Search Results - "Drebushchak, V. A"
-
1
Thermal expansion of solids: review on theories
Published in Journal of thermal analysis and calorimetry (01-10-2020)“…The coefficient of thermal expansion of a solid can be derived from (1) anharmonicity of atomic vibrations; (2) lattice dynamics; (3) equation of state by G…”
Get full text
Journal Article -
2
Structural similarity and similarity in thermal properties of the polymorphs: melting and crystallization from the melt of tolbutamide and chlorpropamide
Published in Journal of thermal analysis and calorimetry (01-10-2020)“…The polymorphism of tolbutamide and chlorpropamide under melting/crystallization was investigated with using DSC and in situ X-ray powder diffraction. The…”
Get full text
Journal Article -
3
Calorimetric measurements of sodium chloride dihydrate (hydrohalite)
Published in Journal of thermal analysis and calorimetry (01-06-2020)“…Calorimetric measurements of sodium chloride dihydrate NaCl·2H 2 O (mineral name hydrohalite) were carried out with using DSC. Heat capacity from 190 to 250 K…”
Get full text
Journal Article -
4
Model-free temperature scaling for heat capacity
Published in Journal of thermal analysis and calorimetry (01-10-2017)“…In treating the experimental data on the heat capacity of solids, the essence of any model application is in the searching for the scaling factors ( k i or 1/Θ…”
Get full text
Journal Article -
5
Cooling rate “window” in the crystallization of metacetamol form II
Published in Journal of thermal analysis and calorimetry (01-02-2017)“…Melting and crystallization of metacetamol (C 8 H 9 NO 2 , N-(3-hydroxyphenyl)acetamide, structural isomer of paracetamol) were measured using DSC cycling…”
Get full text
Journal Article -
6
Calibration coefficient of a heat-flow DSC; Part II. Optimal calibration procedure
Published in Journal of thermal analysis and calorimetry (01-01-2005)“…One-point (Mettler) and many-point (Netzsch) heat flow calibration of a DSC is discussed. It is shown that the two types of calibration are the alternative…”
Get full text
Journal Article -
7
Glycine phases formed from frozen aqueous solutions: revisited
Published in The Journal of chemical physics (14-08-2012)“…Glycine phases formed when aqueous solutions were frozen and subsequently heated under different conditions were studied by Raman scattering, x-ray…”
Get more information
Journal Article -
8
-
9
The investigation of ancient pottery: Application of thermal analysis
Published in Journal of Thermal Analysis and Calorimetry (01-11-2005)“…Ancient ceramic samples (single fragments and different parts of pots, unbroken and repaired; total about 180 samples) dated from the transitional period of…”
Get full text
Journal Article -
10
CHANGES IN THE HEAT CAPACITY OF Al2O3-Cr2O3 SOLID SOLUTIONS NEAR THE POINT OF ANTIFERROMAGNETIC PHASE TRANSITION IN Cr2O3
Published in Journal of thermal analysis and calorimetry (01-12-2007)“…Al2O3-Cr2O3 solid solutions with 0, 4, 7, 10 and 20 mol% of corundum were synthesized using a high-pressure/high-temperature apparatus and characterized by…”
Get full text
Journal Article -
11
Calibration coefficient of a heat-flow DSC Part 1. Relation to the sensitivity of a thermocouple
Published in Journal of thermal analysis and calorimetry (01-01-2004)“…Relation between the calibration coefficient of a DSC sensor k(T) and the sensitivity of a thermocouple *e(T) which the sensor is made from was derived from…”
Get full text
Journal Article -
12
Thermoanalytical investigations of ancient ceramics
Published in Journal of thermal analysis and calorimetry (01-07-2018)“…The review consists of four parts. Part I is about the thermal transformation in clay minerals under firing and about the properties of fired clay. The…”
Get full text
Journal Article -
13
Synthesis and calorimetric investigation of stoichiometric Fe-spinels: MgFe2O4
Published in Journal of crystal growth (15-04-2004)“…Spinel MgFe2O4 was synthesized at 1373K from oxides MgO and Fe2O3 using silica-tube technique with intermediate grinding. The product is homogeneous and fine…”
Get full text
Journal Article -
14
The Peltier effect
Published in Journal of thermal analysis and calorimetry (2008)“…Thermodynamic consideration of thermoelectricity in metals was applied to the Peltier effect, like it was done recently for the Seebeck effect. The Peltier…”
Get full text
Journal Article -
15
Experimental heat capacity of LiInS2, LiInSe2, LiGaS2, LiGaSe2, and LiGaTe2 from 180 to 460 K
Published in Journal of thermal analysis and calorimetry (01-07-2017)“…Heat capacity of single-crystal samples of five chalcogenides (LiInS 2 , LiInSe 2 , LiGaS 2 , LiGaSe 2 , and LiGaTe 2 ) was measured with DSC in a temperature…”
Get full text
Journal Article -
16
Recommendations on DSC calibration
Published in Journal of thermal analysis and calorimetry (01-05-2016)“…The enthalpy of fusion of indium was measured at the heating rates of 3, 9, and 15 K min.sup.-1 according to two procedures, with and without replacing the…”
Get full text
Journal Article -
17
Synthesis and calorimetric investigation of unstable β-glycine
Published in Journal of crystal growth (01-05-2002)“…A new procedure for the synthesis of the unstable β-polymorph of glycine has been developed. The amount of the sample synthesized in one run is enough to carry…”
Get full text
Journal Article -
18
CRYSTALLINE FORMS OF BETULIN: POLYMORPHISM OR PSEUDOPOLYMORPHISM?
Published in Journal of structural chemistry (01-08-2020)“…By recrystallization with different solvents as well as decomposition of betulin ethanol solvate at room temperature a new crystalline form of the biologically…”
Get full text
Journal Article -
19
Crystallization of sodium chloride dihydrate (hydrohalite)
Published in Journal of crystal growth (01-07-2019)“…•Crystallization behavior of hydrohalite is poorly known.•A simple and fast procedure of hydrohalite crystallization is reported.•From X-ray diffraction…”
Get full text
Journal Article -
20
Polymorphic effects at the eutectic melting in the H2O–glycine system
Published in Journal of thermal analysis and calorimetry (01-03-2013)“…Solid mixtures of ice with three glycine polymorphs were heated up to the eutectic melting and the DSC has detected the eutectic temperatures of −2.8 °C for…”
Get full text
Journal Article