Search Results - "Santos, Wallans"
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Simultaneous determination of caffeine, paracetamol, and ibuprofen in pharmaceutical formulations by high-performance liquid chromatography with UV detection and by capillary electrophoresis with conductivity detection
Published in Journal of separation science (01-05-2015)“…Paracetamol, caffeine and ibuprofen are found in over‐the‐counter pharmaceutical formulations. In this work, we propose two new methods for simultaneous…”
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Dehydration of d-fructose to 5-hydroxymethyl-2-furfural in DMSO using a hydrophilic sulfonated silica catalyst in a process promoted by microwave irradiation
Published in Scientific reports (21-01-2021)“…SiO 2 -SO 3 H, with a surface area of 115 m 2 /g, pore volumes of 0.38 cm 3 g −1 and 1.32 mmol H + /g, was used as a 10% w/w catalyst for the preparation of…”
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A simple method to detect the stimulant modafinil in authentic saliva using a carbon-nanotube screen-printed electrode with adsorptive stripping voltammetry
Published in Sensors and actuators. B, Chemical (15-04-2019)“…•Analytically electrochemical oxidation signals from the stimulant drug modafinil are seen on carbon electrodes.•An electrochemical method using adsorptive…”
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Electrochemical detection of mephedrone using a graphene screen-printed electrode: a new sensitive and selective approach to identify synthetic cathinones in forensic analysis
Published in Analyst (London) (27-03-2023)“…Mephedrone (MEP) is an illicit stimulant drug that belongs to the synthetic cathinone (SC) class, which has been widely used for recreational purposes and…”
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Critical evaluation of voltammetric techniques for antioxidant capacity and activity: Presence of alumina on glassy-carbon electrodes alters the results
Published in Electrochimica acta (20-10-2020)“…Voltammetric techniques have been widely applied to determine the food antioxidant capacity/activity using different electrochemical parameters (peak current,…”
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Simple and Sensitive Determination of Sibutramine in Slimming Tea Beverages Using a Carbon Screen‐printed Electrode with Adsorptive Stripping Voltammetry
Published in Electroanalysis (New York, N.Y.) (01-05-2019)“…The stimulant sibutramine is an anorexic agent found as an adulterant in natural products and multivitamins supplements used for weight‐loss. In this work, a…”
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Electrochemical platform produced by 3D printing for analysis of small volumes using different electrode materials
Published in Talanta (Oxford) (01-12-2023)“…Fused deposition modeling (FDM) 3D printing is a promising additive manufacturing technique to produce low-cost disposable electrochemical devices. However,…”
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Electrochemical detection of eutylone using screen-printed electrodes: Rapid and simple screening method for application in forensic samples
Published in Electrochimica acta (20-04-2022)“…•Portable and fast electrochemical screening for forensic applications.•Sample preparation compatibility for a preliminary and definitive…”
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A nano-carbon electrode optimized for adsorptive stripping voltammetry: Application to detection of the stimulant selegiline in authentic saliva
Published in Sensors and actuators. B, Chemical (15-01-2019)“…•A multilayer nano-carbon modified electrode is prepared and optimized for adsorptive stripping voltammetry.•Multilayers of Carbon Black promote adsorptive…”
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Electrochemical detection of the synthetic cathinone 3,4-methylenedioxypyrovalerone using carbon screen-printed electrodes: A fast, simple and sensitive screening method for forensic samples
Published in Electrochimica acta (10-09-2020)“…In this work, the electrochemical detection of 3,4-methylenedioxypyrovalerone (MDPV), a synthetic cathinone used as a stimulant drug, is presented for the…”
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Rapid and simple voltammetric screening method for Lysergic Acid Diethylamide (LSD) detection in seized samples using a boron-doped diamond electrode
Published in Sensors and actuators. B, Chemical (01-10-2021)“…•Voltammetric detection of LSD using boron-doped diamond electrode.•Interference study for twenty (20) phenethylamines derivatives as NBOMes and NBOHs.•Fast…”
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Altered electrochemistry of amiloride drug on boron-doped diamond electrode: Rapid and selective detection in urine by square-wave cathodic stripping voltammetry for application in doping control
Published in Electrochimica acta (20-03-2021)“…The amiloride (AMI) is a diuretic drug and has been illegally used in sports competitions. The development of simpler and faster analytical methods for AMI…”
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Development of a simple and rapid screening method for the detection of 1-(3-chlorophenyl)piperazine in forensic samples
Published in Talanta (Oxford) (01-10-2021)“…1-(3-chlorophenyl) piperazine (mCPP) is a synthetic drug with hallucinogenic effects that has often been found in seized samples. In this context, easy to use…”
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Fast Screening and Determination of Tadalafil in Pharmaceutics by Batch Injection Analysis (BIA) with Amperometric Detection
Published in Electroanalysis (New York, N.Y.) (01-10-2020)“…Tadalafil (TDL) is the active ingredient of Cialis®, one of the top selling drugs for the treatment of erectile dysfunction and very counterfeit worldwide. In…”
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An innovative approach for selective and robust screening of NBOHs, NBOMes, and LSD in forensic samples using a 3D-Printed electrochemical double cell
Published in Talanta (Oxford) (15-08-2024)“…Lysergic acid diethylamide (LSD) and two phenethylamine classes (NBOHs and NBOMes) are the main illicit drugs found in seized blotter papers. The preliminary…”
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Novel disposable and portable 3D-printed electrochemical apparatus for fast and selective screening of 25E-NBOH in forensic samples
Published in Talanta (Oxford) (01-03-2024)“…The advent of new psychoactive substances (NPS) has caused enormous difficulty for legal control since they are rapidly commercialized, and their chemical…”
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Simple and rapid determination of clonidine in pharmaceutical samples by voltammetry using a bare glassy carbon electrode
Published in Electroanalysis (New York, N.Y.) (01-05-2023)“…This work presents, for the first time, the voltammetric behavior of clonidine (CLO) drug and its determination, using an unmodified glassy carbon electrode…”
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Electrochemistry of the synthetic tryptamine 5-MeO-MiPT at glassy carbon and screen-printed electrodes: A rapid and simple screening method for application in forensic analysis
Published in Sensors and actuators. B, Chemical (15-10-2023)“…5-Methoxy-N-methyl-N-isopropyltryptamine (5-MeO-MiPT), also known as moxy, is a synthetic tryptamine analogue used recreationally as a hallucinogenic drug…”
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Altered electrochemistry of oxcarbazepine on cathodically treated boron-doped diamond electrode: Selective detection by pulsed amperometric detection coupled to flow-injection analysis
Published in Electrochimica acta (10-01-2018)“…This work presents a novel electrochemical method for the determination of oxcarbazepine (OXC) in urine and pharmaceutical samples using a flow injection…”
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