Growth Mode Transition Involving a Potential-Dependent Isotropic to Anisotropic Surface Atom Diffusion Change. Gold Electrodeposition on HOPG followed by STM
The electrodeposition of gold on highly oriented pyrolytic graphite (HOPG) from acid aqueous solutions was studied by using electrochemical techniques complemented with ex-situ scanning tunneling microscopy (STM). The kinetics of gold electrodeposition is consistent with a nucleation and three-dimen...
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| Published in: | Langmuir Vol. 13; no. 1; pp. 100 - 110 |
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| Main Authors: | , , , , , |
| Format: | Journal Article |
| Language: | English |
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American Chemical Society
08-01-1997
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| Abstract | The electrodeposition of gold on highly oriented pyrolytic graphite (HOPG) from acid aqueous solutions was studied by using electrochemical techniques complemented with ex-situ scanning tunneling microscopy (STM). The kinetics of gold electrodeposition is consistent with a nucleation and three-dimensional growth process under diffusion control from the solution side. As the applied potential moves in the negative direction, the gold crystal density increases, and the crystal shape changes from a Euclidean to a dendritic fractal morphology. This transition can be assigned to the anisotropic surface diffusion of gold adatoms induced by the applied electric potential. A model including a potential-dependent energy barrier at step edges accounts for the morphology transition for gold electrodeposition on HOPG. |
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| AbstractList | The electrodeposition of gold on highly oriented pyrolytic graphite (HOPG) from acid aqueous solutions was studied by using electrochemical techniques complemented with ex-situ scanning tunneling microscopy (STM). The kinetics of gold electrodeposition is consistent with a nucleation and three-dimensional growth process under diffusion control from the solution side. As the applied potential moves in the negative direction, the gold crystal density increases, and the crystal shape changes from a Euclidean to a dendritic fractal morphology. This transition can be assigned to the anisotropic surface diffusion of gold adatoms induced by the applied electric potential. A model including a potential-dependent energy barrier at step edges accounts for the morphology transition for gold electrodeposition on HOPG. |
| Author | Hernández Creus, A González, S Martín, H Salvarezza, R. C Carro, P Arvia, A. J |
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| Cites_doi | 10.1103/PhysRevLett.73.1517 10.1016/0022-0728(94)03538-5 10.1016/0039-6028(94)90685-8 10.1021/j100180a064 10.1103/PhysRevLett.71.113 10.1016/0039-6028(94)00844-2 10.1007/978-1-4613-3584-9_7 10.1103/PhysRevLett.72.4025 10.1017/CBO9780511599798 10.1021/ja00028a009 10.1016/0013-4686(92)85114-Z 10.1098/rspa.1949.0095 10.1039/f19837900467 10.1103/PhysRevLett.75.2980 10.1515/zpch-1926-11927 10.1016/0039-6028(96)80063-X 10.1103/PhysRevB.52.2032 10.1149/1.2069340 10.1063/1.1657442 10.1103/PhysRevLett.67.3279 10.1016/0022-0728(95)04479-5 10.1021/j100204a062 10.1103/PhysRevB.52.14263 10.1016/0022-0728(95)04376-4 10.1103/PhysRevLett.68.3741 10.1016/0039-6028(95)01347-4 10.1007/978-3-642-97343-7_6 10.1103/PhysRevLett.74.2295 10.1016/0022-0728(93)80091-U 10.1103/PhysRevLett.62.929 |
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| Keywords | Gold Electric potential Surface diffusion Experimental study STM Acidic solution Crystal growth habit Aqueous solutions Transition elements Growth mechanism Adatoms Crystal growth from solutions Electrodeposition Crystal nucleation Dendrites Kinetics Aggregate |
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| Snippet | The electrodeposition of gold on highly oriented pyrolytic graphite (HOPG) from acid aqueous solutions was studied by using electrochemical techniques... |
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| SubjectTerms | Applied sciences Cross-disciplinary physics: materials science; rheology Electrodeposition, electroplating Exact sciences and technology Materials science Metals. Metallurgy Methods of deposition of films and coatings; film growth and epitaxy Physics |
| Title | Growth Mode Transition Involving a Potential-Dependent Isotropic to Anisotropic Surface Atom Diffusion Change. Gold Electrodeposition on HOPG followed by STM |
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