Search Results - "Vassileva, Emilia"
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Simultaneous speciation analysis of mercury in marine origin samples by high performance liquid chromatography and species - specific isotope dilution inductively coupled plasma mass spectrometry
Published in Talanta (Oxford) (01-09-2020)“…Species-specific isotope dilution inductively coupled plasma quadrupole mass spectrometry reference method and high-performance liquid chromatography were…”
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Journal Article -
2
Determination of methylmercury in marine biota samples: Method validation
Published in Talanta (Oxford) (01-05-2014)“…Regulatory authorities are expected to measure concentration of contaminants in foodstuffs, but the simple determination of total amount cannot be sufficient…”
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Journal Article -
3
Determination of ultra-trace level of 232Th in seawater by ICP-SFMS after matrix separation and preconcentration
Published in Analytica chimica acta (13-02-2018)“…This article describes the development and validation of an analytical procedure for the matrix separation, preconcentration and determination of sub-ng kg−1…”
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Journal Article -
4
Reference measurements for total mercury and methyl mercury content in marine biota samples using direct or species-specific isotope dilution inductively coupled plasma mass spectrometry
Published in Talanta (Oxford) (01-11-2016)“…The analytical procedures for reference measurements of the total Hg and methyl mercury (MeHg) mass fractions at various concentration levels in marine biota…”
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5
Off-line preconcentration and inductively coupled plasma sector field mass spectrometry simultaneous determination of Cd, Co, Cu, Mn, Ni, Pb and Zn mass fractions in seawater: Procedure validation
Published in Spectrochimica acta. Part B: Atomic spectroscopy (01-03-2019)“…Despite the ongoing reduction of emissions of contaminants into the environment, the ocean still represents the most anthropogenically impacted ecosystem…”
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Reference Measurements for Priority and Essential Trace Elements and Methyl Mercury with Isotope Dilution Inductively Coupled Plasma-Mass Spectrometry for Seafood Safety Assessment and CRM Production
Published in Food analytical methods (01-02-2020)“…The continuous release of anthropogenic pollutants into marine environment increases the needs for the development of analytical procedures for their accurate…”
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7
Determination of low-level plutonium in seawater by sector field inductively coupled plasma mass spectrometry: method validation
Published in Environmental science and pollution research international (01-03-2017)“…Sources of plutonium isotopes to the marine environment are well defined, both spatially and temporally which makes plutonium (Pu) a potential tracer for…”
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Journal Article -
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Reference measurements for cadmium, copper, mercury, lead, zinc and methyl mercury mass fractions in scallop sample by isotope dilution inductively coupled plasma mass spectrometry
Published in Microchemical journal (01-09-2014)“…A marine certified reference material (CRM), IAEA 452, prepared with scallop (Pecten maximus) sample was recently produced by the Environment Laboratories of…”
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Journal Article -
9
Chemical Forms of Mercury in Blue Marlin Billfish: Implications for Human Exposure
Published in Environmental science & technology letters (11-05-2021)“…Although fish is an important source of nutrients, including some of the healthiest proteins, long-chain fatty acids, and essential selenium, species at the…”
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Journal Article -
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Determination of ultra-trace level 241Am in marine sediment and seawater by combining TK200-TK221 tandem-column extraction chromatography and SF ICP-MS
Published in Talanta (Oxford) (01-05-2024)“…Sound strategies for marine chemical monitoring call for measurement systems capable of producing comparable analytical results with demonstrated quality. This…”
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Journal Article -
11
Rapid determination of femtomolar methylmercury in seawater using automated GC-AFS method: Optimisation of the extraction step and method validation
Published in Talanta (Oxford) (01-09-2021)“…Among ionic mercury species methyl mercury (MMHg) is the most toxic form present in the environment, which is known to be bio-accumulative neurotoxin in the…”
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Journal Article -
12
Influence of the correction for moisture/water content on the quality of the certification of cadmium, copper and lead mass fractions in rice
Published in Food chemistry (15-02-2008)“…The moisture/water content of rice sample was determined by means of three different methods: oven drying, Karl Fischer titration and thermogravimetry. These…”
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Journal Article Conference Proceeding -
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Method validation for high resolution sector field inductively coupled plasma mass spectrometry determination of the emerging contaminants in the open ocean: Rare earth elements as a case study
Published in Spectrochimica acta. Part B: Atomic spectroscopy (01-02-2017)“…Analytical procedure for the determination of fourteen rare earth elements (REEs) in the seawater samples has been developed and validated. The elements (La,…”
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Journal Article -
14
Certification measurement of the cadmium, copper and lead contents in rice using isotope dilution inductively coupled plasma mass spectrometry
Published in Analytica chimica acta (09-08-2004)“…This paper describes the certification of the Cd, Cu and Pb amount contents in a rice material, that were used as reference values for round 19 of the…”
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Journal Article -
15
Determination of cadmium, copper, mercury, lead and zinc mass fractions in marine sediment by isotope dilution inductively coupled plasma mass spectrometry applied as a reference method
Published in Microchemical journal (01-09-2016)“…Isotope Dilution Inductively Coupled Plasma Mass Spectrometry (ID ICP-MS) has been applied for the determination of the total mass fractions of five trace…”
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Journal Article -
16
Determination of methylmercury in marine sediment samples: Method validation and occurrence data
Published in Analytica chimica acta (01-01-2015)“…[Display omitted] •A method for MeHg determination at trace level in marine sediments is completely validated.•Validation is performed according to ISO-17025…”
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Journal Article -
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Determination of methylmercury in marine biota samples with advanced mercury analyzer: Method validation
Published in Food chemistry (01-06-2015)“…•A method for determination of MeHg at trace level in marine biota is validated.•Validation was performed according to the ISO-17025 and Eurachem…”
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Journal Article -
18
Determination of ultra-trace level 241 Am in marine sediment and seawater by combining TK200-TK221 tandem-column extraction chromatography and SF ICP-MS
Published in Talanta (Oxford) (26-01-2024)“…Sound strategies for marine chemical monitoring call for measurement systems capable of producing comparable analytical results with demonstrated quality. This…”
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Journal Article -
19
Determination of ultra-trace level of ^sup 232^Th in seawater by ICP-SFMS after matrix separation and preconcentration
Published in Analytica chimica acta (13-02-2018)“…This article describes the development and validation of an analytical procedure for the matrix separation, preconcentration and determination of sub-ng kg-1…”
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Journal Article -
20
Development of procedure for measurement of Pb isotope ratios in seawater by application of seaFAST sample pre-treatment system and Sector Field Inductively Coupled Plasma Mass Spectrometry
Published in Spectrochimica acta. Part B: Atomic spectroscopy (01-12-2016)“…Anthropogenic Pb in the oceans, derived from high-temperature industrial processes, fuel combustion and incineration can have an isotopic signature distinct…”
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