Binding and Activation of Small Molecules by Three-Coordinate Cr(I)
[(i-Pr2Ph)2nacnacCr]2(μ-η2:η2-N2) (2) has been prepared and structurally characterized; it contains a bridging side-on bonded dinitrogen ligand with a N−N distance of 1.249(5) Å. Reactions of this reactive Cr(I) synthon with various small molecules resulted in a series of unusual molecules and trans...
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| Published in: | Journal of the American Chemical Society Vol. 129; no. 26; pp. 8090 - 8091 |
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| Main Authors: | , , , |
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04-07-2007
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| Abstract | [(i-Pr2Ph)2nacnacCr]2(μ-η2:η2-N2) (2) has been prepared and structurally characterized; it contains a bridging side-on bonded dinitrogen ligand with a N−N distance of 1.249(5) Å. Reactions of this reactive Cr(I) synthon with various small molecules resulted in a series of unusual molecules and transformations; thus CO yielded the binuclear isocarbonyl [(i-Pr2Ph)2nacnacCr]2(CO)(μ-η:η1-CO)2, ethylene gave [(i-Pr2Ph)2nacnacCr]2(μ-η:η2-C2H4), O2 oxidatively added to produce (i-Pr2Ph)2nacnacCr(O)2, and azobenzene afforded the product of NN bond cleavage [(i-Pr2Ph)2nacnacCr]2(μ-NPh)2. 2 can be prepared in good yield and affords a facile entry to low-coordinate Cr(I) coordination chemistry. |
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| AbstractList | [(i-Pr2Ph)2nacnacCr]2(μ-η2:η2-N2) (2) has been prepared and structurally characterized; it contains a bridging side-on bonded dinitrogen ligand with a N−N distance of 1.249(5) Å. Reactions of this reactive Cr(I) synthon with various small molecules resulted in a series of unusual molecules and transformations; thus CO yielded the binuclear isocarbonyl [(i-Pr2Ph)2nacnacCr]2(CO)(μ-η:η1-CO)2, ethylene gave [(i-Pr2Ph)2nacnacCr]2(μ-η:η2-C2H4), O2 oxidatively added to produce (i-Pr2Ph)2nacnacCr(O)2, and azobenzene afforded the product of NN bond cleavage [(i-Pr2Ph)2nacnacCr]2(μ-NPh)2. 2 can be prepared in good yield and affords a facile entry to low-coordinate Cr(I) coordination chemistry. |
| Author | Monillas, Wesley H Theopold, Klaus H Yap, Glenn P. A MacAdams, Leonard A |
| Author_xml | – sequence: 1 givenname: Wesley H surname: Monillas fullname: Monillas, Wesley H – sequence: 2 givenname: Glenn P. A surname: Yap fullname: Yap, Glenn P. A – sequence: 3 givenname: Leonard A surname: MacAdams fullname: MacAdams, Leonard A – sequence: 4 givenname: Klaus H surname: Theopold fullname: Theopold, Klaus H |
| BackLink | https://www.ncbi.nlm.nih.gov/pubmed/17567016$$D View this record in MEDLINE/PubMed |
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| Snippet | [(i-Pr2Ph)2nacnacCr]2(μ-η2:η2-N2) (2) has been prepared and structurally characterized; it contains a bridging side-on bonded dinitrogen ligand with a N−N... |
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| Title | Binding and Activation of Small Molecules by Three-Coordinate Cr(I) |
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