Search Results - "Neue, Uwe D"
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1
Theory of peak capacity in gradient elution
Published in Journal of Chromatography A (24-06-2005)“…Peak capacity is the best measure of the performance of a gradient separation. In this paper, the theory of peak capacity for the standard operating conditions…”
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2
Investigation of the effect of pressure on retention of small molecules using reversed-phase ultra-high-pressure liquid chromatography
Published in Journal of Chromatography A (31-10-2008)“…The effect of inlet pressure on the retention of a series of low molecular weight acids, bases and neutrals, was investigated at constant temperature in…”
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3
Further investigations of the effect of pressure on retention in ultra-high-pressure liquid chromatography
Published in Journal of Chromatography A (15-01-2010)“…In this study, we investigated further the large increases in retention with pressure that we observed previously in RP-LC especially for ionised solutes…”
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4
Comparison of the acidity of residual silanol groups in several liquid chromatography columns
Published in Journal of Chromatography A (31-01-2003)“…The silanol acidity of Waters Resolve C 18, Waters Resolve silica, Waters Symmetry C 18, Waters Symmetry silica, Waters XTerra MS C 18 and underivatized XTerra…”
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5
Implications of column peak capacity on the separation of complex peptide mixtures in single- and two-dimensional high-performance liquid chromatography
Published in Journal of Chromatography A (24-12-2004)“…Column peak capacity was utilized as a measure of column efficiency for gradient elution conditions. Peak capacity was evaluated experimentally for…”
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6
The combined effect of silanols and the reversed-phase ligand on the retention of positively charged analytes
Published in Journal of Chromatography A (21-01-2005)“…The nature of the interaction of positively charged analytes with the surface of reversed-phase bonded phases has been investigated as a function of both pH…”
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7
Characterization of HPLC packings
Published in Journal of separation science (01-03-2003)“…Several chromatographic test procedures are in use for the characterization of commercially available packings. The results of the test procedure used in our…”
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8
Estimation of the extent of the water-rich layer associated with the silica surface in hydrophilic interaction chromatography
Published in Journal of Chromatography A (30-05-2008)“…The possible presence of a mobile phase layer rich in water on the surface of silica columns used under conditions typical in hydrophilic interaction…”
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9
Effects of extra-column band spreading, liquid chromatography system operating pressure, and column temperature on the performance of sub-2-μm porous particles
Published in Journal of Chromatography A (07-08-2009)“…The effects of extra-column band spreading, LC system operating pressure, and separation temperature were investigated for sub-2-μm particle columns using both…”
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10
Peak capacity in gradient reversed-phase liquid chromatography of biopolymers Theoretical and practical implications for the separation of oligonucleotides
Published in Journal of chromatography (26-10-2007)“…Reversed-phase ultra-performance liquid chromatography was used for biopolymer separations in isocratic and gradient mode. The gradient elution mode was…”
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11
Performance of idealized column structures under high pressure
Published in Journal of Chromatography A (18-05-2007)“…We have examined the influence of the longitudinal temperature and pressure gradients in columns operated under very high pressures on the coefficients of the…”
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12
Selectivity in reversed-phase separations influence of the stationary phase
Published in Journal of chromatography (15-09-2006)“…The selectivity difference between 15 different stationary phases was measured using a large number of analytes at 2 or 3 different pH values (3, 7 and 10)…”
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13
Stationary phase characterization and method development
Published in Journal of separation science (01-07-2007)“…The properties of stationary phases and their characterization methods are reviewed. New and significant developments have occurred in the last few years, and…”
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14
Comment on “Submicrometer Plate Heights for Capillaries Packed with Silica Colloidal Crystals”
Published in Analytical chemistry (Washington) (01-01-2011)Get full text
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15
application of novel 1.7 μm ethylene bridged hybrid particles for hydrophilic interaction chromatography
Published in Journal of separation science (01-05-2008)“…An un-derivatized 1.7 μm ethylene bridged hybrid (BEH) particle was evaluated for its utility in retaining polar species in hydrophilic interaction…”
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16
Peak compression in reversed-phase gradient elution
Published in Journal of Chromatography A (07-04-2006)“…Previous reports suggest that peak widths in linear gradient elution are consistently larger than predicted by theory; however, if gradient compression is…”
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17
Selectivity in reversed-phase separations: General influence of solvent type and mobile phase pH
Published in Journal of separation science (01-05-2007)“…The influence of the mobile phase on retention is studied in this paper for a group of over 70 compounds with a broad range of multiple functional groups. We…”
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18
The determination of the plate count for large molecules under reversed-phase gradient conditions
Published in Journal of Chromatography A (02-04-2010)“…The true performance of HPLC columns in the gradient separation of macromolecules can be assessed by measuring the true plate count, if we know the retention…”
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19
Ion-pair reversed-phase high-performance liquid chromatography analysis of oligonucleotides:: Retention prediction
Published in Journal of Chromatography A (07-06-2002)“…An ion-pair reversed-phase HPLC method was evaluated for the separation of synthetic oligonucleotides. Mass transfer in the stationary phase was found to be a…”
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20
The application of small porous particles, high temperatures, and high pressures to generate very high resolution LC and LC/MS separations
Published in Journal of separation science (01-05-2007)“…The effect of combining sub‐2 μm porous particles with elevated operating temperatures on chromatographic performance has been investigated in terms of…”
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