Search Results - "Campos, Patrick T"
-
1
Regiochemistry of cyclocondensation reactions in the synthesis of polyazaheterocycles
Published in Beilstein journal of organic chemistry (10-02-2017)“…The syntheses of several polyazaheterocycles are demonstrated. The cyclocondensation reactions between β-enaminodiketones [CCl C(O)C(=CNMe )C(O)-CO Et] and…”
Get full text
Journal Article -
2
Structural Investigation, UV–Vis Analysis and Crystal Packing of Spiro[chromeno[4,3-b]quinoline-6,1′-cycloalkan]-7-amine: Novel Tacrine Hybrids by Single Crystal X-Ray Diffraction
Published in Journal of chemical crystallography (01-06-2018)“…The structure of four spiro[chromeno[4,3- b ]quinoline-6,1′-cycloalkan]-7-amine ( 1 – 4 ) was determined by X-ray diffraction methods. The quinoline rings were…”
Get full text
Journal Article -
3
Evaluation of the Antioxidant Activity of Copper(II) Complexes containing Tris-(hydroxymethyl)aminomethane (TRIS) Units
Published in Zeitschrift für anorganische und allgemeine Chemie (1950) (01-10-2016)“…The structural analysis and the SOD‐like activity of CuII complexes [(Cu)(C16H18N3O5)]ClO4 (1) and [(Cu)4(C36H52N8O12)] (2) are described with ligands obtained…”
Get full text
Journal Article -
4
2-Methyl-5-(4-tol-yl)-7-(trifluoro-meth-yl)pyrazolo[1,5-a]pyrimidine
Published in Acta crystallographica. Section E, Structure reports online (01-01-2008)“…In the title compound, C(15)H(12)F(3)N(3), the pyrazolo[1,5-a]pyrimidine system ring is essentially planar with a maximum deviation from the mean plane of…”
Get full text
Journal Article -
5
Ultrasound promoted the synthesis of N-propargylic β-enaminones
Published in Ultrasonics sonochemistry (01-03-2012)“…► Synthesis of novel N-propargylic β-enaminones. ► Comparison among different methodologies. ► Ultrasound irradiation efficiently leads to the desired…”
Get full text
Journal Article -
6
Synthesis and Structure of Novel 1-Aryl-4,4,4-trichloro-1,3-butanediones
Published in Synthetic communications (01-03-2012)“…Novel 1-aryl-4,4,4-trichloro-1,3-butanediones in good yields (80-97%) were synthesized in one pot through acetal acylation with trichloroacetyl chloride…”
Get full text
Journal Article -
7
Molecular structure of pyrazolo[1,5- a]pyrimidines: X-ray diffractometry and theoretical study
Published in Journal of molecular structure (17-09-2009)“…The structure of 7-trichloromethyl-2-methylpyrazolo[1,5- a]pyrimidine ( 1) and 3-bromo-2-methyl-7-(thien-2-yl)pyrazolo[1,5- a]pyrimidine ( 2) was determined by…”
Get full text
Journal Article -
8
Experimental and calculated structural parameters of 5-trihalomethyl-4,5-dihydro-1H-pyrazole derivatives, novel analgesic agents
Published in Journal of molecular structure (15-01-2009)“…The crystal structures of four novel analgesic agents, methyl 5-hydroxy-3- or 4-methyl-5-trichloro[trifluoro]methyl-4,5-dihydro-1H-pyrazole-1-ca r boxylate,…”
Get full text
Journal Article -
9
Structural investigations of 5-hydroxy-4,5-dihydroisoxazoles
Published in Journal of molecular structure (14-12-2011)“…► 4,5-Dihydroisoxazoles were characterized and compared with similar structures. ► A robust supramolecular synthon O-H⋅⋅⋅N,O in 4,5-dihydroisoxazole were…”
Get full text
Journal Article -
10
Supramolecular structure of enaminones in solid-state
