Search Results - "O'Neil, Glen D."
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Single-step fabrication of electrochemical flow cells utilizing multi-material 3D printing
Published in Electrochemistry communications (01-02-2019)“…Here we present methodology for fabricating electrochemical flow cells with embedded carbon-composite electrodes in a single step using simultaneous 3D…”
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Electrodeposition Parameters Dramatically Influence the Morphology, Stability, and Performance of n‐Si/Pt Light‐Addressable Electrochemical Sensors
Published in ChemElectroChem (01-12-2023)“…Light addressable electrochemical (LAE) sensors have seen great utility in the past several years because they enable multiple localized electrochemical…”
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Voltammetric pH Measurements in Unadulterated Foodstuffs, Urine, and Serum with 3D-Printed Graphene/Poly(Lactic Acid) Electrodes
Published in Analytical chemistry (Washington) (17-11-2020)“…The pH of a system is a critical descriptor of its chemistryimpacting reaction rates, solubility, chemical speciation, and homeostasis. As a result, pH is one…”
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Trace Analysis of Heavy Metals (Cd, Pb, Hg) Using Native and Modified 3D Printed Graphene/Poly(Lactic Acid) Composite Electrodes
Published in Electroanalysis (New York, N.Y.) (01-04-2020)“…Here we investigate the use of 3D printed graphene/poly(lactic acid) (PLA) electrodes for quantifying trace amounts of Hg, Pb, and Cd. We prepared cylindrical…”
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Square-Wave Voltammetry Enables Measurement of Light-Activated Oxidations and Reductions on n‑Type Semiconductor/Metal Junction Light-Addressable Electrochemical Sensors
Published in Analytical chemistry (Washington) (20-06-2023)“…Light-addressable electrochemical (LAE) sensing is a photoelectrochemical technique that enables high-density, individually addressed electrochemical…”
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Photoelectrochemistry of Redox-Active Self-Assembled Monolayers Formed on n‑Si/Au Nanoparticle Photoelectrodes
Published in Langmuir (20-08-2024)“…Controlling the chemistry of the electrode–solution interface is critically important for applications in sensing, energy storage, corrosion prevention,…”
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Direct Identification and Analysis of Heavy Metals in Solution (Hg, Cu, Pb, Zn, Ni) by Use of in Situ Electrochemical X‑ray Fluorescence
Published in Analytical chemistry (Washington) (05-05-2015)“…The development and application of a new methodology, in situ electrochemical X-ray fluorescence (EC-XRF), is described that enables direct identification and…”
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Evidence of martian perchlorate, chlorate, and nitrate in Mars meteorite EETA79001: Implications for oxidants and organics
Published in Icarus (New York, N.Y. 1962) (01-02-2014)“…•Analyses of martian meteorite EETA79001 show presence of ClO4-, ClO3-, and NO3-.•ClO4- concentration too high to be accounted for by accumulation during 12kyr…”
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Light-Addressable Electrochemical Sensing with Electrodeposited n‑Silicon/Gold Nanoparticle Schottky Junctions
Published in Analytical chemistry (Washington) (18-08-2020)“…Light-addressable electrochemical sensors (LAESs) are a class of sensors that use light to activate an electrochemical reaction on the surface of a…”
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Identification of the perchlorate parent salts at the Phoenix Mars landing site and possible implications
Published in Icarus (New York, N.Y. 1962) (01-04-2014)“…•New analyses of Phoenix data identifies dominant perchlorate salt as calcium-perchlorate.•Results suggest that Ca(ClO4)2 in soil has rarely, if ever, been in…”
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Solid Contact Ion-Selective Electrodes for in Situ Measurements at High Pressure
Published in Analytical chemistry (Washington) (02-05-2017)“…Solid contact polymeric ion-selective electrodes (SC-ISEs) have been fabricated using microporous carbon (μPC) as the ion-to-electron transducer, loaded with a…”
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Scanning Line Probe Microscopy: Beyond the Point Probe
Published in Analytical chemistry (Washington) (02-10-2018)“…Scanning probe microscopy (SPM) techniques have become indispensable tools for studying nano- and microscale materials and processes but suffer from a…”
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Electrochemical X‑ray Fluorescence Spectroscopy for Trace Heavy Metal Analysis: Enhancing X‑ray Fluorescence Detection Capabilities by Four Orders of Magnitude
Published in Analytical chemistry (Washington) (06-05-2014)“…The development of a novel analytical technique, electrochemical X-ray fluorescence (EC-XRF), is described and applied to the quantitative detection of heavy…”
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Electrochemistry of Aqueous Colloidal Graphene Oxide on Pt Electrodes
Published in Langmuir (12-08-2014)“…The electrochemical behavior of colloidal solutions of graphene oxide (GO) is described here in detail. The GO reduction is shown to exhibit near-reversible…”
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Stability and Lifetime of Potassium Solid-Contact Ion Selective Electrodes for Continuous and Autonomous Measurements
Published in Electroanalysis (New York, N.Y.) (01-11-2012)“…The current generation of solid‐contact ion‐selective electrodes (SC‐ISE) suffer from lack of stability and lifetime. When using such sensors for remote,…”
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Carbon-Nanofiber-Based Nanocomposite Membrane as a Highly Stable Solid-State Junction for Reference Electrodes
Published in Analytical chemistry (Washington) (15-07-2011)“…There is currently a need for a reliable solid-state reference electrode, especially in applications such as autonomous sensing or long-term environmental…”
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Toward single-step production of functional electrochemical devices using 3D printing: Progress, challenges, and opportunities
Published in Current opinion in electrochemistry (01-04-2020)“…Sensors and devices that incorporate 3D printed components have gained significant attention because they are easily customized and rapidly prototyped, can…”
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The use of graphene oxide as a fixed charge carrier in ion-selective electrodes
Published in Electrochemistry communications (01-06-2015)“…Here we present for the first time the use of graphene oxide nanoparticles as fixed-charge carriers for the development of membrane-based cation selective…”
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Development of Carbon Nanomaterial-Based Sensors for Applications in a Microfluidic Total Analysis System
Published 01-01-2014“…The continued understanding of the geochemistry of extreme environments requires tools that are able to deliver high-quality measurements. Ion-selective…”
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Dissertation -
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Development of Carbon Nanomaterial-Based Sensors for Applications in a Microfluidic Total Analysis System
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Dissertation