Enhanced catalytic transfer hydrogenation of biomass-based furfural into furfuryl alcohol over Co3O4-based mixed oxide catalysts from hydrotalcite
Catalytic furfural (FF) into high value-added furfuryl alcohol (FOL) is a very important biomass improvement process and remains a challenging task. Herein, a series of Co-based composite oxide (CoMgAl-LDO) catalysts with highly dispersed Co3O4-based spinel oxide nanoparticles were synthesized by th...
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| Published in: | Applied catalysis. A, General Vol. 684; p. 119909 |
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| Main Authors: | , , , , , , |
| Format: | Journal Article |
| Language: | English |
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Elsevier B.V
25-08-2024
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| Abstract | Catalytic furfural (FF) into high value-added furfuryl alcohol (FOL) is a very important biomass improvement process and remains a challenging task. Herein, a series of Co-based composite oxide (CoMgAl-LDO) catalysts with highly dispersed Co3O4-based spinel oxide nanoparticles were synthesized by the topological transformation of Co-based ternary layered hydroxides (CoMgAl-LDH) under calcination conditions and tested for catalytic transfer hydrogenation of FF to FOL using isopropanol (2-PrOH) as hydrogen donor. The CoMgAl-LDO, especially Co1.5Mg1.5Al1-LDO calcinated at 500 °C (Co1.5Mg1.5Al1-LDO-500) offered the outstanding catalytic performance for the catalytic transfer hydrogenation of FF to FOL (99.7 % FF conversion and 95.9 % FOL selectivity), which was attributed to effectively dispersed active sites, abundant acid-base sites and mesoporous structure. Additionally, the Co1.5Mg1.5Al1-LDO-500 catalyst manifested good stability with wider universality to other carbonyl compounds, making the catalytic system extremely economical and practical in various biomass hydrogenation processes.
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•Co3O4-based mixed oxide (CoMgAl-LDO) catalysts were synthesized by the calcination of Co-based hydrotalcites (CoMgAl-LDH).•Co1.5Mg1.5Al1-LDO-500 (500 ℃) exhibited excellent performance in the hydrogenation of furfural to furfuryl alcohol.•The dispersion of active Co3O4, abundant acid-base sites and mesoporous structure enhanced the performance of the catalyst. |
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| AbstractList | Catalytic furfural (FF) into high value-added furfuryl alcohol (FOL) is a very important biomass improvement process and remains a challenging task. Herein, a series of Co-based composite oxide (CoMgAl-LDO) catalysts with highly dispersed Co3O4-based spinel oxide nanoparticles were synthesized by the topological transformation of Co-based ternary layered hydroxides (CoMgAl-LDH) under calcination conditions and tested for catalytic transfer hydrogenation of FF to FOL using isopropanol (2-PrOH) as hydrogen donor. The CoMgAl-LDO, especially Co1.5Mg1.5Al1-LDO calcinated at 500 °C (Co1.5Mg1.5Al1-LDO-500) offered the outstanding catalytic performance for the catalytic transfer hydrogenation of FF to FOL (99.7 % FF conversion and 95.9 % FOL selectivity), which was attributed to effectively dispersed active sites, abundant acid-base sites and mesoporous structure. Additionally, the Co1.5Mg1.5Al1-LDO-500 catalyst manifested good stability with wider universality to other carbonyl compounds, making the catalytic system extremely economical and practical in various biomass hydrogenation processes.
[Display omitted]
•Co3O4-based mixed oxide (CoMgAl-LDO) catalysts were synthesized by the calcination of Co-based hydrotalcites (CoMgAl-LDH).•Co1.5Mg1.5Al1-LDO-500 (500 ℃) exhibited excellent performance in the hydrogenation of furfural to furfuryl alcohol.•The dispersion of active Co3O4, abundant acid-base sites and mesoporous structure enhanced the performance of the catalyst. |
| ArticleNumber | 119909 |
| Author | Cheng, Shifang Xu, Jing Ding, Junfang Feng, Xinya Pan, Ganen Chen, Yakai Xu, Xingliang |
| Author_xml | – sequence: 1 givenname: Shifang surname: Cheng fullname: Cheng, Shifang organization: College of Chemistry and Material Science, Shandong Agricultural University, Taian, Shandong, China – sequence: 2 givenname: Junfang surname: Ding fullname: Ding, Junfang organization: College of Chemistry and Chemical Engineering, Inner Mongolia University, Hohhot, China – sequence: 3 givenname: Yakai surname: Chen fullname: Chen, Yakai organization: College of Chemistry and Material Science, Shandong Agricultural University, Taian, Shandong, China – sequence: 4 givenname: Ganen surname: Pan fullname: Pan, Ganen organization: College of Chemistry and Material Science, Shandong Agricultural University, Taian, Shandong, China – sequence: 5 givenname: Xinya surname: Feng fullname: Feng, Xinya organization: College of Chemistry and Material Science, Shandong Agricultural University, Taian, Shandong, China – sequence: 6 givenname: Xingliang surname: Xu fullname: Xu, Xingliang email: xxlsdau@163.com organization: College of Chemistry and Material Science, Shandong Agricultural University, Taian, Shandong, China – sequence: 7 givenname: Jing surname: Xu fullname: Xu, Jing email: jiaxu@sdau.edu.cn organization: College of Chemistry and Material Science, Shandong Agricultural University, Taian, Shandong, China |
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| Keywords | Transfer hydrogenation Hydrotalcite Furfural Furfuryl alcohol Co3O4 |
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| Title | Enhanced catalytic transfer hydrogenation of biomass-based furfural into furfuryl alcohol over Co3O4-based mixed oxide catalysts from hydrotalcite |
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