Search Results - "FLORES, Alex F. C"
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Efficient sonochemical synthesis of novel 3,5-diaryl-4,5-dihydro-1H-pyrazole-1-carboximidamides
Published in Ultrasonics sonochemistry (2010)“…An ultrasound-assisted preparation of a series of novel 3,5-diaryl-4,5-dihydro-1H-pyrazole-1-carboximidamides that proceeds via the efficient reaction of…”
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2
Ultrasound promoted synthesis of thioesters from 2-mercaptobenzoxa(thia)zoles
Published in Ultrasonics sonochemistry (01-02-2010)“…An ultrasound-enhanced method has been developed for the synthesis of a variety of thioesters from benzoyl chlorides and 2-mercaptobenzoxa(thia)zoles. Applying…”
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3
Environmentally friendly sonocatalysis promoted preparation of 1-thiocarbamoyl-3,5-diaryl-4,5-dihydro-1H-pyrazoles
Published in Ultrasonics sonochemistry (01-08-2009)“…An efficient and green synthesis of thiocarbamoyl-3,5-diaryl-4,5-dihydro-1H-pyrazoles via the condensation of chalcones with thiosemicarbazide in ethanol and…”
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4
Ultrasound promoted greener synthesis of 2-(3,5-diaryl-4,5-dihydro-1 H-pyrazol-1-yl)-4-phenylthiazoles
Published in Ultrasonics sonochemistry (2011)“…A rapid and cleaner procedure for the synthesis of a series of 2-(3,5-diaryl-4,5-dihydro-1 H-pyrazol-1-yl)-4-phenylthiazoles under ultrasonic irradiation in…”
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5
Ultrasound assisted efficient conversion of aromatic aldehydes from oximes
Published in Ultrasonics sonochemistry (01-01-2013)“…This work describes the ultrasound-assisted regeneration of aldehydes from oximes in ethanol and phosphoric acid as mediator of the reaction. The large scale…”
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6
Synthesis in Water and Antimicrobial Activity of 5-Trichloromethyl-4,5-dihydroisoxazoles
Published in Synthetic communications (02-09-2013)“…Two series of 5-trichloromethylisoxazoles were synthesized from the cyclocondensation of 1,1,1-trichloro-4-methoxy-3-alken-2-ones [Cl 3 CC(O)C(R 2 ) = C(R 1…”
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Physico-chemical characterization of asolectin–genistein liposomal system: An approach to analyze its in vitro antioxidant potential and effect in glioma cells viability
Published in Chemistry and physics of lipids (01-12-2015)“…[Display omitted] •Genistein–asolectin liposomes interaction was studied by several techniques.•Genistein effects on liposomes were correlated with its…”
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8
Ultrasound-Promoted Environmentally Friendly Synthesis of 5-(3,3,3-Trifluoro-2-oxopropylidene)pyrrolidin-2-ones
Published in Synthetic communications (19-03-2015)“…A facile, one-pot, ultrasound-promoted synthesis of N-substituted 5-(3,3,3-trifluoro-2-oxopropylidene)pyrrolidin-2-ones from methyl…”
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9
Cyclocondensation between fatty acid hydrazides and 1,1,1-trifluoro-4-alkoxy-3-alken-2-ones: Introducing a trifluoromethylated head onto fatty acid moieties
Published in Synthetic communications (17-11-2017)“…This paper reports the regioselective synthesis of new trifluoromethylated lipid derivatives, namely,…”
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10
From Levulinic Acid to Biheterocycles: Synthesis of 1-[(5-Hydroxy-5-trifluoromethyl-3-substituted-4,5-dihydro-1H-pyrazol-1-yl)-3-(5-trifluoromethyl-1H-pyrazol-3-yl)propan-1-ones
Published in Synthetic communications (19-05-2015)“…We develop an efficient method to synthesize novel propionyl-spaced bisheterocyclic compounds. It entails cyclocondensation of…”
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11
Synthesis of diverse N-acyl-pyrazoles via cyclocondensation of hydrazides with α-oxeketene dithioacetal
