Synthesis of a Diblock Copolymer with Pendent Luminescent and Charge Transport Units through Nitroxide-Mediated Free Radical Polymerization
We present the efficient polymerization of a vinyl monomer bearing electron-transporting units, 2-[4-(4‘-vinylbiphenylyl)]-5-(4-tert-butylphenyl)-1,3,4-oxadiazole (vPBD), by using a TEMPO (2,2,6,6-tetramethylpiperidine-1-oxyl)-mediated radical polymerization method. A kinetic study using this monome...
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| Published in: | Macromolecules Vol. 35; no. 5; pp. 1543 - 1548 |
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| Language: | English |
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26-02-2002
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| Abstract | We present the efficient polymerization of a vinyl monomer bearing electron-transporting units, 2-[4-(4‘-vinylbiphenylyl)]-5-(4-tert-butylphenyl)-1,3,4-oxadiazole (vPBD), by using a TEMPO (2,2,6,6-tetramethylpiperidine-1-oxyl)-mediated radical polymerization method. A kinetic study using this monomer showed a quasi-living free radical character. The corresponding homopolymer was obtained in high yield with a very narrow polydispersity. Further reaction of the isolated polymer with another vinyl monomer bearing luminescent groups, 4-tert-butyl-4‘-(4-vinylstyryl)-trans-stilbene (v3PV), gave a diblock copolymer containing both functional groups. |
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| AbstractList | We present the efficient polymerization of a vinyl monomer bearing electron-transporting units, 2-[4-(4‘-vinylbiphenylyl)]-5-(4-tert-butylphenyl)-1,3,4-oxadiazole (vPBD), by using a TEMPO (2,2,6,6-tetramethylpiperidine-1-oxyl)-mediated radical polymerization method. A kinetic study using this monomer showed a quasi-living free radical character. The corresponding homopolymer was obtained in high yield with a very narrow polydispersity. Further reaction of the isolated polymer with another vinyl monomer bearing luminescent groups, 4-tert-butyl-4‘-(4-vinylstyryl)-trans-stilbene (v3PV), gave a diblock copolymer containing both functional groups. |
| Author | Hilberer, Alain Hadziioannou, Georges de Boer, Bert Boiteau, Laurent Moroni, Marc Werts, Michel |
| Author_xml | – sequence: 1 givenname: Laurent surname: Boiteau fullname: Boiteau, Laurent – sequence: 2 givenname: Marc surname: Moroni fullname: Moroni, Marc – sequence: 3 givenname: Alain surname: Hilberer fullname: Hilberer, Alain – sequence: 4 givenname: Michel surname: Werts fullname: Werts, Michel – sequence: 5 givenname: Bert surname: de Boer fullname: de Boer, Bert – sequence: 6 givenname: Georges surname: Hadziioannou fullname: Hadziioannou, Georges |
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| Cites_doi | 10.1021/ma00102a039 10.1016/0379-6779(95)03402-6 10.1021/ma961131g 10.1002/marc.1996.030170908 10.1002/(SICI)1521-4095(199808)10:12<901::AID-ADMA901>3.0.CO;2-B 10.1021/ja00103a055 10.1021/cm990535v 10.1002/(SICI)1521-4095(199806)10:9<680::AID-ADMA680>3.0.CO;2-H 10.1002/1521-3773(20010119)40:2<428::AID-ANIE428>3.0.CO;2-N 10.1021/ma00128a069 10.1021/ma00063a054 10.1016/0014-3057(89)90040-2 10.1021/ja984013c 10.1021/ma9910944 10.1016/S0032-3861(01)00388-3 10.1002/(SICI)1521-3773(19980302)37:4<402::AID-ANIE402>3.0.CO;2-9 10.1002/marc.1996.030171004 |
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| Keywords | Chemical solution Nitroxyl Living polymer Luminescent material Styrene derivative copolymer Experimental study Lateral group Absorption spectrum Styrene derivative polymer Monodispersed polymer Free radical polymerization Preparation Piperidine derivatives Diblock copolymer Oxadiazole derivatives Luminescence spectrum |
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| SubjectTerms | Applied sciences Exact sciences and technology Organic polymers Physicochemistry of polymers Polymers with particular properties Preparation, kinetics, thermodynamics, mechanism and catalysts |
| Title | Synthesis of a Diblock Copolymer with Pendent Luminescent and Charge Transport Units through Nitroxide-Mediated Free Radical Polymerization |
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