Superhydrophobic Surfaces of Electrodeposited Polypyrroles Bearing Fluorinated Liquid Crystalline Segments
Two intrinsic properties of fluorinated tails (F-butyl to F-octyl) were combined in the elaboration of superhydrophobic surfaces by electrochemical polymerization: their promesogenic characteristic and their ability to increase both hydrophobicity and oleophobicity. We report the synthesis and the c...
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| Published in: | Macromolecules Vol. 43; no. 22; pp. 9365 - 9370 |
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23-11-2010
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| Abstract | Two intrinsic properties of fluorinated tails (F-butyl to F-octyl) were combined in the elaboration of superhydrophobic surfaces by electrochemical polymerization: their promesogenic characteristic and their ability to increase both hydrophobicity and oleophobicity. We report the synthesis and the characterization of pyrrole monomers bearing fluorinated liquid crystalline segments. The electrodeposited corresponding polymer films were characterized by cyclic voltammetry, static and dynamic contact angle measurements, and scanning electron microscopy. Sticky superhydrophobic surfaces were obtained with a F-hexyl or a F-octyl tail. The presence of mesogenic segments improves the surface hydrophobicity and increases the surface roughness, clearly observed with F-butyl and F-hexyl chains. |
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| AbstractList | Two intrinsic properties of fluorinated tails (F-butyl to F-octyl) were combined in the elaboration of superhydrophobic surfaces by electrochemical polymerization: their promesogenic characteristic and their ability to increase both hydrophobicity and oleophobicity. We report the synthesis and the characterization of pyrrole monomers bearing fluorinated liquid crystalline segments. The electrodeposited corresponding polymer films were characterized by cyclic voltammetry, static and dynamic contact angle measurements, and scanning electron microscopy. Sticky superhydrophobic surfaces were obtained with a F-hexyl or a F-octyl tail. The presence of mesogenic segments improves the surface hydrophobicity and increases the surface roughness, clearly observed with F-butyl and F-hexyl chains. |
| Author | Guittard, Frederic Darmanin, Thierry Taffin de Givenchy, Elisabeth |
| Author_xml | – sequence: 1 givenname: Thierry surname: Darmanin fullname: Darmanin, Thierry – sequence: 2 givenname: Elisabeth surname: Taffin de Givenchy fullname: Taffin de Givenchy, Elisabeth – sequence: 3 givenname: Frederic surname: Guittard fullname: Guittard, Frederic email: Frederic.GUITTARD@unice.fr |
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| Cites_doi | 10.1002/352760393X 10.1021/ie50320a024 10.1063/1.2745251 10.1021/ma992112k 10.1021/la901193g 10.1080/026782999204183 10.1039/jm9960601107 10.1016/j.jcis.2009.03.073 10.1039/B711226B 10.1080/19447024508659707 10.1021/la101734s 10.1002/3527603905 10.1021/la703821h 10.1021/la801040z 10.1080/0267829031000065155 10.1016/0379-6779(94)90217-8 10.1039/B712575P 10.1039/b904766b 10.1002/adfm.200701454 10.1002/anie.200500266 10.1039/b804617d 10.1080/15421400590955154 10.1039/b810184a 10.1002/adma.200800836 10.1021/ma992111s 10.1080/00397919608003488 10.1016/j.jcis.2006.07.052 10.1016/j.cocis.2006.06.002 10.1021/la103310m 10.1021/la703766c 10.1039/tf9444000546 10.1021/ma050394k 10.1039/b602486f 10.1080/02678290410001667353 10.1007/s003960100487 10.1021/ja901392s |
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| Keywords | Fluorine containing polymer Aromatic polymer Pyrrole derivative polymer Chiral compound Hydrophobicity Experimental study Electrochemical polymerization Lateral group Conjugated polymer Electrochemical properties Thioester Morphology Preparation Microroughness Surface properties Hydrophobic group Sulfur containing polymer |
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| Title | Superhydrophobic Surfaces of Electrodeposited Polypyrroles Bearing Fluorinated Liquid Crystalline Segments |
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