Search Results - "Fyfe, C. A"
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Quantitative NMR imaging study of the mechanism of drug release from swelling hydroxypropylmethylcellulose tablets
Published in Journal of controlled release (03-09-2000)“…NMR imaging has been used to study the release behavior of two model drugs, triflupromazine–HCl and 5-fluorouracil, from swelling hydroxypropylmethylcellulose…”
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Investigation of Hydrogel Formation from Hydroxypropylmethylcellulose (HPMC) by NMR Spectroscopy and NMR Imaging Techniques
Published in Macromolecules (06-10-1997)“…NMR imaging has been used to investigate the in situ swelling behavior of 2-hydroxypropylmethylcellulose (HPMC) tablets in a sample geometry chosen for the…”
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NMR imaging investigations of drug delivery devices using a flow-through USP dissolution apparatus
Published in Journal of controlled release (31-07-2000)“…A system for performing NMR imaging experiments on drug delivery devices within a flow-through dissolution apparatus, USP Apparatus 4, has been developed. The…”
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One- and two-dimensional high-resolution solid-state NMR studies of zeolite lattice structures
Published in Chemical reviews (01-11-1991)Get full text
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Simple, efficient syntheses of zeolite ZSM-11 ( MEL) at temperatures below 100 °C using very dense gels
Published in Microporous and mesoporous materials (01-03-2012)“…Dense gel syntheses of phase pure MEL at temperatures below 100 °C with crystallisation times similar to conventional syntheses at much higher temperatures…”
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Complications in investigations of the swelling of hydrogel matrices due to the presence of trapped gas
Published in Journal of controlled release (02-03-1998)“…In recent studies, NMR imaging has been used to investigate the swelling of hydroxypropylmethylcellulose (HPMC) tablets and to determine polymer concentration…”
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Solid-state NMR detection, characterization, and quantification of the multiple aluminum environments in US-Y catalysts by (27)Al MAS and MQMAS experiments at very high field
Published in Journal of the American Chemical Society (06-06-2001)“…The detection of all of the aluminum present in steamed zeolite H-Y catalysts by (27)Al MAS NMR at 14.4 T (600 MHz for (1)H) and 18.8T (800 MHz for (1)H) is…”
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Efficient, low-cost, minimal reagent syntheses of high silica zeolites using extremely dense gels below 100 °C
Published in Microporous and mesoporous materials (01-10-2011)“…The powder XRD pattern in the figure demonstrates the high quality of MFI samples prepared from very dense gels with stochiometric quantities of silica and…”
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Harvesting and climate effects on organic matter characteristics in British Columbia coastal forests
Published in Journal of environmental quality (01-03-2002)“…As part of investigations into the effects of harvesting old-growth forest, we characterized carbon in five organic matter pools in eight forest…”
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Solid-State NMR Characterization of the Mineral Searlesite and Its Detection in Complex Synthesis Mixtures
Published in Inorganic chemistry (05-11-2001)“…The mineral searlesite (NaBSi2O5(OH)2) was synthesized and characterized by 1H, 11B, 23Na, and 29Si magic-angle spinning (MAS) NMR spectroscopy. From these…”
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INEPT Experiments in Solid-State NMR
Published in Journal of the American Chemical Society (01-10-1995)Get full text
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Observation of muonium in zeolites
Published in Physica. B, Condensed matter (01-02-2003)“…Muonium has been directly detected over a range of temperatures and fields by transverse field μSR in different zeolites: 3A, 13X, USY, ZSM-5, and S-115 (a…”
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Journal Article Conference Proceeding -
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Resolving crystallographically distinct tetrahedral sites in silicalite and ZSM-5 by solid-state NMR
Published in Nature (London) (01-01-1982)“…"Magic-angle-spinning" NMR has revealed fresh insights into the atomic structure of the polymorph of silica, silicalite, which has exceptional absorptive…”
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Use of NMR imaging in the optimization of a compression-coated regulated release system
Published in Journal of controlled release (12-02-1998)“…Nuclear magnetic resonance (NMR) imaging is routinely used to detect the protons of mobile water molecules within samples. In this investigation, this…”
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Lattice Energy-Minimization Calculation in the Further Investigation of XRD and NMR Studies of Zeolite Frameworks
Published in Chemistry of materials (01-02-2000)“…A knowledge of the local structure of zeolite frameworks is an important prerequisite for a detailed and quantitative understanding of e.g. catalytic…”
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Monitoring of structural changes accompanying ultrastabilization of faujasitic zeolite catalysts
Published in Nature (London) (01-01-1982)“…By recording high-resolution solid-state NMR spectra of zeolitic samples spun (at similar to 3 kHz) at the magic angle ( theta = 54 degree 44' so that 3 cos…”
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Direct Solid-State 13C NMR Evidence for Covalent Bond Formation between an Immobilized Vinylsilane Linking Agent and Polymer Matrixes
Published in Macromolecules (01-05-1995)Get full text
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Zeolite Nanoclusters Coated onto the Mesopore Walls of SBA-15
Published in Journal of the American Chemical Society (10-11-2004)“…Ultrahigh-field 27Al MAS and MQMAS NMR and 129Xe NMR were used to characterize the zeolite-coated SBA-15 materials. This study shows evidence that zeolite…”
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Proton NMR method for the quantitative determination of the water content of the polymeric fluorosulfonic acid Nafion-H
Published in Macromolecules (01-02-1986)Get full text
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Measurement of Cryoprotective Solvent Penetration into Intact Organ Tissues Using High-Field NMR Microimaging
Published in Cryobiology (01-09-1997)“…Existing methods are not able to monitor accurately the penetration of cryoprotective solvents (CPS) into intact tissues. In this study, NMR imaging is shown…”
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