Enhancing the properties of bone China ceramics by treatment with microporous SiO2 nanoparticles
In this study, microporous silicon dioxide nanoparticles (SiO 2 –NPs) were used to improve the physical, chemical, and mechanical properties of bone China ceramics. Microporous SiO 2 –NPs were prepared economically from sodium metasilicate (SMS) as a precursor with cetyltrimethylammonium bromide (CT...
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Published in: | Chemical papers Vol. 76; no. 9; pp. 5879 - 5891 |
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Main Authors: | , , , |
Format: | Journal Article |
Language: | English |
Published: |
Warsaw
Versita
01-09-2022
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Subjects: | |
Online Access: | Get full text |
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Summary: | In this study, microporous silicon dioxide nanoparticles (SiO
2
–NPs) were used to improve the physical, chemical, and mechanical properties of bone China ceramics. Microporous SiO
2
–NPs were prepared economically from sodium metasilicate (SMS) as a precursor with cetyltrimethylammonium bromide (CTAB) as a surfactant at different concentrations. The prepared SiO
2
–NPs were characterized using scanning electron microscopy, transmission electron microscopy, X-ray diffraction, and Raman spectroscopy to confirm the formation of microporous SiO
2
–NPs. The optimum concentrations of the precursor and surfactant used in the SiO
2
–NPs synthesis were set to be 1.5% and 2 g/200 ml, with a size range of 7–96 nm. SiO
2
–NPs prepared at the optimum concentrations were incorporated into bone China at different concentrations to evaluate their effect on flexural strength and elasticity. The bone China prepared using 1% SiO
2
–NPs (B
1
) had the highest flexural strength and Young's modulus values. Sample characteristics, including self-cleaning, differential scanning calorimetry, thermogravimetric analysis, bulk density (BD), apparent porosity (AP), and water absorption (WA), were investigated. The results revealed outstanding characteristic such as self-cleaning ability, remarkable increase in AP and WA, and a decrease in BD. |
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ISSN: | 0366-6352 1336-9075 2585-7290 |
DOI: | 10.1007/s11696-022-02296-9 |