Search Results - "Anupõld, Tiit"
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Symmetry-based recoupling in double-rotation NMR spectroscopy
Published in The Journal of chemical physics (07-11-2008)“…In this contribution, we extend the theory of symmetry-based pulse sequences of types CN(n) (nu) and RN(n) (nu) in magic-angle-spinning nuclear resonance…”
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New Limits for Solid-State 17O NMR Spectroscopy: Complete Resolution of Multiple Oxygen Sites in a Simple Biomolecule
Published in Journal of the American Chemical Society (21-06-2006)“…A solid-state 17O NMR 1H-decoupled double angle rotation (DOR) study of monosodium l-glutamate monohydrate (l-MSG) is reported. It is shown that all eight…”
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Ultra-high resolution 17O solid-state NMR spectroscopy of biomolecules: a comprehensive spectral analysis of monosodium L-glutamate·monohydrate
Published in Physical chemistry chemical physics : PCCP (14-07-2011)“…Monosodium L-glutamate monohydrate, a multiple oxygen site (eight) compound, is used to demonstrate that a combination of high-resolution solid-state NMR…”
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Separation of isotropic chemical and second-order quadrupolar shifts by multiple-quantum double rotation NMR
Published in Journal of magnetic resonance (1997) (01-04-2009)“…Using a two-dimensional multiple-quantum (MQ) double rotation (DOR) experiment the contributions of the chemical shift and quadrupolar interaction to isotropic…”
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Experimental and Theoretical 17O NMR Study of the Influence of Hydrogen-Bonding on CO and O−H Oxygens in Carboxylic Solids
Published in The journal of physical chemistry. A, Molecules, spectroscopy, kinetics, environment, & general theory (09-02-2006)“…A systematic solid-state 17O NMR study of a series of carboxylic compounds, maleic acid, chloromaleic acid, KH maleate, KH chloromaleate, K2 chloromaleate, and…”
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The determination of 17O NMR parameters of hydroxyl oxygen: A combined deuteration and DOR approach
Published in Magnetic resonance in chemistry (01-12-2007)“…The direct detection of hydroxyl oxygen (OH) by 17O double‐rotation (DOR) NMR is very challenging because of the strong OH dipole interaction. It is shown…”
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New opportunities for double rotation NMR of half-integer quadrupolar nuclei
Published in Journal of magnetic resonance (1997) (01-02-2006)“…A combined approach is presented which expands the applicability of double rotation (DOR) by overcoming its most prominent disadvantages: spinning stability…”
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New Limits for Solid-State 17 O NMR Spectroscopy: Complete Resolution of Multiple Oxygen Sites in a Simple Biomolecule
Published in Journal of the American Chemical Society (01-06-2006)Get full text
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The determination of17O NMR parameters of hydroxyl oxygen: A combined deuteration and DOR approach
Published in Magnetic resonance in chemistry (01-12-2007)Get full text
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