Search Results - "Cailleu, Dominique"
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Mass Spectrometry, Ion Mobility Separation and Molecular Modelling: A Powerful Combination for the Structural Characterisation of Substituted Cyclodextrins Mixtures
Published in International journal of molecular sciences (01-11-2022)“…When working on the synthesis of substituted cyclodextrins (CDs), the main challenge remains the analysis of the reaction media content. Our objective in this…”
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A Deeper Investigation of Drug Degradation Mixtures Using a Combination of MS and NMR Data: Application to Indapamide
Published in Molecules (Basel, Switzerland) (07-05-2019)“…A global approach that is based on a combination of mass spectrometry (MS) and nuclear magnetic resonance (NMR) data has been developed for a complete and…”
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Combined LC-MS/MS and Molecular Networking Approach Reveals Antioxidant and Antimicrobial Compounds from Erismadelphus exsul Bark
Published in Plants (Basel) (03-06-2022)“…Erismadelphus exsul Mildbr bark is widely used in Gabonese folk medicine. However, little is known about the active compounds associated with its biological…”
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High reactivity of the nickel-rich LiNi1-x-yMnxCoyO2 layered materials surface towards H2O/CO2 atmosphere and LiPF6-based electrolyte
Published in Journal of power sources (31-08-2020)“…Storage of nickel-rich LiNi1-x-yMnxCoyO2 positive active materials under improper environmental conditions brings about undesirable surface reactions causing…”
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Metabolic profiling of maize mutants deficient for two glutamine synthetase isoenzymes using ¹H-NMR-based metabolomics
Published in Phytochemical analysis (01-01-2010)“…Introduction - Maize mutants deficient for the expression of two genes encoding cytosolic glutamine syntehtase (GS) isoenzymes GS1.3 and GS1.4 displayed…”
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Towards a better understanding of vinylene carbonate derived SEI-layers by synthesis of reduction compounds
Published in Journal of power sources (01-07-2019)“…Here two chemical reduction pathways to synthesize the vinylene carbonate (VC) and poly(VC) reduction products are investigated, with the precise aim of…”
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Chemical reactivity of lithium difluorophosphate as electrolyte additive in LiNi0.6Co0.2Mn0.2O2/graphite cells
Published in Electrochimica acta (10-09-2022)“…From the literature overview, lithium difluorophosphate salt, LiPO2F2, is considered a powerful electrolyte additive capable of enhancing lithium-ion…”
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Improving the environmental compatibility of enzymatic synthesis of sugar-based surfactants using green reaction media
Published in Process biochemistry (1991) (01-06-2022)“…The enzymatic synthesis of sugar-based surfactants is often performed in non-conventional media that do not meet any longer the current environmental…”
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IL versus DES: Impact on chitin pretreatment to afford high quality and highly functionalizable chitosan
Published in Carbohydrate polymers (01-10-2021)“…Chitin is mainly extracted from crustaceans, but this resource is seasonally dependent and can represent a major drawback to satisfy the traceability criterion…”
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Toward Conductive Additive Free Organic Electrode for Lithium‐Ion Battery Using Supramolecular Columnar Organization
Published in Small (Weinheim an der Bergstrasse, Germany) (01-01-2024)“…With the aim to meet the greatest challenge facing organic batteries, namely the low conductivity of the electrodes, the electrochemical properties of a series…”
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1-ethyl-3-methyl imidazolium acetate, hemicellulolytic enzymes and laccase-mediator system: Toward an integrated co-valorization of polysaccharides and lignin from Miscanthus
Published in Industrial crops and products (01-07-2023)“…The pretreatment of Miscanthus x giganteus with the ionic liquid 1-ethyl-3-methylimidazolium acetate ([Emim][OAc]), followed by enzymatic hydrolysis and…”
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Influence of common preanalytical variations on the metabolic profile of serum samples in biobanks
Published in Journal of biomolecular NMR (01-12-2011)“…A blood pre-centrifugation delay of 24 h at room temperature influenced the proton NMR spectroscopic profiles of human serum. A blood pre-centrifugation delay…”
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Structural characterization and rheological properties of a galactomannan from Astragalus gombo Bunge seeds harvested in Algerian Sahara
Published in Carbohydrate polymers (01-11-2017)“…•High yield polysaccharides extracted from Astragalus gombo seeds.•Galactomannan from Astragalus gombo seeds with mannose/galactose=1.7.•High molecular weight…”
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Combined MS-NMR approach for the quality control of food supplements containing amino acids
Published in Food control (01-06-2018)“…A global analytical control of dietary supplements has become essential. In this field, additives containing amino acids (AAs) are of growing interest in the…”
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Use of qNMR for speciation of flaxseeds (Linum usitatissimum) and quantification of cyanogenic glycosides
Published in Analytical and bioanalytical chemistry (01-12-2017)“…This report describes a routine method taking less than 20 min to quantify cyanogenic glycosides such as linustatin and neolinustatin from flaxseeds ( Linum…”
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Benefits of methylated cyclodextrins in the development of midazolam pharmaceutical formulations
Published in Journal of pharmaceutical sciences (01-07-2013)“…Midazolam (MDZ) is a benzodiazepine commonly administered in preanesthesia of children by oral or by sublingual routes. To mask its bitter taste and enhance…”
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Processing of NMR and MS metabolomics data using chemometrics methods: a global tool for fungi biotransformation reactions monitoring
Published in Metabolomics (01-08-2019)“…Introduction Biotransformation constitutes an important aspect of the drug discovery process, to mimic human metabolism of active principal ingredient but also…”
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Osmoregulated trehalose-derived oligosaccharides in Sinorhizobium meliloti
Published in FEBS letters (20-08-2010)“…Sinorhizobium meliloti is a soil bacterium accumulating glutamate, N-acetylglutaminyl glutamine amide and trehalose in hyperosmolarity. Besides these…”
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5‐O‐Caffeoylshikimic acid from Solanum somalense leaves: Advantage of centrifugal partition chromatography over conventional column chromatography
Published in Journal of separation science (01-09-2014)“…Solanum somalense leaves, used in Djibouti for their medicinal properties, were extracted by MeOH. Because of the high polyphenol and flavonoid contents of the…”
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Arylnaphthalene and aryltetralin‐type lignans in hairy root cultures of Linum perenne, and the stereochemistry of 6‐methoxypodophyllotoxin and one diastereoisomer by HPLC‐MS and NMR spectroscopy
Published in Phytochemical analysis (01-09-2015)“…INTRODUCTION: Hairy root cultures of Linum sp. are an alternative for the high production of lignans. Linum perenne is known to produce arylnaphthalene‐type…”
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