“Silver Effect” in Gold(I) Catalysis: An Overlooked Important Factor
Clear experimental evidence from X-ray photoelectron spectroscopy and 31P NMR spectroscopy has been obtained for the first time to confirm that the combination of Ag+ cation with [L-Au]+ results in the formation of different complexes in solution. Re-evaluation of literature-reported gold-catalyzed...
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| Published in: | Journal of the American Chemical Society Vol. 134; no. 21; pp. 9012 - 9019 |
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| Main Authors: | , , , , , , , , , |
| Format: | Journal Article |
| Language: | English |
| Published: |
United States
American Chemical Society
30-05-2012
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| Online Access: | Get full text |
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| Abstract | Clear experimental evidence from X-ray photoelectron spectroscopy and 31P NMR spectroscopy has been obtained for the first time to confirm that the combination of Ag+ cation with [L-Au]+ results in the formation of different complexes in solution. Re-evaluation of literature-reported gold-catalyzed reactions revealed a significant difference in the reactivities with and without silver. In extreme cases (more than “rare”), the conventional [L-Au]+ catalysts could not promote the reaction without the presence of silver. This investigation has therefore revealed a long-overlooked “silver effect” in gold catalysis and should lead to revision of the actual mechanism. |
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| AbstractList | Clear experimental evidence from X-ray photoelectron spectroscopy and (31)P NMR spectroscopy has been obtained for the first time to confirm that the combination of Ag(+) cation with [L-Au](+) results in the formation of different complexes in solution. Re-evaluation of literature-reported gold-catalyzed reactions revealed a significant difference in the reactivities with and without silver. In extreme cases (more than "rare"), the conventional [L-Au](+) catalysts could not promote the reaction without the presence of silver. This investigation has therefore revealed a long-overlooked "silver effect" in gold catalysis and should lead to revision of the actual mechanism. Clear experimental evidence from X-ray photoelectron spectroscopy and 31P NMR spectroscopy has been obtained for the first time to confirm that the combination of Ag+ cation with [L-Au]+ results in the formation of different complexes in solution. Re-evaluation of literature-reported gold-catalyzed reactions revealed a significant difference in the reactivities with and without silver. In extreme cases (more than “rare”), the conventional [L-Au]+ catalysts could not promote the reaction without the presence of silver. This investigation has therefore revealed a long-overlooked “silver effect” in gold catalysis and should lead to revision of the actual mechanism. |
| Author | Wang, Dawei Zhang, Hui Shi, Xiaodong Sharma, Sripadh Jirak, James Liu, Xingbo Petersen, Jeffrey L Akhmedov, Novruz G Cai, Rong Thummanapelli, Sravan K |
| AuthorAffiliation | West Virginia University |
| AuthorAffiliation_xml | – name: West Virginia University |
| Author_xml | – sequence: 1 givenname: Dawei surname: Wang fullname: Wang, Dawei – sequence: 2 givenname: Rong surname: Cai fullname: Cai, Rong – sequence: 3 givenname: Sripadh surname: Sharma fullname: Sharma, Sripadh – sequence: 4 givenname: James surname: Jirak fullname: Jirak, James – sequence: 5 givenname: Sravan K surname: Thummanapelli fullname: Thummanapelli, Sravan K – sequence: 6 givenname: Novruz G surname: Akhmedov fullname: Akhmedov, Novruz G – sequence: 7 givenname: Hui surname: Zhang fullname: Zhang, Hui – sequence: 8 givenname: Xingbo surname: Liu fullname: Liu, Xingbo – sequence: 9 givenname: Jeffrey L surname: Petersen fullname: Petersen, Jeffrey L – sequence: 10 givenname: Xiaodong surname: Shi fullname: Shi, Xiaodong email: Xiaodong.Shi@mail.wvu.edu |
| BackLink | https://www.ncbi.nlm.nih.gov/pubmed/22563621$$D View this record in MEDLINE/PubMed |
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| Snippet | Clear experimental evidence from X-ray photoelectron spectroscopy and 31P NMR spectroscopy has been obtained for the first time to confirm that the combination... Clear experimental evidence from X-ray photoelectron spectroscopy and (31)P NMR spectroscopy has been obtained for the first time to confirm that the... |
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| Title | “Silver Effect” in Gold(I) Catalysis: An Overlooked Important Factor |
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