Published in Molecular diversity (01-11-2017)“…An elegant, efficient, and highly regioselective approach for the synthesis of novel methyl 5-amino-3-(methylthio)-1-differently substituted-1 H…”
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12
From Renewable Levulinic Acid to a Diversity of 3-(Azol-3-yl)Propanoates
Published in Journal of heterocyclic chemistry (01-05-2014)“…Efficient heterocyclization of methyl 7,7,7‐trifluoro‐4‐methoxy‐6‐oxo‐4‐heptenoate and methyl 7,7,7‐trichloro‐4‐methoxy‐6‐oxo‐4‐heptenoate into isoxazole and…”
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13
Cycloaromatization Reaction of 4-Alkoxy-1,1,1-trifluoroalk-3-en-2-ones with 2,6-Diaminotoluene: The Unexpected Regioselective Synthesis of 2,4,7,8-Tetrasubstituted Quinolines
Published in Journal of heterocyclic chemistry (01-02-2013)“…This article reports a convenient and general method for the regioselective synthesis of a new series of…”
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14
Synthesis, Structure, and Cyclocondensation of the 4,4,4-Trifluoro-3,3-dihydroxy-2-methyl-1-(thien-2-yl)-1-butanone with Hydroxylamine and Hydrazine
Published in Journal of spectroscopy (Hindawi) (01-01-2018)“…The synthesis of 4,4,4-trifluoro-3,3-dihydroxy-2-methyl-1-(thien-2-yl)butan-1-one (3) through acylation of 1,1-dimethoxy-1-(thien-2-yl)propane (1) with…”
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15
Highly Chemoselective Synthesis of 6-Alkoxy-1-alkyl(aryl)-3-trifluoroacetyl-1,4,5,6-tetrahydropyridines and 1-Alkyl(aryl)-6-amino-3-trifluoroacetyl-1,4,5,6-tetrahydropyridines
Published in European Journal of Organic Chemistry (01-03-2009)“…A simple and highly chemoselective method for the synthesis of a large series of novel 6‐alkoxy‐1‐alkyl(aryl)‐3‐trifluoroacetyl‐1,4,5,6‐tetrahydropyridines and…”
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Book Review Journal Article -
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Synthesis and Structure of Novel 1-Aryl-4,4,4-trichloro-1,3-butanediones
Published in Synthetic communications (01-03-2012)“…Novel 1-aryl-4,4,4-trichloro-1,3-butanediones in good yields (80-97%) were synthesized in one pot through acetal acylation with trichloroacetyl chloride…”
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17
Convergent procedure for the synthesis of trifluoromethyl-containing N-(pyridinyl-triazolyl)pyrimidin-2-amines
Published in Journal of fluorine chemistry (01-12-2010)“…This study describes a simple and efficient procedure to synthesize a novel series of fourteen 4-substituted…”
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18
Experimental and calculated structural parameters of 5-trihalomethyl-4,5-dihydro-1H-pyrazole derivatives, novel analgesic agents
Published in Journal of molecular structure (15-01-2009)“…The crystal structures of four novel analgesic agents, methyl 5-hydroxy-3- or 4-methyl-5-trichloro[trifluoro]methyl-4,5-dihydro-1H-pyrazole-1-ca r boxylate,…”
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19
Microwave-assisted synthesis of novel 5-trichloromethyl-4,5-dihydro-1H-1-pyrazole methyl esters under solvent free conditions
Published in Journal of the Brazilian Chemical Society (01-04-2006)“…Twelve novel 5-trichloromethyl-4,5-dihydro-1H-1-pyrazole ethyl esters have been synthesized in good yields (70-98%) by using environmentally benign microwave…”
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20
Synthesis of the omega-brominated alpha-trifluoroacetylcycloalkanones and their isoxazole derivatives
Published in Journal of the Brazilian Chemical Society (01-01-2006)“…The reactions of a serie of the 2-trifluoroacetyl-1-methoxy-1-cycloalkenes (1a-1e) and 2-trifluoroacetylcycloalkanones (2a-2e) with molecular bromine to obtain…”
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