Effect of Flexibility and Nanotriboelectrification on the Dynamic Reversibility of Water Intrusion into Nanopores: Pressure-Transmitting Fluid with Frequency-Dependent Dissipation Capability

In this article, the effect of a porous material’s flexibility on the dynamic reversibility of a nonwetting liquid intrusion was explored experimentally. For this purpose, high-pressure water intrusion together with high-pressure in situ small-angle neutron scattering were applied for superhydrophob...

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Published in:	ACS applied materials & interfaces Vol. 11; no. 43; pp. 40842 - 40849
Main Authors:	Lowe, Alexander, Tsyrin, Nikolay, Chorążewski, Mirosław, Zajdel, Paweł, Mierzwa, Michał, Leão, Juscelino B, Bleuel, Markus, Feng, Tong, Luo, Dong, Li, Mian, Li, Dan, Stoudenets, Victor, Pawlus, Sebastian, Faik, Abdessamad, Grosu, Yaroslav
Format:	Journal Article
Language:	English
Published:	American Chemical Society 30-10-2019
Subjects:	porous material flexibility anti-vibration protection MOF smart working body energy storage/dissipation
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Abstract	In this article, the effect of a porous material’s flexibility on the dynamic reversibility of a nonwetting liquid intrusion was explored experimentally. For this purpose, high-pressure water intrusion together with high-pressure in situ small-angle neutron scattering were applied for superhydrophobic grafted silica and two metal–organic frameworks (MOFs) with different flexibility [ZIF-8 and Cu2(tebpz) (tebpz = 3,3′,5,5′tetraethyl-4,4′-bipyrazolate)]. These results established the relation between the pressurization rate, water intrusion–extrusion hysteresis, and porous materials’ flexibility. It was demonstrated that the dynamic hysteresis of water intrusion into superhydrophobic nanopores can be controlled by the flexibility of a porous material. This opens a new area of applications for flexible MOFs, namely, a smart pressure-transmitting fluid, capable of dissipating undesired vibrations depending on their frequency. Finally, nanotriboelectric experiments were conducted and the results showed that a porous material’s topology is important for electricity generation while not affecting the dynamic hysteresis at any speed.
AbstractList	In this article, the effect of a porous material’s flexibility on the dynamic reversibility of a nonwetting liquid intrusion was explored experimentally. For this purpose, high-pressure water intrusion together with high-pressure in situ small-angle neutron scattering were applied for superhydrophobic grafted silica and two metal–organic frameworks (MOFs) with different flexibility [ZIF-8 and Cu2(tebpz) (tebpz = 3,3′,5,5′tetraethyl-4,4′-bipyrazolate)]. These results established the relation between the pressurization rate, water intrusion–extrusion hysteresis, and porous materials’ flexibility. It was demonstrated that the dynamic hysteresis of water intrusion into superhydrophobic nanopores can be controlled by the flexibility of a porous material. This opens a new area of applications for flexible MOFs, namely, a smart pressure-transmitting fluid, capable of dissipating undesired vibrations depending on their frequency. Finally, nanotriboelectric experiments were conducted and the results showed that a porous material’s topology is important for electricity generation while not affecting the dynamic hysteresis at any speed.
Author	Faik, Abdessamad Grosu, Yaroslav Li, Dan Zajdel, Paweł Leão, Juscelino B Lowe, Alexander Tsyrin, Nikolay Chorążewski, Mirosław Bleuel, Markus Feng, Tong Mierzwa, Michał Luo, Dong Pawlus, Sebastian Li, Mian Stoudenets, Victor
AuthorAffiliation	Department of Chemistry NIST Center for Neutron Research Institute of Chemistry University of Silesia University of Maryland Institute of Physics CIC Energigune National Technical University of Ukraine “Igor Sikorsky Kyiv Polytechnic Institute” Laboratory of Thermomolecular Energetics Department of Materials Science and Engineering Silesian Center for Education and Interdisciplinary Research College of Chemistry and Materials Science
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