Thermodynamics of dimer fullerene complex [(Me 3Si) 3C 60] 2 in the range from 0 ⩽ T/K ⩽ 480
In the present work, firstly the temperature dependence of heat capacity C p ,m ∘ = f ( T ) of the crystalline fullerene complex [(Me 3Si) 3C 60] 2 has been measured between T = (6 and 350) K and T = (330 and 480) K by precision adiabatic vacuum and dynamic calorimetry, respectively. The irreversibl...
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| Published in: | The Journal of chemical thermodynamics Vol. 39; no. 5; pp. 798 - 803 |
|---|---|
| Main Authors: | , , , , , , , , , |
| Format: | Journal Article |
| Language: | English |
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01-05-2007
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| Abstract | In the present work, firstly the temperature dependence of heat capacity
C
p
,m
∘
=
f
(
T
)
of the crystalline fullerene complex [(Me
3Si)
3C
60]
2 has been measured between
T
=
(6 and 350)
K and
T
=
(330 and 480)
K by precision adiabatic vacuum and dynamic calorimetry, respectively. The irreversible endothermic effect was detected in the temperature range from
T
=
(400 to 466)
K and its thermodynamic characteristics have been determined and analysed. This transformation was caused by the opening of a dimeric bond between fullerene fragments and the decomposition of the tested complex on heating. The experimental data were used for calculating the standard (
p
∘
=
0.1
MPa) thermodynamic functions
C
p
,m
∘
/
R
,
Δ
0
T
H
m
∘
/
RT
,
Δ
0
T
S
m
∘
/
R
and
Φ
m
∘
/
R
=
Δ
0
T
S
m
∘
/
R
-
Δ
0
T
H
m
∘
/
RT
(where
R is gas constant) in the range 0
⩽
T/K
⩽
400. The value of the standard entropy of formation of the complex from simple substances at
T
=
298.15
K has been estimated. |
|---|---|
| AbstractList | In the present work, firstly the temperature dependence of heat capacity
C
p
,m
∘
=
f
(
T
)
of the crystalline fullerene complex [(Me
3Si)
3C
60]
2 has been measured between
T
=
(6 and 350)
K and
T
=
(330 and 480)
K by precision adiabatic vacuum and dynamic calorimetry, respectively. The irreversible endothermic effect was detected in the temperature range from
T
=
(400 to 466)
K and its thermodynamic characteristics have been determined and analysed. This transformation was caused by the opening of a dimeric bond between fullerene fragments and the decomposition of the tested complex on heating. The experimental data were used for calculating the standard (
p
∘
=
0.1
MPa) thermodynamic functions
C
p
,m
∘
/
R
,
Δ
0
T
H
m
∘
/
RT
,
Δ
0
T
S
m
∘
/
R
and
Φ
m
∘
/
R
=
Δ
0
T
S
m
∘
/
R
-
Δ
0
T
H
m
∘
/
RT
(where
R is gas constant) in the range 0
⩽
T/K
⩽
400. The value of the standard entropy of formation of the complex from simple substances at
T
=
298.15
K has been estimated. |
| Author | Ob’edkov, A.M. Gorina, E.A. Smirnova, N.N. Bykova, T.A. Titova, S.N. Ketkov, S.Yu Ruchenin, V.A. Domrachev, G.A. Kalakutskaya, L.V. Markin, A.V. |
| Author_xml | – sequence: 1 givenname: A.V. surname: Markin fullname: Markin, A.V. email: markin@calorimetry-center.ru organization: Chemistry Institute, Nizhny Novgorod State University, Gagarin Pr. 23/5,603950, Nizhny Novgorod, Russian Federation – sequence: 2 givenname: N.N. surname: Smirnova fullname: Smirnova, N.N. organization: Chemistry Institute, Nizhny Novgorod State University, Gagarin Pr. 23/5,603950, Nizhny Novgorod, Russian Federation – sequence: 3 givenname: T.A. surname: Bykova fullname: Bykova, T.A. organization: Chemistry Institute, Nizhny Novgorod State University, Gagarin Pr. 23/5,603950, Nizhny Novgorod, Russian Federation – sequence: 4 givenname: V.A. surname: Ruchenin fullname: Ruchenin, V.A. organization: Chemistry Institute, Nizhny Novgorod State University, Gagarin Pr. 23/5,603950, Nizhny Novgorod, Russian Federation – sequence: 5 givenname: S.N. surname: Titova fullname: Titova, S.N. organization: Razuvaev Institute of Organometallic Chemistry of Russian Academy of Sciences, Tropinin Str. 49, 603950, Nizhny Novgorod, Russian Federation – sequence: 6 givenname: E.A. surname: Gorina fullname: Gorina, E.A. organization: Razuvaev Institute of Organometallic Chemistry of Russian Academy of Sciences, Tropinin Str. 49, 603950, Nizhny Novgorod, Russian Federation – sequence: 7 givenname: L.V. surname: Kalakutskaya fullname: Kalakutskaya, L.V. organization: Razuvaev Institute of Organometallic Chemistry of Russian Academy of Sciences, Tropinin Str. 49, 603950, Nizhny Novgorod, Russian Federation – sequence: 8 givenname: A.M. surname: Ob’edkov fullname: Ob’edkov, A.M. organization: Razuvaev Institute of Organometallic Chemistry of Russian Academy of Sciences, Tropinin Str. 49, 603950, Nizhny Novgorod, Russian Federation – sequence: 9 givenname: S.Yu surname: Ketkov fullname: Ketkov, S.Yu organization: Razuvaev Institute of Organometallic Chemistry of Russian Academy of Sciences, Tropinin Str. 49, 603950, Nizhny Novgorod, Russian Federation – sequence: 10 givenname: G.A. surname: Domrachev fullname: Domrachev, G.A. organization: Razuvaev Institute of Organometallic Chemistry of Russian Academy of Sciences, Tropinin Str. 49, 603950, Nizhny Novgorod, Russian Federation |
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| Cites_doi | 10.1103/PhysRevB.61.11936 10.1007/s11172-005-0072-3 10.1006/jcht.1996.0173 10.1107/S0108768102001970 10.1016/S0040-6031(99)00419-0 10.1021/ja0202614 10.1134/S1063783406050301 10.1103/PhysRevLett.66.2911 10.1126/science.259.5097.955 10.1016/0038-1098(92)90149-4 10.1016/S0040-6031(97)00066-X 10.1007/BF01430721 10.1016/j.tca.2004.03.011 10.1246/bcsj.39.2050 |
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| Keywords | Fullerene complex[(Me 3Si) 3C 60] 2 Heat capacity Standard thermodynamic functions Microcalorimetry Thermodynamic characteristics of transformation |
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| Snippet | In the present work, firstly the temperature dependence of heat capacity
C
p
,m
∘
=
f
(
T
)
of the crystalline fullerene complex [(Me
3Si)
3C
60]
2 has been... |
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| SubjectTerms | Fullerene complex[(Me 3Si) 3C 60] 2 Heat capacity Microcalorimetry Standard thermodynamic functions Thermodynamic characteristics of transformation |
| Title | Thermodynamics of dimer fullerene complex [(Me 3Si) 3C 60] 2 in the range from 0 ⩽ T/K ⩽ 480 |
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