Search Results - "Ayala, Juan H."
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Vacuum-assisted headspace-solid phase microextraction for determining volatile free fatty acids and phenols. Investigations on the effect of pressure on competitive adsorption phenomena in a multicomponent system
Published in Analytica chimica acta (15-04-2017)“…This work proposes a new vacuum headspace solid-phase microextraction (Vac-HSSPME) method combined to gas chromatography-flame ionization detection for the…”
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Utilization of highly robust and selective crosslinked polymeric ionic liquid-based sorbent coatings in direct-immersion solid-phase microextraction and high-performance liquid chromatography for determining polar organic pollutants in waters
Published in Talanta (Oxford) (01-09-2016)“…Several crosslinked polymeric ionic liquid (PIL)-based sorbent coatings of different nature were prepared by UV polymerization onto nitinol wires. They were…”
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Evaluation of Structurally Different Ionic Liquid-Based Surfactants in a Green Microwave-Assisted Extraction for the Flavonoids Profile Determination of Mangifera sp. and Passiflora sp. Leaves from Canary Islands
Published in Molecules (Basel, Switzerland) (15-10-2020)“…Aqueous solutions of ionic liquids (ILs) with surface active properties were used as extraction solvents, taking advantage of their impressive solvation…”
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Influence of Ligand Functionalization of UiO-66-Based Metal-Organic Frameworks When Used as Sorbents in Dispersive Solid-Phase Analytical Microextraction for Different Aqueous Organic Pollutants
Published in Molecules (Basel, Switzerland) (03-11-2018)“…Four metal-organic frameworks (MOFs), specifically UiO-66, UiO-66-NH₂, UiO-66-NO₂, and MIL-53(Al), were synthesized, characterized, and used as sorbents in a…”
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Application of a Pillared-Layer Zn-Triazolate Metal-Organic Framework in the Dispersive Miniaturized Solid-Phase Extraction of Personal Care Products from Wastewater Samples
Published in Molecules (Basel, Switzerland) (15-02-2019)“…The pillared-layer Zn-triazolate metal-organic framework (CIM-81) was synthesized, characterized, and used for the first time as a sorbent in a dispersive…”
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Mixed Functionalization of Organic Ligands in UiO-66: A Tool to Design Metal-Organic Frameworks for Tailored Microextraction
Published in Molecules (Basel, Switzerland) (10-10-2019)“…The mixed-ligand strategy was selected as an approach to tailor a metal-organic framework (MOF) with microextraction purposes. The strategy led to the…”
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Green solid-phase microextraction fiber coating based on the metal-organic framework CIM-80(Al): Analytical performance evaluation in direct immersion and headspace using gas chromatography and mass spectrometry for the analysis of water, urine and brewed coffee
Published in Analytica chimica acta (09-10-2020)“…A new solid-phase microextraction (SPME) fiber coating was prepared by the immobilization of the metal-organic framework (MOF) CIM-80(Al) on nitinol wires by a…”
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The metal–organic framework HKUST-1 as efficient sorbent in a vortex-assisted dispersive micro solid-phase extraction of parabens from environmental waters, cosmetic creams, and human urine
Published in Talanta (Oxford) (01-07-2015)“…Three metal–organic frameworks (MOFs), specifically HKUST-1, MOF-5, and MIL-53(Al), have been synthetized, characterized, studied and compared in a…”
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Headspace solid-phase microextraction based on the metal-organic framework CIM-80(Al) coating to determine volatile methylsiloxanes and musk fragrances in water samples using gas chromatography and mass spectrometry
Published in Talanta (Oxford) (01-09-2021)“…A headspace solid-phase microextraction (HS-SPME) method was developed using the metal-organic framework (MOF) CIM-80(Al) as extraction phase and in…”
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Effervescence tablets based on magnetic ionic liquids as simple microdevices for the in situ dispersive liquid-liquid microextraction of urinary biomarkers