Published in Journal of molecular structure (24-09-2010)“…The crystalline structure of four enaminones [R 1C(O)CH C(Me)NR 2R 3, where R 1 = CCl 3, R 2 = H, R 3 = Bn ( 1); R 1 = CHCl 2, R 2 = H, R 3 = Bn ( 2); R 1 =…”
Get full text
Journal Article -
11
Influence of bulky and halogen substituents on crystal packing of pyrazolo[1,5- a]pyrimidines
Published in Journal of molecular structure (12-10-2011)“…► Molecular and packing structures were determined by X-ray crystallography. ► Cl⋯Cl, Cl⋯Br and Cl⋯N were found as main intermolecular interactions. ►…”
Get full text
Journal Article -
12
Efficient preparation of novel N-propargylic β-enaminones from the reaction of β-alkoxyvinyltrihalomethyl[carboxy]ketones and propargylamines
Published in ARKIVOC (16-06-2010)Get full text
Journal Article Web Resource -
13
Design, synthesis, and structure of alkyl 1H-pyrazolecarboxylates from a raspberry ketone methyl ether
Published in Chemistry of heterocyclic compounds (New York, N.Y. 1965) (01-10-2020)“…This paper reports a one-pot synthesis of 5-[2-(4-methoxyphenyl)ethyl]-1 H -pyrazole-3-carboxylates via cyclocondensation of…”
Get full text
Journal Article -
14
New trifluoromethyl-containing (E)-N′-arylidene-[3-alkyl(aryl/heteroaryl)-4,5-dihydro-1H-pyrazol-1-yl]carbohydrazides: Synthesis, crystal structure and antimicrobial/antioxidant activity
Published in Journal of fluorine chemistry (01-03-2012)“…The regioselective synthesis and structural study via X-ray diffraction of a series of twenty-seven new…”
Get full text
Journal Article -
15
Structural studies of 2-methyl-7-substituted pyrazolo[1,5-a]pyrimidines
Published in Journal of heterocyclic chemistry (01-11-2010)“…Six pyrazolo[1,5‐a]pyrimidines bearing a 7‐trifluoromethyl (three compounds), a 7‐trichloromethyl (two compounds), and a 7‐ethoxycarbonyl (one compound) have…”
Get full text
Journal Article -
16
-
17
X-ray structure, semi-empirical MO calculations and [pi]-electron delocalization of 1-cyanoacetyl-5-trifluoromethyl-5-hydroxy-4,5-dihydro-1H-pyrazo les
Published in Journal of molecular structure (22-04-2010)“…The structure of three 1-cyanoacetyl-3-alkyl[aryl]-5-trifluoromethyl-5-hydroxy-4,5-dihydr o -1H-pyrazoles ( 1- 3) has been determined by X-ray diffractometry…”
Get full text
Journal Article -
18
Synthesis and Structural Analysis of Trichloroacetamidoxime
Published in Journal of chemical crystallography (01-07-2012)“…The trichloroacetoamidoxime was synthesized following the principles of green chemistry in excellent yield (90 %). This compound crystallizes in the…”
Get full text
Journal Article -
19
X-ray structure, semi-empirical MO calculations and π-electron delocalization of 1-cyanoacetyl-5-trifluoromethyl-5-hydroxy-4,5-dihydro-1 H-pyrazoles
Published in Journal of molecular structure (2010)“…The structure of three 1-cyanoacetyl-3-alkyl[aryl]-5-trifluoromethyl-5-hydroxy-4,5-dihydro-1 H-pyrazoles ( 1– 3) has been determined by X-ray diffractometry…”
Get full text
Journal Article -
20
Experimental and calculated structural parameters of 5-trihalomethyl-4,5-dihydro-1 H-pyrazole derivatives, novel analgesic agents
Published in Journal of molecular structure (2009)“…The crystal structures of four novel analgesic agents, methyl 5-hydroxy-3- or 4-methyl-5-trichloro[trifluoro]methyl-4,5-dihydro-1 H-pyrazole-1-carboxylate,…”
Get full text
Journal Article