and heteroatoms-regulated N-doped porous carbon aerogel for ultrahigh microwave absorption
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