Search Results - "de Aquino Neto, Francisco Radler"
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Determination of adulterants in whey protein food supplements by liquid chromatography coupled to Orbitrap high resolution mass spectrometry
Published in Brazilian Journal of Food Technology (01-01-2019)“…Liquid chromatography coupled to Orbitrap high resolution mass spectrometry was shown to be an adequate technique to control the adulteration of whey protein…”
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2
Qualitative transformations of street‐seized ecstasy over a decade: A case study in Rio de Janeiro (Brazil)
Published in Journal of forensic sciences (01-07-2024)“…The illegal drug market is constantly evolving, with new drugs being created and existing ones being modified. Adulterants are often added to the mix, and the…”
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3
Feasibility study for the development of a certified reference material of nitrofuran metabolites in chicken breast muscle from incurred samples
Published in Measurement : journal of the International Measurement Confederation (01-12-2018)“…•The present work involves a study to develop a metabolite-incurred reference material.•Water content and mass fraction of nitrofuran metabolites in chicken…”
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4
Hansen Solubility Parameters Applied to the Extraction of Phytochemicals
Published in Plants (Basel) (01-08-2023)“…In many analytical chemical procedures, organic solvents are required to favour a better global yield upon the separation, extraction, or isolation of the…”
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5
Extraction of Diterpene-Phytochemicals in Raw and Roasted Coffee Beans and Beverage Preparations and Their Relationship
Published in Plants (Basel) (01-04-2023)“…Cafestol and kahweol are expressive furane-diterpenoids from the lipid fraction of coffee beans with relevant pharmacological properties for human health. Due…”
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6
Symptoms prevalence among office workers of a sealed versus a non-sealed building: Associations to indoor air quality
Published in Environment international (01-11-2009)“…An increasing number of complaints related to time spent in artificially ventilated buildings have been progressively reported and attributed, at least in…”
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Distribution of polycyclic aromatic hydrocarbons in surface sediments and waters from Guanabara Bay, Rio de Janeiro, Brazil
Published in Journal of the Brazilian Chemical Society (2007)“…Polycyclic aromatic hydrocarbons (PAHs) were identified and quantified in sediment and water samples from 12 sites in the north-northeast region of the…”
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8
Quantitative evaluation of sedimentary organic matter from Laguna Mar Chiquita, Argentina
Published in Organic geochemistry (01-04-2008)“…Laguna Mar Chiquita (Central Argentina) is a highly variable saline lake particularly suitable for palaeolimnological studies. The most recent (20th century)…”
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Development and validation of a multidimensional gas chromatography/combustion/isotope ratio mass spectrometry-based test method for analyzing urinary steroids in doping controls
Published in Analytica chimica acta (07-11-2018)“…The misuse of the steroid hormone testosterone for performance enhancement has been frequently reported in the past, and its administration is prohibited in…”
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10
New approaches to monitor semi-volatile organic compounds released during coffee roasting using flow-through/active sampling and comprehensive two-dimensional gas chromatography
Published in Food research international (01-05-2019)“…A novel dynamic approach is described to profile volatile organic compound (VOC) and semi-VOC (SVOC) emission during coffee roasting aimed at analysing…”
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11
Risk factors and future directions for preventing and diagnosing exertional rhabdomyolysis
Published in Neuromuscular disorders : NMD (01-07-2021)“…•Exertional Rhabdomyolysis (ERM) represents a potentially serious health condition.•ERM is common in military personnel, untrained and high-performance…”
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12
Lipase-catalysed esters synthesis of cafestol and kahweol
Published in Food chemistry (01-09-2018)“…•A preparative method was developed to obtain 1.290 g of cafestol and kahweol (C&K).•Lipase-catalysed esterification was established by Central Composite…”
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13
Use of quantitative 1H and 13C NMR to determine the purity of organic compound reference materials: a case study of standards for nitrofuran metabolites
Published in Analytical and bioanalytical chemistry (01-03-2021)“…Comparability of measurement results and their metrological traceability to the International System of Units (SI) are fundamental tools to ensure reliable…”
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14
Implementation and Performance of the Gas Chromatography/Combustion/Isotope Ratio Mass Spectrometry-Based Method for the Confirmatory Analysis of Endogenous Anabolic Steroids during the Rio de Janeiro Olympic and Paralympic Games 2016
Published in Analytical chemistry (Washington) (17-09-2019)“…Carbon isotope ratio (CIR) confirmation is one of the most complex and delicate analyses in the doping control field, due to the nature of the molecules to be…”
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15
Investigating the capability of UA-DLLME and DART-HRMS in the analysis of benzodiazepines in whole human blood
Published in Forensic chemistry (01-07-2024)“…[Display omitted] •Determination of benzodiazepines in ante and postmortem human blood samples.•UA-DLLME enabled an efficient extraction of 10 benzodiazepines…”
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16
Gene doping and genomic science in sports: where are we?
Published in Bioanalysis (01-06-2020)“…The misuse of sport-related gene transfer methods in elite athletes is a real and growing concern. The success of gene therapy in the treatment of hereditary…”
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Detection of designer steroid methylstenbolone in “nutritional supplement” using gas chromatography and tandem mass spectrometry: Elucidation of its urinary metabolites
Published in Steroids (01-02-2013)“…► Detection of designer steroid methylstenbolone in “nutritional supplement”. ► Identification of two long-term 16-hydroxylated methylstenbolone metabolites. ►…”
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18
Comparative profile of pollutants generated by a stationary engine fueled with diesel, biodiesel, and ethanol
Published in Journal of aerosol science (01-10-2016)“…Fossil fuel emissions derived from crude oil have a significant impact on the environment, climate change, air pollution, and others. Under these…”
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Running ahead of doping: analytical advances and challenges faced by modern laboratories ahead of Rio 2016
Published in Bioanalysis (01-09-2016)Get full text
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20
Atmospheric distribution of organic compounds from urban areas near Olympic games sites in Rio de Janeiro, Brazil
Published in Microchemical journal (01-07-2017)“…The hydrocarbon composition of atmospheric particulate matter (PM) and Volatile Organic Compounds (VOC) from urban areas of Rio de Janeiro City were studied to…”
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