Search Results - "Machado De Carvalho, Leandro"
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Determination of phenolic and triterpenic compounds in Jatropha gossypiifolia L by Ultra-high performance liquid chromatography-tandem mass spectrometric (UHPLC-MS/MS)
Published in Brazilian Journal of Pharmaceutical Sciences (01-01-2020)“…This work describes the chemical characterization of extracts of Jatropha gossypiifolia (from Amazonia region) concerning the presence of phenolic and…”
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Pulsed voltammetric/amperometric detection of polycyclic aromatic sulfur heterocycles (PASHs) at the gold disc electrode for studies in petroleum asphalts
Published in Journal of solid state electrochemistry (01-11-2020)“…This work describes the voltammetric and amperometric behavior of a high number of PASHs (sulfides, thiophenes, benzothiophenes, dibenzothiophenes,…”
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3
Regulatory framework for dietary supplements and the public health challenge
Published in Revista de saúde pública (01-01-2019)“…The new regulatory framework for dietary supplements in Brazil prompted this analysis of the current outlook of these products and the challenges posed by the…”
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4
Indirect Electrochemical Sensing of Radicals and Radical Scavengers in Biological Matrices
Published in Angewandte Chemie (International ed.) (01-01-2007)“…Breaking cover: Hydroxyl radicals OH. destroy the self‐assembled monolayer (SAM) of hexanethiol on gold and mercury electrodes and thus allow the…”
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Electrochemical Assay to Quantify the Hydroxyl Radical Scavenging Activity of Medicinal Plant Extracts
Published in Electroanalysis (New York, N.Y.) (01-02-2010)“…A new electrochemical assay has been developed which is based on quantifying the attack of OH. radicals on a self‐assembled thiol monolayer on electrodes in…”
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Simultaneous determination of Ba, Co, Fe, and Ni in nuts by high-resolution continuum source atomic absorption spectrometry after extraction induced by solid-oil-water emulsion breaking
Published in Food chemistry (30-05-2021)“…[Display omitted] •A simple, low-cost and fast extraction method was developed;•Extraction of Ba, Co, Fe and Ni was achieved by breaking a solid-oil-water…”
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A new method based on extraction induced by emulsion breaking for determination of Co and Ni in chocolate bars by graphite furnace atomic absorption spectrometry
Published in Food chemistry (01-08-2024)“…This paper describes a new experimental configuration of extraction induced by emulsion breaking method to extract and determine Ni and Co in chocolate bars by…”
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Extraction induced by emulsion breaking for simultaneous determination of Co, Fe and Ni in petroleum asphalt cement by high-resolution continuum source atomic absorption spectrometry
Published in Fuel (Guildford) (01-10-2020)“…[Display omitted] •New extraction method for Co, Fe and Ni determination in asphalt is proposed.•Method simpler and faster than methods of total digestion of…”
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9
Diagnóstico de emissões de poluentes atmosféricos na produção de misturas asfálticas
Published in Transportes (Rio de Janeiro) (11-12-2023)“…Os pavimentos asfálticos são comumente utilizados em grandes centros urbanos no Brasil. No entanto, vários contaminantes do ar são emitidos durante o ciclo de…”
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10
Extraction induced by emulsion breaking to assay Cr, Cu and Mn in asphalt samples by high-resolution continuum source atomic absorption spectrometry and its comparison with other sample preparation methods
Published in Talanta (Oxford) (01-11-2021)“…This paper reports the development of a method based on the extraction induced by emulsion breaking (EIEB) for the determination of Cr, Cu and Mn in asphalt by…”
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11
A liquid chromatography-atmospheric pressure photoionization tandem mass spectrometric (LC-APPI-MS/MS) method for the determination of triterpenoids in medicinal plant extracts
Published in Journal of mass spectrometry. (01-08-2016)“…An analytical method using liquid chromatography‐atmospheric pressure photoionization tandem mass spectrometry with toluene as a dopant was developed for the…”
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12
Distribution of metals in different environmental compartments and oxidative stress biomarkers in Bryconops caudomaculatus (Osteichthyes: Characiformes) from a bauxite mining area in the Eastern Amazon
Published in Environmental research (01-01-2023)“…The Eastern Amazon is rich in bauxite ore. The extraction and processing of bauxite lead to the mobilization of Aluminum (Al) and other metals in…”
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13
Evaluation of aging processes of petroleum asphalt cements by solid state electrochemical monitoring
Published in Electrochimica acta (20-04-2018)“…The changes in the chemistry of organosulfur compounds from asphalt cements during aging are studied using solid state voltammetry of immobilized…”
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14
Silver nano/microparticle toxicity in the shrimp Litopenaeus vannamei (Boone, 1931)
Published in Comparative biochemistry and physiology. Toxicology & pharmacology (01-02-2023)“…The effects of silver nano/microparticles (AgP) on juvenile Litopenaeus vannamei shrimp were evaluated through several responses, aiming to use it as a…”
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Elemental Analysis of Pharmaceutical Products for Chronic Kidney Disease by High-Resolution Continuum Source Graphite Furnace Atomic Absorption Spectrometry (HR-CS GFAAS)
Published in Analytical letters (02-01-2022)“…Here is reported the development of methods for the determination of Al, Cd, Cu, Mo, and Pb by high-resolution continuum source graphite furnace atomic…”
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16
A cleanup method using solid phase extraction for the determination of organosulfur compounds in petroleum asphalt cements
Published in Fuel (Guildford) (15-08-2017)“…[Display omitted] •Cleanup method for the determination of model organosulfur compounds in asphalt cements.•Use of a commercially available aminopropyl…”
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17
Screening of pharmacologic adulterant classes in herbal formulations using voltammetry of microparticles
Published in Journal of pharmaceutical and biomedical analysis (23-02-2013)“…[Display omitted] ► Screening of different families of adulterants is obtained by voltammetry of microparticles. ► Application to identify synthetic…”
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Analysis of Pharmacologic Adulteration in Dietary Supplements by Capillary Zone Electrophoresis Using Simultaneous Contactless Conductivity and UV Detection
Published in Chromatographia (01-04-2018)“…The consumption of dietary supplements is increasing every year all over the world. In addition, the consumption has been accompanied by the increased…”
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Reversed-Phase High-Performance Liquid Chromatography for the Determination of 15 Rare Earth Elements in Surface Water Sample Collected in a Mining Area from Lavras do Sul/RS, Brazil
Published in Chromatographia (01-05-2019)“…A methodology was developed to assay 15 rare earth elements (REE) (La to Lu and Y) in a surface water sample from a mining area. The samples were collected in…”
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Determination of Rare Earth Elements in Natural Water Samples by Rapid Sequential High-Resolution Continuum Source Flame Atomic Absorption Spectrometry (HR CS FAAS) and inductively Coupled Plasma-Mass Spectrometry (ICP-MS)
Published in Analytical letters (02-09-2019)“…A method was developed to sequentially assay ten rare earth elements by high-resolution continuum source flame atomic absorption spectrometry. The rare earth…”
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