Garnet-Type Fast Li-Ion Conductors with High Ionic Conductivities for All-Solid-State Batteries
All-solid-state Li-ion batteries with metallic Li anodes and solid electrolytes could offer superior energy density and safety over conventional Li-ion batteries. However, compared with organic liquid electrolytes, the low conductivity of solid electrolytes and large electrolyte/electrode interfacia...
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| Published in: | ACS applied materials & interfaces Vol. 9; no. 14; pp. 12461 - 12468 |
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| Main Authors: | , , , , |
| Format: | Journal Article |
| Language: | English |
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American Chemical Society
12-04-2017
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| Abstract | All-solid-state Li-ion batteries with metallic Li anodes and solid electrolytes could offer superior energy density and safety over conventional Li-ion batteries. However, compared with organic liquid electrolytes, the low conductivity of solid electrolytes and large electrolyte/electrode interfacial resistance impede their practical application. Garnet-type Li-ion conducting oxides are among the most promising electrolytes for all-solid-state Li-ion batteries. In this work, the large-radius Rb is doped at the La site of cubic Li6.10Ga0.30La3Zr2O12 to enhance the Li-ion conductivity for the first time. The Li6.20Ga0.30La2.95Rb0.05Zr2O12 electrolyte exhibits a Li-ion conductivity of 1.62 mS cm–1 at room temperature, which is the highest conductivity reported until now. All-solid-state Li-ion batteries are constructed from the electrolyte, metallic Li anode, and LiFePO4 active cathode. The addition of Li(CF3SO2)2N electrolytic salt in the cathode effectively reduces the interfacial resistance, allowing for a high initial discharge capacity of 152 mAh g–1 and good cycling stability with 110 mAh g–1 retained after 20 cycles at a charge/discharge rate of 0.05 C at 60 °C. |
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| AbstractList | All-solid-state Li-ion batteries with metallic Li anodes and solid electrolytes could offer superior energy density and safety over conventional Li-ion batteries. However, compared with organic liquid electrolytes, the low conductivity of solid electrolytes and large electrolyte/electrode interfacial resistance impede their practical application. Garnet-type Li-ion conducting oxides are among the most promising electrolytes for all-solid-state Li-ion batteries. In this work, the large-radius Rb is doped at the La site of cubic Li
Ga
La
Zr
O
to enhance the Li-ion conductivity for the first time. The Li
Ga
La
Rb
Zr
O
electrolyte exhibits a Li-ion conductivity of 1.62 mS cm
at room temperature, which is the highest conductivity reported until now. All-solid-state Li-ion batteries are constructed from the electrolyte, metallic Li anode, and LiFePO
active cathode. The addition of Li(CF
SO
)
N electrolytic salt in the cathode effectively reduces the interfacial resistance, allowing for a high initial discharge capacity of 152 mAh g
and good cycling stability with 110 mAh g
retained after 20 cycles at a charge/discharge rate of 0.05 C at 60 °C. All-solid-state Li-ion batteries with metallic Li anodes and solid electrolytes could offer superior energy density and safety over conventional Li-ion batteries. However, compared with organic liquid electrolytes, the low conductivity of solid electrolytes and large electrolyte/electrode interfacial resistance impede their practical application. Garnet-type Li-ion conducting oxides are among the most promising electrolytes for all-solid-state Li-ion batteries. In this work, the large-radius Rb is doped at the La site of cubic Li6.10Ga0.30La3Zr2O12 to enhance the Li-ion conductivity for the first time. The Li6.20Ga0.30La2.95Rb0.05Zr2O12 electrolyte exhibits a Li-ion conductivity of 1.62 mS cm-1 at room temperature, which is the highest conductivity reported until now. All-solid-state Li-ion batteries are constructed from the electrolyte, metallic Li anode, and LiFePO4 active cathode. The addition of Li(CF3SO2)2N electrolytic salt in the cathode effectively reduces the interfacial resistance, allowing for a high initial discharge capacity of 152 mAh g-1 and good cycling stability with 110 mAh g-1 retained after 20 cycles at a charge/discharge rate of 0.05 C at 60 °C. All-solid-state Li-ion batteries with metallic Li anodes and solid electrolytes could offer superior energy density and safety over conventional Li-ion batteries. However, compared with organic liquid electrolytes, the low conductivity of solid electrolytes and large electrolyte/electrode interfacial resistance impede their practical application. Garnet-type Li-ion conducting oxides are among the most promising electrolytes for all-solid-state Li-ion batteries. In this work, the large-radius Rb is doped at the La site of cubic Li6.10Ga0.30La3Zr2O12 to enhance the Li-ion conductivity for the first time. The Li6.20Ga0.30La2.95Rb0.05Zr2O12 electrolyte exhibits a Li-ion conductivity of 1.62 mS cm–1 at room temperature, which is the highest conductivity reported until now. All-solid-state Li-ion batteries are constructed from the electrolyte, metallic Li anode, and LiFePO4 active cathode. The addition of Li(CF3SO2)2N electrolytic salt in the cathode effectively reduces the interfacial resistance, allowing for a high initial discharge capacity of 152 mAh g–1 and good cycling stability with 110 mAh g–1 retained after 20 cycles at a charge/discharge rate of 0.05 C at 60 °C. |
| Author | Pang, Wei Kong Guo, Xin Peterson, Vanessa K Wei, Lu Wu, Jian-Fang |
| AuthorAffiliation | Australian Centre for Neutron Scattering Australian Nuclear Science and Technology Organisation Laboratory of Solid State Ionics, School of Materials Science and Engineering University of Wollongong Institute for Superconducting & Electronic Materials, Faculty of Engineering |
| AuthorAffiliation_xml | – name: Institute for Superconducting & Electronic Materials, Faculty of Engineering – name: University of Wollongong – name: Laboratory of Solid State Ionics, School of Materials Science and Engineering – name: Australian Nuclear Science and Technology Organisation – name: Australian Centre for Neutron Scattering |
| Author_xml | – sequence: 1 givenname: Jian-Fang surname: Wu fullname: Wu, Jian-Fang organization: Laboratory of Solid State Ionics, School of Materials Science and Engineering – sequence: 2 givenname: Wei Kong orcidid: 0000-0002-5118-3885 surname: Pang fullname: Pang, Wei Kong organization: University of Wollongong – sequence: 3 givenname: Vanessa K surname: Peterson fullname: Peterson, Vanessa K organization: University of Wollongong – sequence: 4 givenname: Lu surname: Wei fullname: Wei, Lu email: lwei@hust.edu.cn organization: Laboratory of Solid State Ionics, School of Materials Science and Engineering – sequence: 5 givenname: Xin orcidid: 0000-0003-1546-8119 surname: Guo fullname: Guo, Xin email: xguo@hust.edu.cn organization: Laboratory of Solid State Ionics, School of Materials Science and Engineering |
| BackLink | https://www.ncbi.nlm.nih.gov/pubmed/28332828$$D View this record in MEDLINE/PubMed |
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| Snippet | All-solid-state Li-ion batteries with metallic Li anodes and solid electrolytes could offer superior energy density and safety over conventional Li-ion... |
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| Title | Garnet-Type Fast Li-Ion Conductors with High Ionic Conductivities for All-Solid-State Batteries |
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