Search Results - "MANS, Daniel J"
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Quality Assessment of U.S. Marketplace Vancomycin for Injection Products Using High-Resolution Liquid Chromatography-Mass Spectrometry and Potency Assays
Published in Antimicrobial Agents and Chemotherapy (01-06-2012)“…Classifications Services AAC Citing Articles Google Scholar PubMed Related Content Social Bookmarking CiteULike Delicious Digg Facebook Google+ Mendeley Reddit…”
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Broadly Applicable Stereoselective Syntheses of Serrulatane, Amphilectane Diterpenes, and Their Diastereoisomeric Congeners Using Asymmetric Hydrovinylation for Absolute Stereochemical Control
Published in Journal of the American Chemical Society (08-08-2018)“…A stereogenic center, placed at an exocyclic location next to a chiral carbon in a ring to which it is attached, is a ubiquitous structural motif seen in many…”
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Journal Article -
3
Selective melamine detection in multiple sample matrices with a portable Raman instrument using surface enhanced Raman spectroscopy-active gold nanoparticles
Published in Analytica chimica acta (06-07-2012)“…[Display omitted] ► Initial work for field deployable screening of melamine in multiple matrices. ► Without extensive sample preparation, colorimetric…”
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4
Ethylene in Organic Synthesis. Repetitive Hydrovinylation of Alkenes for Highly Enantioselective Syntheses of Pseudopterosins
Published in Journal of the American Chemical Society (20-04-2011)“…In this report we highlight the significant potential of ethylene as a reagent for the introduction of a vinyl group with excellent stereoselectivity at three…”
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5
Sensitive Detection of Oversulfated Chondroitin Sulfate in Heparin Sodium or Crude Heparin with a Colorimetric Microplate Based Assay
Published in Analytical chemistry (Washington) (01-05-2011)“…In this work we describe a 96-well microplate assay for oversulfated chondroitin sulfate A (OSCS) in heparin, based on a water-soluble cationic polythiophene…”
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6
Rapid-screening detection of acetildenafils, sildenafils and avanafil by ion mobility spectrometry
Published in Journal of pharmaceutical and biomedical analysis (05-03-2013)“…[Display omitted] ► IMS used to test herbal supplements for undeclared ED adulterants. ► 8 Viagra® analogs and the new Stendra™ drug were detected at low…”
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7
Synthesis and detection of N-sulfonated oversulfated chondroitin sulfate in marketplace heparin
Published in Analytical biochemistry (01-12-2015)“…N-sulfonated oversulfated chondroitin sulfate (NS–OSCS), recently reported as a potential threat to the heparin supply, was prepared along with its…”
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8
Qualitative screening for adulterants in weight-loss supplements by ion mobility spectrometry
Published in Journal of pharmaceutical and biomedical analysis (01-12-2012)“…Ion mobility spectrometry (IMS) served as a rapid, qualitative screening tool for the analysis of adulterated weight-loss products. We have previously shown…”
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9
Rapid screening and structural elucidation of a novel sibutramine analogue in a weight loss supplement: 11-Desisobutyl-11-benzylsibutramine
Published in Journal of pharmaceutical and biomedical analysis (01-09-2013)“…[Display omitted] ► A novel analogue of sibutramine was detected in weight loss supplements. ► Nuclear magnetic resonance and tandem mass spectrometry led to…”
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10
Genotoxicity of 2-bromo-3′-chloropropiophenone
Published in Toxicology and applied pharmacology (15-07-2013)“…Impurities are present in any drug substance or drug product. They can be process-related impurities that are not completely removed during purification or are…”
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11
Assay of possible economically motivated additives or native impurities levels in heparin by 1H NMR, SAX-HPLC, and anticoagulation time approaches
Published in Journal of pharmaceutical and biomedical analysis (05-09-2010)“…New assays have been developed to detect the presence of economically motivated additives (EMAs) and poor manufacturing processes in heparin. Here, selected…”
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Journal Article -
12
Exocyclic Stereocontrol via Asymmetric Hydrovinylation in the General Synthesis of Pseudopterogorgia Natural Products: Stereoselective X-Y-Mediated Cyclization Studies of an Allene-Ynamide and an Allene-Aldehyde
Published 01-01-2008“…Asymmetric hydrovinylation, the heterodimerization of a prochiral olefin with ethylene gas, has been used to control the exocyclic stereochemistry in the…”
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Dissertation -
13
Exocyclic stereocontrol via asymmetric hydrovinylation in the general synthesis of Pseudopterogorgia natural products. Stereoselective X -Y -mediated cyclization studies of an allene -ynamide and an allene -aldehyde
Published 01-01-2008“…Asymmetric hydrovinylation, the heterodimerization of a prochiral olefin with ethylene gas, has been used to control the exocyclic stereochemistry in the…”
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Dissertation -
14
Exocyclic stereocontrol via asymmetric hydrovinylation in the general synthesis of Pseudopterogorgia natural products. Stereoselective X -Y -mediated cyclization studies of an allene -ynamide and an allene -aldehyde
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Dissertation