Search Results - "Marcé, R.M."
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Efficient tandem solid-phase extraction and liquid chromatography-triple quadrupole mass spectrometry method to determine polar benzotriazole, benzothiazole and benzenesulfonamide contaminants in environmental water samples
Published in Journal of Chromatography A (27-09-2013)“…•Simultaneous determination of benzotriazoles, benzothiazoles and benzenesulfonamides.•Separation of both tolyltriazole and toluenesulfonamide isomers were…”
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Molecularly-imprinted polymers: useful sorbents for selective extractions
Published in TrAC, Trends in analytical chemistry (Regular ed.) (01-12-2010)“…We review and discuss the most common protocols for synthesizing molecularly-imprinted polymers (MIPs), highlighting their main advantages and drawbacks. We…”
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3
Determination of glucocorticoids in sewage and river waters by ultra-high performance liquid chromatography–tandem mass spectrometry
Published in Journal of Chromatography A (10-02-2012)“…► UHPLC–MS/MS method for determining nine glucocorticoids in environmental waters. ► We obtained limits of detection and quantification at low ng/L levels. ►…”
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4
New materials in sorptive extraction techniques for polar compounds
Published in Journal of Chromatography A (08-06-2007)“…This paper provides an overview of the new developments in material and format technology that improve the extraction of polar compounds in several extraction…”
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Synthesis by precipitation polymerisation of molecularly imprinted polymer microspheres for the selective extraction of carbamazepine and oxcarbazepine from human urine
Published in Journal of Chromatography A (20-03-2009)“…Two molecularly imprinted polymers (MIPs), in the physical form of well-defined polymer microspheres, were synthesised via precipitation polymerisation (PP)…”
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Determination of N-nitrosamines and nicotine in air particulate matter samples by pressurised liquid extraction and gas chromatography-ion trap tandem mass spectrometry
Published in Talanta (Oxford) (15-10-2013)“…N-nitrosamines are potentially hazardous pollutants, classified as probable carcinogenic and mutagenic by the U.S. Environmental Protection Agency (EPA). In…”
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New hydrophilic materials for solid-phase extraction
Published in TrAC, Trends in analytical chemistry (Regular ed.) (01-05-2005)“…Solid-phase extraction (SPE) is increasingly being used as a sample-pre-treatment technique to cover a wide range of analytes, including the most polar. This…”
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Thermal desorption-gas chromatography–mass spectrometry method to determine phthalate and organophosphate esters from air samples
Published in Journal of Chromatography A (16-08-2013)“…•Efficient method for determining phthalate and organophosphate esters in gas phase.•These compounds are for the first time determined in gas phase from…”
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Journal Article Conference Proceeding -
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Hydrophilic hypercrosslinked polymeric sorbents for the solid-phase extraction of polar contaminants from water
Published in Journal of Chromatography A (07-05-2010)“…Three new hypercrosslinked polymers with hydrophilic character arising from hydroxyl moieties in their skeletons have been prepared in microsphere format and…”
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Journal Article Conference Proceeding -
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Preparation of a polar monolithic stir bar based on methacrylic acid and divinylbenzene for the sorptive extraction of polar pharmaceuticals from complex water samples
Published in Journal of Chromatography A (17-02-2012)“…► We prepared a new polar monolithic coating based on poly(MAA-co-DVB) for SBSE. ► The new coating was applied for the SBSE of polar analytes from water…”
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Determination of polyether ionophores in urban sewage sludge by pressurised liquid extraction and liquid chromatography–tandem mass spectrometry: Study of different clean-up strategies
Published in Journal of Chromatography A (12-04-2013)“…► Several clean-up strategies to reduce the matrix effect in sewage sludge extracts were studied. ► Pressurised liquid extraction provides recoveries up to 90%…”
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12
Synthesis and application of hypercrosslinked polymers with weak cation-exchange character for the selective extraction of basic pharmaceuticals from complex environmental water samples
Published in Journal of Chromatography A (05-03-2010)“…The synthesis of high specific surface area sorbents (HXLPP-WCX) in the form of hypercrosslinked polymer microspheres with narrow particle size distributions,…”
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Novel amide polar-embedded reversed-phase column for the fast liquid chromatography–tandem mass spectrometry method to determine polyether ionophores in environmental waters
Published in Journal of Chromatography A (09-11-2012)“…► Fast LC–MS/MS method to determine five polyether ionophores in environmental waters. ► SPE procedure developed provides recoveries close to 90% for all…”
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Synthesis and application of a carbamazepine-imprinted polymer for solid-phase extraction from urine and wastewater
Published in Analytica chimica acta (30-07-2007)“…A molecularly imprinted polymer (MIP) designed to enable the selective extraction of carbamazepine (CBZ) from effluent wastewater and urine samples has been…”
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Solid-phase microextraction coupled to high-performance liquid chromatography to determine phenolic compounds in water samples
Published in Journal of Chromatography A (12-04-2002)“…Solid-phase microextraction (SPME) coupled to high-performance liquid chromatography (HPLC) with ultraviolet (UV) and electrochemical detection (ED) has been…”
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Comparison of different fibers for the solid-phase microextraction of phthalate esters from water
Published in Journal of Chromatography A (13-07-2001)“…Solid-phase microextraction (SPME) coupled to gas chromatography–mass spectrometry (GC–MS) has been applied to determine six phthalate esters and one adipate…”
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New polymeric and other types of sorbents for solid-phase extraction of polar organic micropollutants from environmental water
Published in TrAC, Trends in analytical chemistry (Regular ed.) (01-06-1998)“…This article describes different types of sorbents for the solid-phase extraction of polar organic pollutants from environmental water and emphasizes the use…”
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Stir bar sorptive extraction and large volume injection gas chromatography to determine a group of endocrine disrupters in water samples
Published in Journal of Chromatography A (25-07-2003)“…Stir bar sorptive extraction (SBSE) combined with gas chromatography (GC) with mass spectrometric detection (MS) has been applied to determine a group of…”
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Application of on-line solid-phase extraction–gas chromatography–mass spectrometry to the determination of endocrine disruptors in water samples
Published in Journal of Chromatography A (19-07-2002)“…We have applied a method based on solid-phase extraction (SPE), on-line coupled to gas chromatography–mass spectrometry through an on-column interface, to…”
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Journal Article Conference Proceeding -
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Comparison of different sorbents for on-line solid-phase extraction of pesticides and phenolic compounds from natural water followed by liquid chromatography
Published in Journal of Chromatography A (01-01-1998)“…Three different sorbents, Carbopack B, a carbon black, Bond Elut PPL, a functionalized polymeric resin, and HYSphere-1, a higher cross-linking polymeric resin,…”
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