Enhancing the properties of bone China ceramics by treatment with microporous SiO2 nanoparticles

In this study, microporous silicon dioxide nanoparticles (SiO 2 –NPs) were used to improve the physical, chemical, and mechanical properties of bone China ceramics. Microporous SiO 2 –NPs were prepared economically from sodium metasilicate (SMS) as a precursor with cetyltrimethylammonium bromide (CT...

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Bibliographic Details
Published in:Chemical papers Vol. 76; no. 9; pp. 5879 - 5891
Main Authors: Abou Elmaaty, Tarek M., Sayed-Ahmed, Khaled, El Gohari, Mohamed M., Noaman, Rokaya
Format: Journal Article
Language:English
Published: Warsaw Versita 01-09-2022
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Summary:In this study, microporous silicon dioxide nanoparticles (SiO 2 –NPs) were used to improve the physical, chemical, and mechanical properties of bone China ceramics. Microporous SiO 2 –NPs were prepared economically from sodium metasilicate (SMS) as a precursor with cetyltrimethylammonium bromide (CTAB) as a surfactant at different concentrations. The prepared SiO 2 –NPs were characterized using scanning electron microscopy, transmission electron microscopy, X-ray diffraction, and Raman spectroscopy to confirm the formation of microporous SiO 2 –NPs. The optimum concentrations of the precursor and surfactant used in the SiO 2 –NPs synthesis were set to be 1.5% and 2 g/200 ml, with a size range of 7–96 nm. SiO 2 –NPs prepared at the optimum concentrations were incorporated into bone China at different concentrations to evaluate their effect on flexural strength and elasticity. The bone China prepared using 1% SiO 2 –NPs (B 1 ) had the highest flexural strength and Young's modulus values. Sample characteristics, including self-cleaning, differential scanning calorimetry, thermogravimetric analysis, bulk density (BD), apparent porosity (AP), and water absorption (WA), were investigated. The results revealed outstanding characteristic such as self-cleaning ability, remarkable increase in AP and WA, and a decrease in BD.
ISSN:0366-6352
1336-9075
2585-7290
DOI:10.1007/s11696-022-02296-9