Search Results - "Sevillano Cabeza, A"
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New micromethod combining miniaturized matrix solid-phase dispersion and in-tube in-valve solid-phase microextraction for estimating polycyclic aromatic hydrocarbons in bivalves
Published in Journal of Chromatography A (21-11-2008)“…Miniaturized matrix solid-phase dispersion (MSPD) was developed for the extraction of common polycyclic aromatic hydrocarbons (PAHs) from bivalve samples (100…”
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In-tube solid-phase microextraction coupled by in valve mode to capillary LC-DAD: Improving detectability to multiresidue organic pollutants analysis in several whole waters
Published in Journal of Chromatography A (16-04-2010)“…A simple and fast capillary chromatographic method has been developed to identify and quantify organic pollutants at sub-ppb levels in real water samples. The…”
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Rapid fluorimetric assay for primary amine groups in water samples
Published in Analytical and bioanalytical chemistry (01-07-2003)“…Bond Elut C(18) solid-phase extraction cartridges were used for pre-concentration followed by derivatization with o-phthaldialdehyde-N-acetylcysteine (OPA-NAC)…”
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Creatinine determination in urine samples by batchwise kinetic procedure and flow injection analysis using the Jaffé reaction: chemometric study
Published in Talanta (Oxford) (24-12-2001)“…The classical Jaffé reaction for the determination of creatinine in urine samples is tested. A comparative study of the main analytical characteristics…”
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Off-line dansylation of amines using C18 solid-phase packings : study of the fluorescence and chemiluminescence detection by post-column derivatization with oxalic acid bis(2, 4, 6-trichloro phenyl ester)/H2O2 in liquid chromatography. Determination of amphetamines in urine samples
Published in Analytica chimica acta (04-01-1999)Get full text
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Automated pre-column derivatization of amines in biological samples with dansyl chloride and with or without post-column chemiluminescence formation by using TCPO-H2O2
Published in Analyst (London) (01-12-1998)“…On-line automation of two different liquid chromatographic procedures, a pre-column derivatization system and a pre- and post-column system, in order to…”
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Liquid Chromatographic Analysis of Amphetamine and Related Compounds in Urine Using Solid-Phase Extraction and 3,5-Dinitrobenzoyl Chloride for Derivatization
Published in Journal of chromatographic science (01-04-1997)“…A chromatographic method for the analysis of amphetamine and related compounds in urine using 3,5-dinitrobenzoyl chloride (3,5-DNB) as a labeling reagent is…”
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Improved detection limits for screening of diuretics by coupled liquid chromatography and ultraviolet-visible spectrophotometry
Published in Journal of chromatography (26-02-1993)“…Experimental conditions have been studied in order to improve the sensitivity for the analysis of diuretics and probenecid in urine samples by high-performance…”
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Estimation of diuretic drugs in biological fluids by HPLC
Published in Chromatographia (01-02-1992)Get full text
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Determination of triamterene in urine by HPLC using fluorescence detection and column-switching
Published in Chromatographia (1994)“…A liquid chromatographic method incorporating column-switching and fluorimetric detection for the determination of triamterene in untreated urine, is…”
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Determination of methamphetamine in urine samples with sodium 1,2-naphthoquinone-4-sulphonate
Published in Fresenius' Journal of Analytical Chemistry (01-04-1994)Get full text
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Determination of vitamin B12 as cobalt by use of a catalytic-spectrophotometric method
Published in Analyst (London) (01-03-1987)Get more information
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Urine polyamines determination using dansyl chloride derivatization in solid-phase extraction cartridges and HPLC
Published in Analyst (London) (01-04-1999)“…The derivatization of biogenic amines such as putrescine, cadaverine, spermidine and spermine with dansyl chloride in solid phase extraction cartridges is…”
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o-Phthalaldehyde– N-acetylcysteine polyamine derivatives: formation and stability in solution and in C 18 supports
Published in Journal of chromatography. Biomedical applications (15-08-2001)“…A comparative study of different derivatization procedures has been performed in order to improve the stability of the reaction products o-phthalaldehyde–…”
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Improved amphetamine and methamphetamine determination in urine by normal-phase high-performance liquid chromatography with sodium 1,2-naphthoquinone 4-sulphonate as derivatizing agent and solid-phase extraction for sample clean-up
Published in Journal of chromatography. Biomedical applications (20-01-1995)“…Solid-phase extraction techniques were evaluated for the treatment of urine samples in the analysis of amphetamine and methamphetamine by normal-phase…”
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On-Line Derivatization into Precolumns for the Determination of Drugs by Liquid Chromatography and Column Switching: Determination of Amphetamines in Urine
Published in Analytical chemistry (Washington) (01-03-1996)“…A chromatographic system for the on-line derivatization of drugs using column switching is described. The system uses a 20 mm × 2.1 mm i.d. precolumn packed…”
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A new derivatization procedure for the determination of cephalexin with 1,2-naphthoquinone 4-sulphonate in pharmaceutical and urine samples using solid-phase extraction cartridges and UV–visible detection
Published in Analytica chimica acta (07-09-1998)“…The present report shows how to derivatize cephalexin with 1,2-naphthoquinone-4-sulphonate (NQS) into solid-phase extraction cartridges (C 18) using UV–visible…”
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Off-line dansylation of amines using C 18 solid-phase packings: study of the fluorescence and chemiluminescence detection by post-column derivatization with oxalic acid bis(2, 4, 6-trichloro phenyl ester)/H 2O 2 in liquid chromatography. Determination of amphetamines in urine samples
Published in Analytica chimica acta (1999)“…Dansylation of amines (primaries and secondaries) using C 18 solid-phase supports is described. The time of analysis and the handing sample have been markedly…”
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