Chemo-enzymatic synthesis of (S,S)-2,2′-(ethylenediamino)dibutan-1-ol

A chemo-enzymatic method is proposed for the preparation of ( S,S )-2,2′-(ethylenediamino)dibutan-1-ol based on the synthesis of racemic (±)- N -carbobenzoxy-2-amino-butan-1-ol and its enantioselective acylation in the presence of lipase at a key resolution step to release the optically active alcoh...

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Bibliographic Details

Published in:	Russian chemical bulletin Vol. 72; no. 5; pp. 1268 - 1273
Main Authors:	Yufryakov, V. S., Tsvetikova, M. A., Bystrova, N. A., Kochetkov, K. A.
Format:	Journal Article
Language:	English
Published:	New York Springer US 01-05-2023 Springer Nature B.V
Subjects:	Acylation Brief Communications Chemistry Chemistry and Materials Science Chemistry/Food Science Enantiomers Inorganic Chemistry Optical activity Organic Chemistry Synthesis ( 2,2′-(ethylenediamino)dibutan-1-ol PPL lipase enantioselective acylation chemo-enzymatic cleavage
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