Fracture surface analysis of free-standing diamond films

Free-standing CVD diamond disk-shaped films of varying thicknesses between ∼40 and 1000 μm were fractured in ball-on-ring flexure using a high-precision hydraulic testing machine. Some of the films were smooth on the side formerly in contact with the substrate and rough (large crystallites) on the r...

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Bibliographic Details
Published in:Journal of materials research Vol. 9; no. 6; pp. 1540 - 1545
Main Authors: Hehn, L.P., Chen, Z., Mecholsky, J.J., Klocek, P., Hoggins, J.T., Trombetta, J.M.
Format: Journal Article
Language:English
Published: New York, USA Cambridge University Press 01-06-1994
Online Access:Get full text
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Summary:Free-standing CVD diamond disk-shaped films of varying thicknesses between ∼40 and 1000 μm were fractured in ball-on-ring flexure using a high-precision hydraulic testing machine. Some of the films were smooth on the side formerly in contact with the substrate and rough (large crystallites) on the reverse side and some of the films were polished. Raman spectroscopic examination showed some of the films to be of high quality and others to be of lower quality (higher levels of non-diamond carbon mixed with diamond phase). All fracture surfaces were examined to identify the origin of failure. Strength varied between 650 and 971 MPa, and the fracture toughness was determined from fracture surface analysis to average 8 ± 1 MPam1/2.
Bibliography:PII:S0884291400074276
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ArticleID:07427
ObjectType-Article-2
SourceType-Scholarly Journals-1
ObjectType-Feature-1
content type line 23
ISSN:0884-2914
2044-5326
DOI:10.1557/JMR.1994.1540