Helium microwave induced plasma atomic emission detection for liquid chromatography utilizing a moving band interface

Helium microwave induced plasma atomic emission detection for liquid chromatography utilizing a moving band interface

A moving band interface is used to separate HPLC solvent from analyte before introduction into a microwave-induced plasma atomic emission detector. Spectral scans indicate that all detectable solvent is removed prior to analyte introduction.

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Bibliographic Details
Published in:Analytical chemistry (Washington) Vol. 65; no. 19; pp. 2596 - 2600
Main Authors: Mason, Peter B, Zhang, Liming, Carnahan, Jon W, Winans, Randall E
Format: Journal Article
Language:English
Published: Washington, DC American Chemical Society 01-10-1993
Subjects:
400100 - Analytical & Separations Chemistry
400201 - Chemical & Physicochemical Properties
Analytical chemistry
AROMATICS
BOILING POINTS
Chemistry
CHLORINATED AROMATIC HYDROCARBONS
Chromatographic methods and physical methods associated with chromatography
CHROMATOGRAPHY
DETECTION
ELEMENTS
EMISSION SPECTRA
EVAPORATION
Exact sciences and technology
FLUIDS
GASES
HALOGENATED AROMATIC HYDROCARBONS
HEATING
HELIUM
INORGANIC, ORGANIC, PHYSICAL AND ANALYTICAL CHEMISTRY
INTERFACES
LIQUID COLUMN CHROMATOGRAPHY
MICROWAVE HEATING
NONMETALS
ORGANIC CHLORINE COMPOUNDS
ORGANIC COMPOUNDS
ORGANIC HALOGEN COMPOUNDS
Other chromatographic methods
PHASE TRANSFORMATIONS
PHYSICAL PROPERTIES
PLASMA HEATING
RARE GASES
SEPARATION PROCESSES
SOLVENTS
SPECTRA
THERMODYNAMIC PROPERTIES
TRANSITION TEMPERATURE
Emission spectrometry
Chlorine
Inductive discharge
Chlorine Organic compounds
Chlorocarbon
Detection limit
HPLC chromatography
Liquid chromatography
Microwave discharge
Interface
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Description
Summary:A moving band interface is used to separate HPLC solvent from analyte before introduction into a microwave-induced plasma atomic emission detector. Spectral scans indicate that all detectable solvent is removed prior to analyte introduction.
Bibliography:istex:7451E7FF6CF5888EEDC2520A161E752B8C3608A4
ark:/67375/TPS-NW0CRSF2-5
W-31109-ENG-38
ISSN:0003-2700
1520-6882
DOI:10.1021/ac00067a009