Thermomechanical properties of multifunctional polymer hybrid nanocomposites based on carbon nanotubes and nanosilica

Nanocomposites containing low wt% of oxidized multi‐walled carbon nanotubes (MWCNT‐OXI), nanosilica (NS), and its hybrid (MWCNT‐OXI/NS) in epoxy resin were produced and evaluated. The used nanoparticles were studied by scanning electron microscopy (SEM), thermogravimetric analysis (TGA), and Raman s...

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Published in:	Journal of applied polymer science Vol. 141; no. 41
Main Authors:	Silva, Bruno Milton Oliveira, Fernandes, Nathália Maria Moraes, Barbosa, Juliano Martins, Pinto, Gabriel Matheus, Benega, Marcos Antônio Gimenes, Taha‐Tijerina, José Jaime, Andrade, Ricardo Jorge Espanhol, Ribeiro, Hélio
Format:	Journal Article
Language:	English
Published:	Hoboken, USA John Wiley & Sons, Inc 05-11-2024 Wiley Subscription Services, Inc
Subjects:	Addition polymerization carbon nanotubes Epoxy resins Glass transition temperature Mechanical properties Multi wall carbon nanotubes multifunctional nanocomposites Nanocomposites Nanoparticles nanosilica Plastic deformation Polymers Raman spectroscopy Storage modulus Thermal conductivity thermal properties Thermal resistance Thermal stability Thermodynamic properties Thermogravimetric analysis Thermomechanical properties
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Abstract	Nanocomposites containing low wt% of oxidized multi‐walled carbon nanotubes (MWCNT‐OXI), nanosilica (NS), and its hybrid (MWCNT‐OXI/NS) in epoxy resin were produced and evaluated. The used nanoparticles were studied by scanning electron microscopy (SEM), thermogravimetric analysis (TGA), and Raman spectroscopy while the nanocomposites were investigated in relation to its morphology, thermal, and mechanical properties. The results demonstrated significant improvements in the storage modulus (E′), glass transition temperature (Tg), and cross link density (CD), for the produced nanocomposites. Increases in thermal conductivity (TC) of up to 85% at 90°C were observed for the nanocomposites containing 1.0 wt% of the hybrid MWCNT‐OXI + NS nanofiller, when compared with neat polymer. It was also verified increases in the resistance to plastic deformation for the nanocomposites, maintained the polymer thermal stability with the addition of these nanoparticles. Finally, the use of MWCNT‐OXI and NS, combined or not, significantly improved the thermal and mechanical properties of polymer, showing multifunctional characteristics for the produced nanocomposites. Model for the epoxy system containing nanosilica, CNTs and its hybrids nanoparticles. MWCNT‐OXI, multi‐walled carbon nanotubes; NS, nanosilica.
AbstractList	Nanocomposites containing low wt% of oxidized multi‐walled carbon nanotubes (MWCNT‐OXI), nanosilica (NS), and its hybrid (MWCNT‐OXI/NS) in epoxy resin were produced and evaluated. The used nanoparticles were studied by scanning electron microscopy (SEM), thermogravimetric analysis (TGA), and Raman spectroscopy while the nanocomposites were investigated in relation to its morphology, thermal, and mechanical properties. The results demonstrated significant improvements in the storage modulus (E′), glass transition temperature (Tg), and cross link density (CD), for the produced nanocomposites. Increases in thermal conductivity (TC) of up to 85% at 90°C were observed for the nanocomposites containing 1.0 wt% of the hybrid MWCNT‐OXI + NS nanofiller, when compared with neat polymer. It was also verified increases in the resistance to plastic deformation for the nanocomposites, maintained the polymer thermal stability with the addition of these nanoparticles. Finally, the use of MWCNT‐OXI and NS, combined or not, significantly improved the thermal and mechanical properties of polymer, showing multifunctional characteristics for the produced nanocomposites. Nanocomposites containing low wt% of oxidized multi‐walled carbon nanotubes (MWCNT‐OXI), nanosilica (NS), and its hybrid (MWCNT‐OXI/NS) in epoxy resin were produced and evaluated. The used nanoparticles were studied by scanning electron microscopy (SEM), thermogravimetric analysis (TGA), and Raman spectroscopy while the nanocomposites