Displacement reactions of 2-chloro- and 2,9-dichloro-1,10-phenanthroline: synthesis of a sulfur-bridged bis-1,10-phenanthroline macrocycle and a 2,2′-amino-substituted-bis-1,10-phenanthroline

The synthesis and structural assignments of 9-chloro-1,1-phenanthroline-2(1 H)-thione and 1,10-dihydro-1,10-phenanthroline-2,9-dithione have been accomplished. The sulfur-bridged bis-1,10-phenanthroline macrocycle was readily prepared by heating the thione or equimolar amounts of the dithione and 2,...

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Bibliographic Details

Published in:	Tetrahedron letters Vol. 50; no. 26; pp. 3195 - 3197
Main Authors:	Krapcho, A. Paul, Sparapani, Silvia, Leenstra, Amber, Seitz, Joshua D.
Format:	Journal Article
Language:	English
Published:	Elsevier Ltd 01-07-2009
Subjects:	1,10-Dihydro-1,10-phenanthro-line-2,9-dithione 2-Amino- and 2,9-diamino-substituted 1,10-phenanthrolines 9-Chloro-1,10-phenanthroline-2(1 H)-thione Amino-substituted-2,2′-bis-1,10-phenanthroline Sulfur-bridged bis-1,1-phenanthroline macrocycle 2-Amino- and 2,9-diamino-substituted 1,10-phenanthrolines 1,10-Dihydro-1,10-phenanthro-line-2,9-dithione Amino-substituted-2,2′-bis-1,10-phenanthroline 9-Chloro-1,10-phenanthroline-2(1 H)-thione Sulfur-bridged bis-1,1-phenanthroline macrocycle
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