Search Results - "Steigerwald, Thomas G."
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Solubility and dissolution kinetics of GaN in supercritical ammonia in presence of ammonoacidic and ammonobasic mineralizers
Published in Journal of crystal growth (01-12-2017)“…•Solubility and dissolution kinetics of GaN under ammonoacidic and -basic conditions.•Results suggest a significant refinement of raw gravimetric literature…”
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Journal Article -
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In situ investigation of decomposing ammonia and ammonobasic solutions under supercritical conditions via UV/vis and Raman Spectroscopy
Published in The Journal of supercritical fluids (01-04-2018)“…[Display omitted] •Visualization of temperature dependence of NH3 decomposing to N2 and H2.•Maximum temperature in the autoclave = 563 °C, at heating…”
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3
Chemical stability of carbon-based inorganic materials for in situ x-ray investigations of ammonothermal crystal growth of nitrides
Published in Journal of crystal growth (15-12-2016)“…The chemical stability of diamond, silicon carbide, vitreous carbon, and boron carbide in supercritical ammonia containing different mineralizers was…”
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4
Feasibility of density and viscosity measurements under ammonothermal conditions
Published in Journal of crystal growth (01-10-2014)“…With an eye on numerical simulations of ammonothermal growth of group III–V bulk single crystals, precise data for viscosity and density are strongly needed…”
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Journal Article Conference Proceeding -
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Flow Stability, Convective Heat Transfer and Chemical Reactions in Ammonothermal Autoclaves—Insights by In Situ Measurements of Fluid Temperatures
Published in Crystals (Basel) (01-09-2020)“…A variety of functional nitride materials, including the important wide bandgap semiconductor GaN, can be crystallized in exceptionally good structural quality…”
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Journal Article -
6
Ceramic liner technology for ammonoacidic synthesis
Published in The Journal of supercritical fluids (01-04-2015)“…•Corrosion behaviour of several ceramics under ammonothermal conditions.•Technical ceramics include: nitride and nitride bonded silicon carbide…”
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Solubility Studies of Sodium Azide in Liquid Ammonia by In Situ Ultrasonic Velocity Measurement
Published in Chemical engineering & technology (01-06-2017)“…Ultrasonic velocity measurement data has been established as a simple and convenient tool to determine different thermodynamic properties of liquids and…”
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High-temperature corrosion of Inconel®Alloy 718, Haynes®282®Alloy and CoWAlloy1&2 in supercritical ammonia/ammonium chloride solution
Published in Journal of crystal growth (15-09-2018)“…•Detailed supercritical corrosion study under ammonoacidic conditions.•Comparison of Co-base and Ni-base superalloys under ammonoacidic conditions.•Mostly…”
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Different corrosion behaviour of autoclaves made of nickel base alloy 718 in ammonobasic and ammonoacidic environments
Published in The Journal of supercritical fluids (01-11-2014)“…•Metallographic investigation of corrosion behaviour of ammonothermal autoclaves.•Ammonobasic conditions lead to formation of corrosion layer.•Ammonoacidic…”
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Electro Discharge Machining – A Suitable Fabrication Process for High‐Pressure/High‐Temperature Equipment
Published in Chemical engineering & technology (01-05-2018)“…Electro discharge machining (EDM) is an important manufacturing process for hard‐to‐cut materials like nickel‐based alloys, e.g., alloy 718. Its high yield…”
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Corrosive Degeneration of Autoclaves for the Ammonothermal Synthesis: Experimental Approach and First Results
Published in Chemical engineering & technology (01-11-2014)“…The ammonothermal growth of different bulk group III nitride materials enables cost‐efficient production of high‐quality single crystals. Despite its…”
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Journal Article -
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Applicability of Metals as Liner Materials for Ammonoacidic Crystal Growth
Published in Chemical engineering & technology (01-11-2014)“…The ammonoacidic crystal growth allows industrial production of bulk semiconductor materials like gallium nitride as a widely known material for applications…”
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Journal Article -
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Determination of GaN solubility in supercritical ammonia with NH4F and NH4Cl mineralizer by in situ x-ray imaging of crystal dissolution
Published in Journal of crystal growth (15-05-2015)“…Quantitative data on the solubility of GaN in supercritical ammonia using NH4F as mineralizer are reported. The solubility is determined by in situ x-ray…”
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Journal Article -
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Determination of GaN solubility in supercritical ammonia with NH sub(4)F and NH sub(4)Cl mineralizer by in situ x-ray imaging of crystal dissolution
Published in Journal of crystal growth (05-05-2015)“…Quantitative data on the solubility of GaN in supercritical ammonia using NH sub(4)F as mineralizer are reported. The solubility is determined by in situ x-ray…”
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Journal Article