Synthesis and Structure of 4-[(anthracene-9′-ylmethylene)amino]-5-R-2,4-Dihydro-3H-1,2,4-Triazole-3-Thiones

By the condensation of 4-amino-5- R -2,4-dihydro-3 H -1,2,4-triazole-3-thiones with anthracene-9- carbaldehyde, respective 4-[(anthracene-9′-ylmethylene)amine)]-5- R -2,4-dihydro-3 H -1,2,4-triazole-3-thiones are prepared and structurally characterized by NMR, UV, IR spectroscopies, high-resolution...

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Bibliographic Details
Published in:	Journal of structural chemistry Vol. 65; no. 8; pp. 1631 - 1640
Main Authors:	Kolodina, A. A., Demidov, O. P., Popov, L. D., Dubonosova, I. V., Khodykina, E. S., Skorova, A. V., Zaichenko, S. B., Borodkina, I. G., Dubonosov, A. D., Metelitsa, A. V., Vlasenko, V. G.
Format:	Journal Article
Language:	English
Published:	Moscow Pleiades Publishing 01-08-2024 Springer Nature B.V
Subjects:	Anthracene Atomic Atomic/Molecular Structure and Spectra Chemistry Chemistry and Materials Science Inorganic Chemistry Mass spectrometry Molecular NMR Nuclear magnetic resonance Optical and Plasma Physics Physical Chemistry Single crystals Solid State Physics Triazoles anthracene single crystal X-ray diffraction azomethine ligands 4-amino-1,2,4-triazole-3-thione
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Summary:	By the condensation of 4-amino-5- R -2,4-dihydro-3 H -1,2,4-triazole-3-thiones with anthracene-9- carbaldehyde, respective 4-[(anthracene-9′-ylmethylene)amine)]-5- R -2,4-dihydro-3 H -1,2,4-triazole-3-thiones are prepared and structurally characterized by NMR, UV, IR spectroscopies, high-resolution mass spectrometry, and single crystal XRD. The effect of a substituent at position 5 in triazole moieties of azomethines obtained on their head-to-head or head-to-tail crystal packings is determined.
ISSN:	0022-4766 1573-8779
DOI:	10.1134/S0022476624080146