Atom Transfer Radical Polymerization of End-Functionalized Hydrogen-Bonding Polymers and Resulting Polymer Miscibility

The synthesis of end-functionalized hydrogen-bonding polymers and the investigation of their melt phase blend behavior are reported. Monofunctional and telechelic ureidopyrimidinone (UPy)-functionalized poly(styrene)s and poly(methyl methacrylate)s were synthesized using atom transfer radical polyme...

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Published in:Macromolecules Vol. 42; no. 23; pp. 9255 - 9262
Main Authors: Wrue, Michelle H, McUmber, Aaron C, Anthamatten, Mitchell
Format: Journal Article
Language:English
Published: Washington, DC American Chemical Society 08-12-2009
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Abstract The synthesis of end-functionalized hydrogen-bonding polymers and the investigation of their melt phase blend behavior are reported. Monofunctional and telechelic ureidopyrimidinone (UPy)-functionalized poly(styrene)s and poly(methyl methacrylate)s were synthesized using atom transfer radical polymerization (ATRP) followed by atom transfer radical coupling (ATRC). Aggregation of UPy end-groups in solution was observed using size exclusion chromatography. The effect of UPy end-groups on blend miscibility in the melt state was studied using optical microscopy and differential scanning calorimetry. The incorporation of associating groups onto one end of either blend component decreases miscibility relative to unfunctionalized parent blends. Lower miscibility was also observed for blends in which both components were monofunctionalized with associating end-groups. The largest decrease in miscibility was observed for blends containing telechelic UPy-functionalized polymers, which were immiscible across the entire composition range.
AbstractList The synthesis of end-functionalized hydrogen-bonding polymers and the investigation of their melt phase blend behavior are reported. Monofunctional and telechelic ureidopyrimidinone (UPy)-functionalized poly(styrene)s and poly(methyl methacrylate)s were synthesized using atom transfer radical polymerization (ATRP) followed by atom transfer radical coupling (ATRC). Aggregation of UPy end-groups in solution was observed using size exclusion chromatography. The effect of UPy end-groups on blend miscibility in the melt state was studied using optical microscopy and differential scanning calorimetry. The incorporation of associating groups onto one end of either blend component decreases miscibility relative to unfunctionalized parent blends. Lower miscibility was also observed for blends in which both components were monofunctionalized with associating end-groups. The largest decrease in miscibility was observed for blends containing telechelic UPy-functionalized polymers, which were immiscible across the entire composition range.
Author Wrue, Michelle H
Anthamatten, Mitchell
McUmber, Aaron C
Author_xml – sequence: 1
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  givenname: Mitchell
  surname: Anthamatten
  fullname: Anthamatten, Mitchell
  email: anthamatten@che.rochester.edu
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Issue 23
Keywords Chemical solution
Polymer blends
Phase diagram
Telechelic polymer
Atom transfer polymerization
Methyl methacrylate polymer
Experimental study
Free radical reaction
Chemical coupling
Preparation
Miscibility
Pyrimidine derivatives
Styrene polymer
Ureas
Molecular aggregation
Thermodynamic properties
Hydrogen bond
Language English
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Snippet The synthesis of end-functionalized hydrogen-bonding polymers and the investigation of their melt phase blend behavior are reported. Monofunctional and...
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SubjectTerms Applied sciences
Exact sciences and technology
Organic polymers
Physicochemistry of polymers
Polymers with particular structures
Preparation, kinetics, thermodynamics, mechanism and catalysts
Title Atom Transfer Radical Polymerization of End-Functionalized Hydrogen-Bonding Polymers and Resulting Polymer Miscibility
URI http://dx.doi.org/10.1021/ma901822k
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