Search Results - "Gilard, Véronique"
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A review of synthetic phosphodiesterase type 5 inhibitors (PDE-5i) found as adulterants in dietary supplements
Published in Journal of pharmaceutical and biomedical analysis (05-01-2018)“…[Display omitted] •80 PDE-5i have been found as adulterants in dietary supplements from 2003 to Mar 2017.•Sildenafil analogues (62%) are the top list and…”
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Benchtop NMR Coupled with Chemometrics: A Workflow for Unveiling Hidden Drug Ingredients in Honey-Based Supplements
Published in Molecules (Basel, Switzerland) (01-05-2024)“…Recently, benchtop nuclear magnetic resonance (NMR) spectrometers utilizing permanent magnets have emerged as versatile tools with applications across various…”
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Screening of “spice” herbal mixtures: From high-field to low-field proton NMR
Published in Forensic science international (01-10-2017)“…[Display omitted] •Both high- and low-field NMR were used for the screening of 41 spice herbal mixtures.•Low-field NMR allows the detection of synthetic…”
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Chemometric Analysis of Low-field 1H NMR Spectra for Unveiling Adulteration of Slimming Dietary Supplements by Pharmaceutical Compounds
Published in Molecules (Basel, Switzerland) (06-03-2020)“…The recent introduction of compact or low-field (LF) NMR spectrometers that use permanent magnets, giving rise to proton (1H) NMR frequencies between 40 and 80…”
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Comparative Chemical Profiling and Monacolins Quantification in Red Yeast Rice Dietary Supplements by 1H-NMR and UHPLC-DAD-MS
Published in Molecules (Basel, Switzerland) (13-01-2020)“…Red yeast rice dietary supplements (RYR DS) are largely sold in Western countries for their cholesterol-lowering/regulating effect due to monacolins, mainly…”
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Evaluation of a Benchtop Cryogen-Free Low-Field 1H NMR Spectrometer for the Analysis of Sexual Enhancement and Weight Loss Dietary Supplements Adulterated with Pharmaceutical Substances
Published in Analytical chemistry (Washington) (02-12-2014)“…Nuclear magnetic resonance (NMR) spectroscopy is a unique tool for detection, structural characterization, and quantification of compounds in complex mixtures…”
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Luminescent lanthanide complexes for reactive oxygen species biosensing and possible application in Alzheimer’s diseases
Published in The FEBS journal (01-05-2022)“…Histopathological hallmarks of Alzheimer’s disease (AD) are intracellular neurofibrillary tangles and extracellular formation of senile plaques composed of the…”
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Fluorine nuclear magnetic resonance spectroscopy of human biofluids in the field of metabolic studies of anticancer and antifungal fluoropyrimidine drugs
Published in Clinica chimica acta (01-04-2006)“…Fluorine-19 nuclear magnetic resonance ( 19F NMR) spectroscopy provides a highly specific tool for the detection, identification and quantification of…”
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Current trends and advances in analytical techniques for the characterization and quantification of biologically recalcitrant organic species in sludge and wastewater: A review
Published in Analytica chimica acta (01-04-2021)“…The study of organic matter in wastewater is a major regulatory and environmental issue and requires new developments to identify non-biodegradable refractory…”
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Synthetic cannabinoids in e-liquids: A proton and fluorine NMR analysis from a conventional spectrometer to a compact one
Published in Forensic science international (01-07-2021)“…•NMR was applied to the analysis of e-liquids containing synthetic cannabinoids.•The 1H NMR profiles of 13 samples of e-liquids were obtained with HF and LF…”
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The POWER saga from 2007 to 2022: An example of a sexual enhancement dietary supplement tainted by different adulterants and still on the market
Published in Journal of pharmaceutical and biomedical analysis (01-04-2023)“…Ten POWER dietary supplements, chronologically called tabs, pills then caps, and advertised as 100% natural aphrodisiacs, were analyzed by 1H NMR from 2007 to…”
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Encapsulation of photosensitizer worsen cell responses after photodynamic therapy protocol and polymer micelles act as biomodulators on their own
Published in International journal of pharmaceutics (30-09-2024)“…[Display omitted] •Polymer micelles increase the amount of photosensitizer delivered to cells.•Encapsulation of photosensitizer accentuates cellular…”
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Characterization of fatty acid forms using benchtop NMR in omega-3 oil supplements
Published in Magnetic resonance in chemistry (01-05-2024)“…Omega-3 fatty acid supplements, such as fish oil and plant-based oils, have gained popularity because of their potential health benefits. However, the quality…”
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1H NMR Analysis of Cerebrospinal Fluid from Alzheimer's Disease Patients: An Example of a Possible Misinterpretation Due to Non-Adjustment of pH
Published in Metabolites (19-02-2014)“…Two publications from the same research group reporting on the detection of new possible biomarkers for the early diagnosis of Alzheimer's disease (AD), based…”
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Comparative study of volatile organic compound profiles in aromatic and non-aromatic rice cultivars using HS-GC–IMS and their correlation with sensory evaluation
Published in Food science & technology (01-07-2024)“…Analyzing of volatile organic compounds (VOCs) is important in rice quality control and breeding aromatic cultivars. This study utilized HS-GC–IMS, known for…”
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Pulsed Field Gradient NMR with Sigmoid Shape Gradient Sampling To Produce More Detailed Diffusion Ordered Spectroscopy Maps of Real Complex Mixtures: Examples with Medicine Analysis
Published in Analytical chemistry (Washington) (15-03-2016)“…NMR diffusion measurements are based on signal attenuation. In the case of complex mixtures for which some molecules are diffusing quickly while others are…”
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Separation of unsaturated C18 fatty acids using perfluorinated‐micellar electrokinetic chromatography: I. Optimization and separation process
Published in Electrophoresis (01-02-2023)“…Ammonium perfluorooctanoate (APFOA) was used as a surfactant for the separation of free unsaturated C18 fatty acids by micellar electrokinetic chromatography…”
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Analytical methods for the detection and characterization of unapproved phosphodiesterase type 5 inhibitors (PDE-5i) used in adulteration of dietary supplements- a review
Published in Food additives & contaminants. Part A, Chemistry, analysis, control, exposure & risk assessment (02-12-2023)“…This article is an up-to-date review of 112 unapproved phosphodiesterase type 5 inhibitors (PDE-5i) found as adulterants in sexual enhancement dietary…”
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First identification and quantification of lorcaserin in an herbal slimming dietary supplement
Published in Journal of pharmaceutical and biomedical analysis (01-09-2014)“…•The illegal adulteration of a dietary supplement claimed to be 100% natural is reported.•The adulterant is the weight-loss prescription drug lorcaserin,…”
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Proton NMR for detection, identification and quantification of adulterants in 160 herbal food supplements marketed for weight loss
Published in Journal of pharmaceutical and biomedical analysis (30-05-2016)“…[Display omitted] •1H NMR analysis of 160 “100% natural” weight loss food supplements.•56% were tainted with 6 active pharmaceutical ingredients.•Sibutramine,…”
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