Search Results - "Mikina, Maciej"
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Modulation of Properties in [1]Benzothieno[3,2- b ][1]benzothiophene Derivatives through Sulfur Oxidation
Published in Molecules (Basel, Switzerland) (01-08-2024)“…This study explores the impact of sulfur oxidation on the structural, optical, and electronic properties of [1]benzothieno[3,2- ][1]benzothiophene ( )…”
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A novel route to a chiral building block for the preparation of cyclopentenyl carbocyclic nucleosides. Synthesis and anticancer activity of enantiomeric neplanocins A
Published in RSC advances (27-08-2020)“…The synthesis of both enantiomers of 3-[( tert -butyldimethylsilyl)oxy]methyl-4,5- O -isopropylidenecyclopent-2-en-1-ol was accomplished in six steps based on…”
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3
Hetero-Diels-Alder reactions of hetaryl and aryl thioketones with acetylenic dienophiles
Published in Beilstein journal of organic chemistry (28-04-2015)“…Selected hetaryl and aryl thioketones react with acetylenecarboxylates under thermal conditions in the presence of LiClO4 or, alternatively, under…”
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Modulation of Properties in 1Benzothieno3,2-b1benzothiophene Derivatives through Sulfur Oxidation
Published in Molecules (Basel, Switzerland) (29-07-2024)“…This study explores the impact of sulfur oxidation on the structural, optical, and electronic properties of [1]benzothieno[3,2-b][1]benzothiophene (BTBT)…”
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5
The First Observation of [gamma]-Sila-Pummerer Rearrangement
Published in Phosphorus, sulfur, and silicon and the related elements (01-04-2013)“…2-Sulfinyl-3-trimethylsilylmethylcycloalkanones unexpectedly undergo γ-sila-Pummerer rearrangement. The first examples of this new type of rearrangement are…”
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The First Observation of γ-Sila-Pummerer Rearrangement
Published in Phosphorus, sulfur, and silicon and the related elements (01-04-2013)“…2-Sulfinyl-3-trimethylsilylmethylcycloalkanones unexpectedly undergo γ-sila-Pummerer rearrangement. The first examples of this new type of rearrangement are…”
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7
Asymmetric synthesis of a cyclopropanecarboxylic acid derivative - the potential agonist/antagonist of GABA receptors
Published in Phosphorus, sulfur, and silicon and the related elements (22-06-2022)“…The synthesis of enantiomerically pure (1S,2S,S P )-1-[hydroxy(methyl)phosphonyl]-2-aminocyclopropanecarboxylic acid (1) (a potential agonist/antagonist of…”
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The sila-Pummerer reaction of γ-silyl substituted cycloalkanoyl sulfoxides: the first examples and a new approach to 3-substituted cycloalk-2-enones
Published in Tetrahedron letters (16-07-2014)“…The thermal decomposition of 3-(α-trimethylsilyl)alkyl substituted 2-(phenylsulfinyl)cycloalkanones occurs via the γ-sila-Pummerer reaction, affording…”
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Stereocontrolled synthesis of enantiopure anticancer cyclopentenone prostaglandin analogues: (−)- and (+)-TEI-9826
Published in Tetrahedron: asymmetry (08-12-2010)“…The synthesis of both enantiomers of TEI-9826 has been accomplished in seven steps with an overall yield of 44% starting from diastereomeric camphor protected…”
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Synthesis of polyamino nitriles, en route to acylpolyamine neurotoxins, via the regioselective michael cyanoethylation of unprotected polyamines. Unusual behaviour of 1-(2-aminoethyl)piperazine
Published in Tetrahedron (17-10-2009)“…The Michael cyanoethylation of 1-(2-aminoethyl)piperazine, 4,4′-methylenebis(cyclohexylamine) and bis(3-aminopropylamine)amine, leading to acrylonitrile free…”
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A Novel Synthesis of Racemic and Enantiomeric Forms of Prostaglandin B 1 Methyl Ester
Published in Journal of organic chemistry (25-08-2000)Get full text
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A Novel Synthesis of Racemic and Enantiomeric Forms of Prostaglandin B1 Methyl Ester
Published in Journal of organic chemistry (25-08-2000)“…3-(Dimethoxyphosphorylmethyl)cyclopent-2-enone was converted into (±)-prostaglandin B1 methyl ester in two steps involving regioselective alkylation at C(2)…”
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Horner Olefination Reaction in Organic Sulfur Chemistry and Synthesis of Natural and Bioactive Products
Published in Phosphorus, sulfur, and silicon and the related elements (01-02-2008)“…This article outlines the results of our work on the application of the Horner olefination reaction for the synthesis of unsaturated sulfur compounds. A…”
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A general approach to 3-phosphorylmethyl cycloalkenones by intramolecular Horner-Wittig reaction of bis-.beta.-ketophosphonates
Published in Journal of organic chemistry (01-11-1994)Get full text
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