Micellar Solutions of Associative Triblock Copolymers: The Relationship between Structure and Rheology
We report the rheology of the micellar solutions formed from narrow-molecular-weight poly(ethylene oxide) chains fully endcapped with C16 or C18 alkanes and correlate the viscoelasticity, characterized by the high-frequency modulus G ∞‘ and a single relaxation time λ, with the measured characteristi...
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| Published in: | Macromolecules Vol. 32; no. 15; pp. 5139 - 5146 |
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27-07-1999
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| Abstract | We report the rheology of the micellar solutions formed from narrow-molecular-weight poly(ethylene oxide) chains fully endcapped with C16 or C18 alkanes and correlate the viscoelasticity, characterized by the high-frequency modulus G ∞‘ and a single relaxation time λ, with the measured characteristics of the micellar solutions. Scaling G ∞‘ by p 3/2 kT/τ R H 3 (p = aggregation number, R H = hydrodynamic radius, 1/τ = attractive virial coefficient, k = Boltzmann's constant, and T = temperature) and plotting against the hydrodynamic volume fraction of micelles collapses the two sets of data. The relaxation time scales as the diffusion time, μ R c 3/kT, for a free hydrophobe escaping from a micellar core of radius R c times a Boltzmann factor accounting for an association energy that increases linearly with hydrophobe length. The low shear viscosity follows as η o = λ G ∞‘. |
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| AbstractList | We report the rheology of the micellar solutions formed from narrow-molecular-weight poly(ethylene oxide) chains fully endcapped with C16 or C18 alkanes and correlate the viscoelasticity, characterized by the high-frequency modulus G ∞‘ and a single relaxation time λ, with the measured characteristics of the micellar solutions. Scaling G ∞‘ by p 3/2 kT/τ R H 3 (p = aggregation number, R H = hydrodynamic radius, 1/τ = attractive virial coefficient, k = Boltzmann's constant, and T = temperature) and plotting against the hydrodynamic volume fraction of micelles collapses the two sets of data. The relaxation time scales as the diffusion time, μ R c 3/kT, for a free hydrophobe escaping from a micellar core of radius R c times a Boltzmann factor accounting for an association energy that increases linearly with hydrophobe length. The low shear viscosity follows as η o = λ G ∞‘. |
| Author | Thibeault, J. C Pham, Q. T Lau, W Russel, W. B |
| Author_xml | – sequence: 1 givenname: Q. T surname: Pham fullname: Pham, Q. T – sequence: 2 givenname: W. B surname: Russel fullname: Russel, W. B – sequence: 3 givenname: J. C surname: Thibeault fullname: Thibeault, J. C – sequence: 4 givenname: W surname: Lau fullname: Lau, W |
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| Cites_doi | 10.1016/0927-7757(96)03514-5 10.1007/978-1-4684-3635-8_11 10.1063/1.1724109 10.1122/1.550530 10.1016/0377-0257(92)80027-U 10.1021/j100133a033 10.1122/1.550391 10.1016/S0377-0257(97)00084-0 10.1021/ma00108a025 10.1021/ma00071a026 10.1122/1.550940 |
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| Keywords | Ethylene oxide polymer Monodispersed polymer Shear viscosity End group Shear modulus Solution structure Concentration effect Hydrophobic group Property structure relationship Aqueous solution Experimental study Micellar solution |
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| SubjectTerms | Applied sciences Exact sciences and technology Organic polymers Physicochemistry of polymers Properties and characterization Solution and gel properties |
| Title | Micellar Solutions of Associative Triblock Copolymers: The Relationship between Structure and Rheology |
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