Microstructural and material property changes in severely deformed Eurofer-97

• Published in: Materials characterization Vol. 215; p. 114144
• Main Authors: Song, Kay, He, Guanze, Reza, Abdallah, Ungár, Tamas, Karamched, Phani, Yang, David, Tolkachev, Ivan, Mizohata, Kenichiro, Thompson, Stephen P., Connolly, Eamonn T., Atwood, Robert C., Michalik, Stefan, Armstrong, David E.J., Hofmann, Felix
• Format: Journal Article
• Language: English
• Published: United States Elsevier Inc 01-09-2024; Elsevier
• Subjects: Annealing; CONDENSED MATTER PHYSICS, SUPERCONDUCTIVITY AND SUPERFLUIDITY; Eurofer-97; High-pressure torsion; Ion-irradiation; Nanocrystalline microstructure; Nanocrystalline microstructure; Eurofer-97; Annealing; Ion-irradiation; High-pressure torsion
• ISSN: 1044-5803
• DOI: 10.1016/j.matchar.2024.114144

Severe plastic deformation changes the microstructure and properties of steels, which may be favourable for their use in structural components of nuclear reactors. In this study, high-pressure torsion (HPT) was used to refine the grain structure of Eurofer-97, a ferritic/martensitic steel. Electron microscopy and X-ray diffraction were used to characterise the microstructural changes. Following HPT at room temperature to a maximum shear strain of 230, the average grain size reduced by a factor of ∼30, with a marked increase in high-angle grain boundaries. Dislocation density also increased by more than one order of magnitude. The thermal stability of the deformed material was investigated via in-situ annealing during synchrotron X-ray diffraction. This revealed substantial recovery between 450 K – 800 K. Irradiation with 20 MeV Fe-ions to ∼0.1 dpa caused a 20% reduction in dislocation density compared to the as-deformed material. However, HPT deformation prior to irradiation only had a minor effect in mitigating the irradiation-induced reductions in thermal diffusivity and surface acoustic wave velocity of the material. Microstructural and material property changes are dominated by deformation compared to irradiation. In light of this, the benefits of using HPT to improve the irradiation resistance of Eurofer-97 are limited. These results provide a multi-faceted view of the changes in ferritic/martensitic steels due to severe plastic deformation, and how these changes can be used to alter material properties.
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•High-pressure torsion of Eurofer-97 produced sub-100 nm grains.•Microstructural changes saturated by a shear strain value of 110.•Recovery of the deformed material occurred between 450 and 800 K.•Irradiation caused a reduction in dislocation density of the deformed material.•Deformed materials exhibited less irradiation-induced changes than the reference.