Published in Analytica chimica acta (01-11-2024)“…Magnetic ionic liquids (MILs) have been explored in dispersive liquid-liquid microextraction (DLLME). Their usage allows to substitute centrifugation and/or…”
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Guanidinium ionic liquid-based surfactants as low cytotoxic extractants: Analytical performance in an in-situ dispersive liquid–liquid microextraction method for determining personal care products
Published in Journal of Chromatography A (20-07-2018)“…•A new guanidinium IL-based surfactant (C8Gu-Cl) was synthetized.•The micellar behavior of C8Gu-Cl was studied with different techniques.•C8Gu-Cl shows low…”
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Insights in the analytical performance of neat metal-organic frameworks in the determination of pollutants of different nature from waters using dispersive miniaturized solid-phase extraction and liquid chromatography
Published in Talanta (Oxford) (01-03-2018)“…Five metal-organic frameworks (MOFs), specifically HKUST-1, MOF-5(Zn), MIL-53(Al), UiO-64 and MOF-74(Zn) are synthesized, characterized, and utilized in a…”
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Evolution and current advances in sorbent-based microextraction configurations
Published in Journal of Chromatography A (20-12-2020)“…•Sorbent-based microextraction strategies are classified in SPME or µ-SPE•Operational steps and sorbent configuration are the criteria for the…”
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A magnetic-based dispersive micro-solid-phase extraction method using the metal-organic framework HKUST-1 and ultra-high-performance liquid chromatography with fluorescence detection for determining polycyclic aromatic hydrocarbons in waters and fruit tea infusions
Published in Journal of Chromatography A (04-03-2016)“…•The composite MOF HKUST-1+Fe3O4 MNPs is prepared by simple mixing.•The material (25mg) is used in a magnetic-assisted extraction method and UHPLC-FD.•The…”
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A green miniaturized aqueous biphasic system prepared with cholinium chloride and a phosphate salt to extract and preconcentrate personal care products in wastewater samples
Published in Journal of Chromatography A (05-07-2021)“…•A miniaturized aqueous biphasic system (µ-ABS) is formed with food additives.•Cholinium chloride is used as extraction phase and K2HPO4 as salting-out…”
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Solid-phase microextraction coatings based on the metal-organic framework ZIF-8: Ensuring stable and reusable fibers
Published in Talanta (Oxford) (01-08-2020)“…Chemical vapor deposition of MOFs (MOF-CVD) has been used to coat solid-phase microextraction (SPME) fibers with ZIF-8, by exposing ZnO layers to the linker…”
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Salt-induced ionic liquid-based microextraction using a low cytotoxic guanidinium ionic liquid and liquid chromatography with fluorescence detection to determine monohydroxylated polycyclic aromatic hydrocarbons in urine
Published in Analytical and bioanalytical chemistry (01-07-2018)“…A novel ionic liquid (IL)-based microextraction method has been developed for the determination of four hydroxylated polycyclic aromatic hydrocarbons (OHPAHs)…”
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Use of a pH-sensitive polymer in a microextraction and preconcentration method directly combined with high-performance liquid chromatography
Published in Journal of Chromatography A (24-05-2020)“…•A pH-sensitive polymer is used in a microextraction and preconcentration method.•The method simply bases on the formation of a hydrogel by modification of…”
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Magnetic ionic liquids as non-conventional extraction solvents for the determination of polycyclic aromatic hydrocarbons
Published in Analytica chimica acta (31-08-2016)“…This work describes the applicability of magnetic ionic liquids (MILs) in the analytical determination of a group of heavy polycyclic aromatic hydrocarbons…”
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Ionic liquid-based miniaturized aqueous biphasic system to develop an environmental-friendly analytical preconcentration method
Published in Talanta (Oxford) (01-10-2019)“…Two ILs containing guanidinium cations (butylguanidinium chloride –C4Gu-Cl– and hexylguanidinium chloride –C6Gu-Cl–) were synthesized and characterized. Their…”
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