Search Results - "MARCE, R. M"
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Efficient tandem solid-phase extraction and liquid chromatography-triple quadrupole mass spectrometry method to determine polar benzotriazole, benzothiazole and benzenesulfonamide contaminants in environmental water samples
Published in Journal of Chromatography A (27-09-2013)“…•Simultaneous determination of benzotriazoles, benzothiazoles and benzenesulfonamides.•Separation of both tolyltriazole and toluenesulfonamide isomers were…”
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Molecularly-imprinted polymers: useful sorbents for selective extractions
Published in TrAC, Trends in analytical chemistry (Regular ed.) (01-12-2010)“…We review and discuss the most common protocols for synthesizing molecularly-imprinted polymers (MIPs), highlighting their main advantages and drawbacks. We…”
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3
A pressurised hot water extraction and liquid chromatography–high resolution mass spectrometry method to determine polar benzotriazole, benzothiazole and benzenesulfonamide derivates in sewage sludge
Published in Journal of Chromatography A (15-08-2014)“…•A pressurised hot water extraction method was developed for the analysis of sludge samples.•Simultaneous determination of benzotriazoles, benzothiazoles and…”
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4
Development and application of a polar coating for stir bar sorptive extraction of emerging pollutants from environmental water samples
Published in Analytica chimica acta (07-11-2011)“…[Display omitted] ► We prepare a new polar monolithic coating for stir bar sorptive extraction (SBSE). ► The new coating is successfully apply for SBSE polar…”
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5
Determination of glucocorticoids in sewage and river waters by ultra-high performance liquid chromatography–tandem mass spectrometry
Published in Journal of Chromatography A (10-02-2012)“…► UHPLC–MS/MS method for determining nine glucocorticoids in environmental waters. ► We obtained limits of detection and quantification at low ng/L levels. ►…”
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Determination of N-nitrosamines and nicotine in air particulate matter samples by pressurised liquid extraction and gas chromatography-ion trap tandem mass spectrometry
Published in Talanta (Oxford) (15-10-2013)“…N-nitrosamines are potentially hazardous pollutants, classified as probable carcinogenic and mutagenic by the U.S. Environmental Protection Agency (EPA). In…”
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Thermal desorption-gas chromatography–mass spectrometry method to determine phthalate and organophosphate esters from air samples
Published in Journal of Chromatography A (16-08-2013)“…•Efficient method for determining phthalate and organophosphate esters in gas phase.•These compounds are for the first time determined in gas phase from…”
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Journal Article Conference Proceeding -
8
Determination of phthalates and organophosphate esters in particulated material from harbour air samples by pressurised liquid extraction and gas chromatography–mass spectrometry
Published in Talanta (Oxford) (15-11-2012)“…A method based on gas chromatography–mass spectrometry (GC–MS) combined with a pressurised liquid extraction (PLE) to determine four organophosphates, seven…”
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Comparison of triple quadrupole mass spectrometry and Orbitrap high-resolution mass spectrometry in ultrahigh performance liquid chromatography for the determination of veterinary drugs in sewage: benefits and drawbacks
Published in Journal of mass spectrometry. (01-07-2014)“…This paper presents a comparison of triple quadrupole tandem mass spectrometry (MS/MS) and Orbitrap high‐resolution mass spectrometry (HRMS) combined to…”
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Hydrophilic hypercrosslinked polymeric sorbents for the solid-phase extraction of polar contaminants from water
Published in Journal of Chromatography A (07-05-2010)“…Three new hypercrosslinked polymers with hydrophilic character arising from hydroxyl moieties in their skeletons have been prepared in microsphere format and…”
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Journal Article Conference Proceeding -
11
Synthesis by precipitation polymerisation of molecularly imprinted polymer microspheres for the selective extraction of carbamazepine and oxcarbazepine from human urine
Published in Journal of Chromatography A (20-03-2009)“…Two molecularly imprinted polymers (MIPs), in the physical form of well-defined polymer microspheres, were synthesised via precipitation polymerisation (PP)…”
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12
Determination of polyether ionophores in urban sewage sludge by pressurised liquid extraction and liquid chromatography–tandem mass spectrometry: Study of different clean-up strategies
Published in Journal of Chromatography A (12-04-2013)“…► Several clean-up strategies to reduce the matrix effect in sewage sludge extracts were studied. ► Pressurised liquid extraction provides recoveries up to 90%…”
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13
Synthesis and application of hypercrosslinked polymers with weak cation-exchange character for the selective extraction of basic pharmaceuticals from complex environmental water samples
Published in Journal of Chromatography A (05-03-2010)“…The synthesis of high specific surface area sorbents (HXLPP-WCX) in the form of hypercrosslinked polymer microspheres with narrow particle size distributions,…”
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Synthetic approaches to parabens molecularly imprinted polymers and their applications to the solid-phase extraction of river water samples
Published in Analytica chimica acta (10-09-2010)“…In this paper we describe the synthesis, characterisation and use of two distinct molecularly imprinted polymers (MIPs) prepared using esters of…”
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Journal Article Conference Proceeding -
15
Synthesis and application of a carbamazepine-imprinted polymer for solid-phase extraction from urine and wastewater
Published in Analytica chimica acta (30-07-2007)“…A molecularly imprinted polymer (MIP) designed to enable the selective extraction of carbamazepine (CBZ) from effluent wastewater and urine samples has been…”
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Preparation of a polar monolithic stir bar based on methacrylic acid and divinylbenzene for the sorptive extraction of polar pharmaceuticals from complex water samples
Published in Journal of Chromatography A (17-02-2012)“…► We prepared a new polar monolithic coating based on poly(MAA-co-DVB) for SBSE. ► The new coating was applied for the SBSE of polar analytes from water…”
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Solid-phase microextraction coupled to high-performance liquid chromatography to determine phenolic compounds in water samples
Published in Journal of Chromatography A (12-04-2002)“…Solid-phase microextraction (SPME) coupled to high-performance liquid chromatography (HPLC) with ultraviolet (UV) and electrochemical detection (ED) has been…”
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Molecularly imprinted polymer with high-fidelity binding sites for the selective extraction of barbiturates from human urine
Published in Journal of Chromatography A (22-07-2011)“…In this paper we describe the synthesis of a molecularly imprinted polymer (MIP) by precipitation polymerisation, with barbital as the template molecule, and…”
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19
Method based on solid-phase microextraction–high-performance liquid chromatography with UV and electrochemical detection to determine estrogenic compounds in water samples
Published in Journal of Chromatography A (26-07-2002)“…We determined a group of estrogenic compounds by solid-phase microextraction (SPME) coupled to high-performance liquid chromatography (HPLC) with both…”
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Application of molecularly imprinted polymers to solid-phase extraction of compounds from environmental and biological samples
Published in TrAC, Trends in analytical chemistry (Regular ed.) (01-02-2006)“…In this paper, we review the current state of the art in the use of molecularly imprinted polymers (MIPs) as selective materials in molecularly imprinted…”
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