TiO2-based nanopowders obtained from different Ti-alkoxides

Pure TiO2 and S-doped TiO2 sol-gel nanopowders were prepared by controlled hydrolysis-condensation of titanium alkoxides. The influence of different Ti-alkoxides (tetraethyl-, tetraisopropyl- and tetrabutyl-orthotitanate) used in obtaining TiO2 porous materials in similar conditions (water/alkoxide...

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Published in:	Journal of thermal analysis and calorimetry Vol. 88; no. 1; pp. 171 - 176
Main Authors:	CRISAN, M, BRAILEANU, Ana, RAILEANU, M, CRISAN, D, TEODORESCU, V. S, BIRJEGA, R, MARINESCU, V. E, MADARASZ, J, POKOL, G
Format:	Conference Proceeding Journal Article
Language:	English
Published:	Dordrecht Springer 01-04-2007
Subjects:	Chemistry Colloidal state and disperse state Exact sciences and technology General and physical chemistry General, apparatus, technics of preparation Titanium IV Oxides Nanoparticle TiO2 nanopowders Doped materials Fabrication property relation X ray diffraction Surface structure Transmission electron microscopy Sol gel process Morphology Organic salt Surface properties Alkoxide Thermal analysis Surface area S-doped TiO2 sol-gel method
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Abstract	Pure TiO2 and S-doped TiO2 sol-gel nanopowders were prepared by controlled hydrolysis-condensation of titanium alkoxides. The influence of different Ti-alkoxides (tetraethyl-, tetraisopropyl- and tetrabutyl-orthotitanate) used in obtaining TiO2 porous materials in similar conditions (water/alkoxide ratio, solvent/alkoxide ratio, pH and temperature of reaction) has been investigated. The relationship between the synthesis conditions and the properties of titania nanosized powders, such as thermal stability, phase composition, crystallinity, morphology and size of particles, BET surface area and the influence of dopant was investigated. The nature of the alkyl group strongly influences the main characteristics of the obtained oxide powders, fact which is pointed out by thermal analysis, X-ray diffraction, TEM and BET surface area measurements.
AbstractList	Pure TiO2 and S-doped TiO2 sol-gel nanopowders were prepared by controlled hydrolysis-condensation of titanium alkoxides. The influence of different Ti-alkoxides (tetraethyl-, tetraisopropyl- and tetrabutyl-orthotitanate) used in obtaining TiO2 porous materials in similar conditions (water/alkoxide ratio, solvent/alkoxide ratio, pH and temperature of reaction) has been investigated. The relationship between the synthesis conditions and the properties of titania nanosized powders, such as thermal stability, phase composition, crystallinity, morphology and size of particles, BET surface area and the influence of dopant was investigated. The nature of the alkyl group strongly influences the main characteristics of the obtained oxide powders, fact which is pointed out by thermal analysis, X-ray diffraction, TEM and BET surface area measurements.
Author	CRISAN, D MADARASZ, J TEODORESCU, V. S BRAILEANU, Ana POKOL, G CRISAN, M RAILEANU, M BIRJEGA, R MARINESCU, V. E
Author_xml	– sequence: 1 givenname: M surname: CRISAN fullname: CRISAN, M organization: Roumanian Academy, Institute of Physical Chemistry Ilie Murgulescu, 202 Splaiul Independen tei, 060021 Bucharest, Romania – sequence: 2 givenname: Ana surname: BRAILEANU fullname: BRAILEANU, Ana organization: Roumanian Academy, Institute of Physical Chemistry Ilie Murgulescu, 202 Splaiul Independen tei, 060021 Bucharest, Romania – sequence: 3 givenname: M surname: RAILEANU fullname: RAILEANU, M organization: Roumanian Academy, Institute of Physical Chemistry Ilie Murgulescu, 202 Splaiul Independen tei, 060021 Bucharest, Romania – sequence: 4 givenname: D surname: CRISAN fullname: CRISAN, D organization: Roumanian Academy, Institute of Physical Chemistry Ilie Murgulescu, 202 Splaiul Independen tei, 060021 Bucharest, Romania – sequence: 5 givenname: V. S surname: TEODORESCU fullname: TEODORESCU, V. S organization: National Institute for Physics of Materials, P.O. Box MG 07, Bucharest, Magurele, Romania – sequence: 6 givenname: R surname: BIRJEGA fullname: BIRJEGA, R organization: National Institute for Lasers, Plasma and Radiation Physics, PO Box MG-36, Bucharest, Romania – sequence: 7 givenname: V. E surname: MARINESCU fullname: MARINESCU, V. E organization: INCDIE ICPE-CA, 313 Spl. Unirii, 030138 Bucharest, Romania – sequence: 8 givenname: J surname: MADARASZ fullname: MADARASZ, J organization: Budapest University of Technology and Economics, Institute of General and Analytical Chemistry, Szt. Gellért tér 4, 1521 Budapest, Hungary – sequence: 9 givenname: G surname: POKOL fullname: POKOL, G organization: Budapest University of Technology and Economics, Institute of General and Analytical Chemistry, Szt. Gellért tér 4, 1521 Budapest, Hungary
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Keywords	Titanium IV Oxides Nanoparticle TiO2 nanopowders Doped materials Fabrication property relation X ray diffraction Surface structure Transmission electron microscopy Sol gel process Morphology Organic salt Surface properties Alkoxide Thermal analysis Surface area S-doped TiO2 sol-gel method
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Title	TiO2-based nanopowders obtained from different Ti-alkoxides
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