Ultrathin Conjugated Polymer Network Films of Carbazole Functionalized Poly(p-Phenylenes) via Electropolymerization

Ultrathin Conjugated Polymer Network Films of Carbazole Functionalized Poly(p-Phenylenes) via Electropolymerization

Ultrathin films of a cross-linked and chemically distinct conjugated poly(p-phenylene) network via electropolymerization are described. The amphiphilic network precursor was synthesized by incorporating the alkoxy carbazole group (−O(CH2)5Cb) to a poly(p-phenylene) (C6PPPOH) backbone. In order to in...

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Published in:The journal of physical chemistry. B Vol. 111; no. 23; pp. 6336 - 6343
Main Authors: Ravindranath, Renu, Ajikumar, Parayil Kumaran, Bahulayan, Sheeja, Hanafiah, Nurmawati Bte Muhammad, Baba, Akira, Advincula, Rigoberto C, Knoll, Wolfgang, Valiyaveettil, Suresh
Format: Journal Article
Language:English
Published: United States American Chemical Society 14-06-2007
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Abstract Ultrathin films of a cross-linked and chemically distinct conjugated poly(p-phenylene) network via electropolymerization are described. The amphiphilic network precursor was synthesized by incorporating the alkoxy carbazole group (−O(CH2)5Cb) to a poly(p-phenylene) (C6PPPOH) backbone. In order to investigate the combined thin film electrochemical and photophysical properties of poly(p-phenylene)s and polycarbazole conjugated polymers, C6PPPC5Cb was deposited on substrates using the Langmuir Blodgett Kuhn (LBK) method. The monolayer isotherm of the polymer, C6PPPC5Cb, showed a liquid expanded region slightly different from the parent polymer C6PPPOH. Multilayers (up to 30 layers) were transferred to different substrates such as quartz, gold coated LaSFN9 and ITO substrates for analysis. For conversion to a conjugated polymer network (CPN) film, the electroactive carbazole group was electropolymerized using cyclic voltammetry (CV) resulting in polycarbazole linking units. The differences in the film properties and corresponding changes in the electrochemical behavior indicate the importance of film thickness and electron/ion transport process in cross linked network films. From the electrochemical studies, the scan rate was found to have a considerable effect on electropolymerization with higher oxidation and reduction peak values found for the rigid network polymer compared to the uncrosslinked polymers.
AbstractList Ultrathin films of a cross-linked and chemically distinct conjugated poly(p-phenylene) network via electropolymerization are described. The amphiphilic network precursor was synthesized by incorporating the alkoxy carbazole group (-O(CH2)5Cb) to a poly(p-phenylene) (C6PPPOH) backbone. In order to investigate the combined thin film electrochemical and photophysical properties of poly(p-phenylene)s and polycarbazole conjugated polymers, C6PPPC5Cb was deposited on substrates using the Langmuir Blodgett Kuhn (LBK) method. The monolayer isotherm of the polymer, C6PPPC5Cb, showed a liquid expanded region slightly different from the parent polymer C6PPPOH. Multilayers (up to 30 layers) were transferred to different substrates such as quartz, gold coated LaSFN9 and ITO substrates for analysis. For conversion to a conjugated polymer network (CPN) film, the electroactive carbazole group was electropolymerized using cyclic voltammetry (CV) resulting in polycarbazole linking units. The differences in the film properties and corresponding changes in the electrochemical behavior indicate the importance of film thickness and electron/ion transport process in cross linked network films. From the electrochemical studies, the scan rate was found to have a considerable effect on electropolymerization with higher oxidation and reduction peak values found for the rigid network polymer compared to the uncrosslinked polymers.
Ultrathin films of a cross-linked and chemically distinct conjugated poly(p-phenylene) network via electropolymerization are described. The amphiphilic network precursor was synthesized by incorporating the alkoxy carbazole group (−O(CH2)5Cb) to a poly(p-phenylene) (C6PPPOH) backbone. In order to investigate the combined thin film electrochemical and photophysical properties of poly(p-phenylene)s and polycarbazole conjugated polymers, C6PPPC5Cb was deposited on substrates using the Langmuir Blodgett Kuhn (LBK) method. The monolayer isotherm of the polymer, C6PPPC5Cb, showed a liquid expanded region slightly different from the parent polymer C6PPPOH. Multilayers (up to 30 layers) were transferred to different substrates such as quartz, gold coated LaSFN9 and ITO substrates for analysis. For conversion to a conjugated polymer network (CPN) film, the electroactive carbazole group was electropolymerized using cyclic voltammetry (CV) resulting in polycarbazole linking units. The differences in the film properties and corresponding changes in the electrochemical behavior indicate the importance of film thickness and electron/ion transport process in cross linked network films. From the electrochemical studies, the scan rate was found to have a considerable effect on electropolymerization with higher oxidation and reduction peak values found for the rigid network polymer compared to the uncrosslinked polymers.
Author Ravindranath, Renu
Ajikumar, Parayil Kumaran
Bahulayan, Sheeja
Hanafiah, Nurmawati Bte Muhammad
Valiyaveettil, Suresh
Knoll, Wolfgang
Advincula, Rigoberto C
Baba, Akira
Author_xml – sequence: 1
  givenname: Renu
  surname: Ravindranath
  fullname: Ravindranath, Renu
– sequence: 2
  givenname: Parayil Kumaran
  surname: Ajikumar
  fullname: Ajikumar, Parayil Kumaran
– sequence: 3
  givenname: Sheeja
  surname: Bahulayan
  fullname: Bahulayan, Sheeja
– sequence: 4
  givenname: Nurmawati Bte Muhammad
  surname: Hanafiah
  fullname: Hanafiah, Nurmawati Bte Muhammad
– sequence: 5
  givenname: Akira
  surname: Baba
  fullname: Baba, Akira
– sequence: 6
  givenname: Rigoberto C
  surname: Advincula
  fullname: Advincula, Rigoberto C
– sequence: 7
  givenname: Wolfgang
  surname: Knoll
  fullname: Knoll, Wolfgang
– sequence: 8
  givenname: Suresh
  surname: Valiyaveettil
  fullname: Valiyaveettil, Suresh
BackLink https://www.ncbi.nlm.nih.gov/pubmed/17521182$$D View this record in MEDLINE/PubMed
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Snippet Ultrathin films of a cross-linked and chemically distinct conjugated poly(p-phenylene) network via electropolymerization are described. The amphiphilic network...
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StartPage 6336
Title Ultrathin Conjugated Polymer Network Films of Carbazole Functionalized Poly(p-Phenylenes) via Electropolymerization
URI http://dx.doi.org/10.1021/jp070127b
https://api.istex.fr/ark:/67375/TPS-LDQS2DMD-G/fulltext.pdf
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