were investigated in relation to its morphology, thermal, and mechanical properties. The results demonstrated significant improvements in the storage modulus ( E ′), glass transition temperature ( T g ), and cross link density (CD), for the produced nanocomposites. Increases in thermal conductivity (TC) of up to 85% at 90°C were observed for the nanocomposites containing 1.0 wt% of the hybrid MWCNT‐OXI + NS nanofiller, when compared with neat polymer. It was also verified increases in the resistance to plastic deformation for the nanocomposites, maintained the polymer thermal stability with the addition of these nanoparticles. Finally, the use of MWCNT‐OXI and NS, combined or not, significantly improved the thermal and mechanical properties of polymer, showing multifunctional characteristics for the produced nanocomposites. Nanocomposites containing low wt% of oxidized multi‐walled carbon nanotubes (MWCNT‐OXI), nanosilica (NS), and its hybrid (MWCNT‐OXI/NS) in epoxy resin were produced and evaluated. The used nanoparticles were studied by scanning electron microscopy (SEM), thermogravimetric analysis (TGA), and Raman spectroscopy while the nanocomposites were investigated in relation to its morphology, thermal, and mechanical properties. The results demonstrated significant improvements in the storage modulus (E′), glass transition temperature (Tg), and cross link density (CD), for the produced nanocomposites. Increases in thermal conductivity (TC) of up to 85% at 90°C were observed for the nanocomposites containing 1.0 wt% of the hybrid MWCNT‐OXI + NS nanofiller, when compared with neat polymer. It was also verified increases in the resistance to plastic deformation for the nanocomposites, maintained the polymer thermal stability with the addition of these nanoparticles. Finally, the use of MWCNT‐OXI and NS, combined or not, significantly improved the thermal and mechanical properties of polymer, showing multifunctional characteristics for the produced nanocomposites. Model for the epoxy system containing nanosilica, CNTs and its hybrids nanoparticles. MWCNT‐OXI, multi‐walled carbon nanotubes; NS, nanosilica.
Author	Benega, Marcos Antônio Gimenes Silva, Bruno Milton Oliveira Andrade, Ricardo Jorge Espanhol Taha‐Tijerina, José Jaime Fernandes, Nathália Maria Moraes Pinto, Gabriel Matheus Barbosa, Juliano Martins Ribeiro, Hélio
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Cites_doi	10.1016/j.polymertesting.2021.107180 10.1021/acsami.7b09945 10.3390/nano10061160 10.1016/j.surfin.2021.101389 10.1016/j.matpr.2019.02.047 10.1016/j.surfin.2023.103211 10.3390/polym8080281 10.1007/s10971-009-1958-6 10.21577/1984-6835.20180072 10.1016/j.polymertesting.2015.03.010 10.1088/1757-899X/1248/1/012084 10.3390/polym14193969 10.1016/j.prostr.2017.07.034 10.1002/app.46560 10.1016/j.carbon.2021.11.067 10.1016/0008-6223(95)00017-8 10.1016/j.carbon.2010.09.047 10.1016/j.susmat.2023.e00684 10.1002/pc.27328 10.1007/3-540-39947-X 10.1021/am3010576 10.1002/app.41216 10.1016/j.jnoncrysol.2012.11.006 10.3390/polym15061398 10.1016/j.polymertesting.2022.107645 10.1016/j.compositesa.2013.01.001 10.1016/j.polymdegradstab.2007.10.005 10.1155/2022/6040629 10.1021/acs.macromol.2c01719 10.1088/1757-899X/978/1/012031 10.1080/15583724.2019.1650063 10.1007/s12633-021-01527-0 10.1590/S0103-50532012000600012
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Snippet	Nanocomposites containing low wt% of oxidized multi‐walled carbon nanotubes (MWCNT‐OXI), nanosilica (NS), and its hybrid (MWCNT‐OXI/NS) in epoxy resin were...
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SubjectTerms	Addition polymerization carbon nanotubes Epoxy resins Glass transition temperature Mechanical properties Multi wall carbon nanotubes multifunctional nanocomposites Nanocomposites Nanoparticles nanosilica Plastic deformation Polymers Raman spectroscopy Storage modulus Thermal conductivity thermal properties Thermal resistance Thermal stability Thermodynamic properties Thermogravimetric analysis Thermomechanical properties
Title	Thermomechanical properties of multifunctional polymer hybrid nanocomposites based on carbon nanotubes and nanosilica
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